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101.
A series of novel copolymers, poly(methacryloyl‐2‐oxy‐1,2,3‐propanetricarboxylic acid‐co‐exo‐3,6‐epoxy‐1,2,3,6‐tetrahydrophthalic acid) [poly(MTCA‐co‐ETAc)], poly(methacryloyl‐2‐oxy‐1,2,3‐propanetricarboxylic acid‐co‐hydrogenethyl‐exo‐3,6‐epoxy‐1,2,3,6‐tetrahydrophthalate) [poly(MTCA‐co‐HEET)], and poly(methacryloyl‐2‐oxy‐1,2,3‐propanetricarboxylic acid‐co‐α‐ethoxy‐exo‐3,6‐epoxy‐1,2,3,6‐tetrahydrophthaloyl‐5‐fluorouracil) [poly(MTCA‐co‐EETFU)], were prepared from corresponding monomers by photopolymerizations at 25°C for 48 h. The polymers were identified by FTIR, 1H‐NMR, and 13C‐NMR spectroscopies. The number‐average molecular weights of the fractionated polymers determined by GPC were in the range from 9400 to 14,900 and polydispersity indices were 1.2–1.4. The in vitro IC50 values of polymers against mouse mammary carcinoma (FM3A), mouse leukemia (P388), and human histiocytic lymphoma (U937) as cancer cell lines and mouse liver cells (AC2F) as a normal cell line were much higher compared to that of 5‐fluorouracil (5‐FU). The in vivo antitumor activities of monomers and polymers against mice bearing sarcoma 180 tumor cell line were better than those of 5‐FU. The inhibition of DNA replication and antiangiogenesis activities of MTCA and copolymers were better compared to those of 5‐FU. © 2004 Wiley Periodicals, Inc. J Appl Polym Sci 94: 57–64, 2004 相似文献
102.
Ju Kumanotani 《Progress in Organic Coatings》1997,34(1-4):135-146
The chemistry and technology of oriental lacquer, proof of long-term durability by a laboratory test, and morphological features of the closely packed shell (polysaccharides–glycoproteins)–core (polymerized urushiol) microgel particles, which are chiefly responsible for degradation due to efflorescence outdoors, are described. The dimerization mechanism of urushiol was demonstrated by separation of over 20 urushiol dimer derivatives. Physiological dimerization of urushiol in the lacquer is very much influenced by the humidity in drying, and the interaction of semiquinone radicals with metal ions, hydrophilic polysaccharides and amphipathic glycoproteins contained in the lacquer. A mechanism for renewable oriental lacquer is proposed, involving harmony of technology and nature within the lacquer tree plantations in south-east Asia. A brief review of studies of lacquer chemistry and synthetic coatings is given. 相似文献
103.
中小学新课改过程中,利用现代信息技术,搞好集体备课,使年轻老师和老教师拧成“一股绳”,建成优秀的教师团队,这样不同班级学生共享到优质的教育教学资源,学校的整体教育教学水平大幅度提升,实现教育公平和教育的均衡发展的。利用信息技术,搞好集体备课,打造好的教师团队,任重道远、我们每个人都责无旁贷。 相似文献
104.
105.
L.?Alonso M.?J.?Fraga M.?JuárezEmail author P.?Carmona 《Journal of the American Oil Chemists' Society》2002,79(1):1-6
A Fourier transform infrared spectroscopic procedure was used to analyze 34 edible fats (22 shortenings and 12 vegetable margarines)
as neat fats (IRNF) to determine their total trans fatty acid (TFA) content. The sloping baseline was corrected with a reference spectrum based on a nonprocessed olive oil.
The calibration was done using seven partially hydrogenated fats with an individual TFA content previously determined by the
combination of gas chromatography (GC) with argentation thin-layer chromatography. Taking into account the different absorptivities
of various trans isomers, different correction factors were calculated using the calibration standards (0.83 and 1.71 for single trans bonds in both diethylene and triethylene and for trans, trans-diethylene fatty acids, respectively) and applied to calculate the total TFA of samples. Moreover, the samples were converted
to their methyl esters and reanalyzed following the same procedure (IRFAME). Differences in TFA content of fats were not found when a t-test was used to compare the results obtained by IRNF vs. either IRFAME or GC, suggesting that IR of neat fats could be used, thus avoiding the need to prepare sample solutions in organic solvents
and to prepare fatty acid methyl esters. The mean TFA content (determined by IRNF) of a representative group of Spanish shortenings (22 samples) that varied widely in terms of fat sources, processes, and
purposes (bakery, sandwiches, ice cream, coatings, chocolate coverings) was 6.55±11.40%, although more than 54% contained
<3% of TFA. Fatty acid composition of shortenings by direct GC using a 100-m polar cyanopolysiloxane capillary column indicated
that the mean trans-18∶2 isomer content was 0.58%, ranging from 0.9 to 3.4%. Small amounts of trans-18∶3 isomers (<0.3%) were observed in 18 of the 22 shortenings studied; the maximal value was <2%. The mean value of the
fraction saturated+TFA of shortenings was high (59.95±12.73%), including two values higher than 83%. 相似文献
106.
铁碳微电解及Fenton氧化法在染料废水处理中的应用 总被引:5,自引:0,他引:5
探讨了铁碳微电解及Fenton氧化法的反应机理、影响因素,总结了微电解和Fenton氧化法的优缺点,概述了微电解与Fenton氧化法联用在废水处理中的应用及其发展前景。 相似文献
107.
以乙酰丙酮为起始原料,经烷基化,羟甲基化,还原,最后与PSCl3环合,成功合成了1-硫代-1-磷杂-3,5-二甲基-4-叔丁基-2,6,7-三氧杂双环[2,2,2]辛烷.目标化合物及部分中间体的结构均通过1H NMR、MS进行了结构确证. 相似文献
108.
在等温条件下,分组对不同初始干-湿段土体含水量、不同时间间隔对非饱和膨胀土的气态水迁移和气液态水混合迁移的规律及其关系进行试验研究,揭示了其随时间的变化过程。试验结果表明,土质情况、含水量水平及含水量梯度对其有重要影响,气态水迁移量与气液混合迁移量都随含水量梯度增加而增加,与时间和位置呈复杂的非线性关系;含水量较小时,土粒对水分的吸附能力较强,致使含水量梯度较大,含水量较大时,土粒周围自由水较多,水分分布较均匀。 相似文献
109.
针对传统高斯噪声去噪算法残余噪声较大的不足,根据噪声对图像视觉的影响,提出了基于像素邻域相关性的去噪算法.首先运用邻域像素的连续性判断像素点是否位于平滑区内;其次对非平滑区根据边缘和纹理的局部连续性运用形态学提取图像边缘和纹理进而定位噪声点;最后对平滑区内的噪声运用自适应邻域进行去噪处理,对非平滑区的噪声仅利用非平滑区的邻域进行平滑,实现了对高斯噪声先定位再去噪.经实验结果验证:与传统方法相比,该算法较好地抑制了图像平滑区内噪声,提高了去噪后图像的视觉效果. 相似文献
110.
地方饮食文化资源及其开发 总被引:1,自引:0,他引:1
鞠明库 《扬州大学烹饪学报》2010,27(4):14-19
地方饮食文化资源是我国悠久饮食文化和丰富旅游资源的重要组成部分,也是当前各地发展饮食业、旅游产业的重要依托。信阳拥有丰富的饮食文化资源,但开发得并不充分,存在诸多问题。开发信阳饮食文化资源的主要策略有:加强对饮食文化资源开发的领导和扶植;大力推进信阳菜发展,弘扬信阳饮食文化;继续举办信阳茶文化节,加快茶文化旅游开发步伐;积极拓展饮食文化资源旅游开发的空间等。 相似文献