天然中子源中子测水技术的初步研究

论述了基于天然中子源的中于测水技术基本原理、仪器设备与方法技术以及在成都地区某地的试验结果。与人工中子源中子测水技术相比．虽然大气中子源方法的灵敏度较差．但避免了人工中子源的辐射防护与管理难题。这对于一些确定地层含水率要求不高．而又需长期监测的场合．如工程地质填图与地质环境动态监测等．天然中子源方法中子测水技术具有一定的应用价值。     

维生素对螺旋霉素发酵的影响

研究了单独添加和组合添加VB1、VB1。和硫辛酸对发酵合成螺旋霉素的影响。结果显示,组合添加0．96mg·L^-1VB1和0．35mg·L^-1硫辛酸时,螺旋霉素产量提高30％。测定结果显示维生素的添加显著增加了乙酸等前体物质的浓度,提高了发酵过程中乙酰激酶、乙酰磷酸转移酶与乙酰CoA合成酶的酶活。由此表明维生素的添加促进螺旋霉素发酵合成可能是因为维生素促进了过程中前体物质的合成,从而增进了内酯环的形成。     

高剂量水平吸收剂量测量用辐射变色薄膜剂量计研究

为建立制备高剂量水平吸收剂量测量的辐射变色薄膜剂量计的方法,对相应的配方及制备工艺进行研究,批量制备了以尼龙为基材,副品红氰化物为染料的辐射变色薄膜剂量计。在60 Coγ参考辐射场中对辐射变色薄膜的各剂量学响应性能进行了研究,结果表明,重复性好于1.0%,在5~210kGy剂量范围内具有较好的剂量响应线性,辐射变色薄膜剂量计辐照后置于低温条件下贮存2周内信号较稳定。此外,该辐射变色薄膜剂量计在本实验范围内未发现明显的剂量率依赖性。通过上述剂量学性能研究,在线性剂量范围内,测量吸收剂量的扩展不确定度为4.2%(k=2)。通过在加速器上进一步实验表明,该膜可用于电子束辐照参数测量。     

FPGA+DDS在激光扫描技术中的应用

针对单路激光扫描光绘机在12 000 DPI精度工作效率低下的缺陷,提出基于FPGA+DDS实现16路激光串行同步扫描的技术.该技术将高速FPGA器件与DDS芯片有机结合起来,原本扫描一个点时间215 ns,经过16路时分复用,在同样的时间内能够完成16个点的扫描.详细介绍了系统的工作原理、硬件设计和相应的软件实现,通过实验测量分析,该技术在高精度条件下,相对4路激光并行扫描光绘机,其工作效率提高了2～4倍.     

EH4音频大地电磁方法在辽东五龙金矿控矿构造及成矿预测研究中的应用

五龙金矿是辽东金矿集区最大的石英脉型金矿床,已累计探明金资源量大于80 t,作为一个开采多年的老矿山,当前面临着矿山资源储量严重不足的问题,亟需寻找深部隐伏资源。通过应用EH4音频大地电磁方法,在五龙金矿的东西两侧分别布设了100线、1000线和1050线3条EH4测量线,采用标量TM模式对原始测量数据进行收集并复核,经计算机处理后绘制出EH4二维反演剖面图。在EH4二维反演剖面图上成功识别出了分别位于矿区东西两侧的100^#断裂和鸡心沟断裂,其垂向延深均超过1 000 m。经过地质观察和坑道钻孔工程揭露,断裂带地表和浅部均存在着明显的金矿化,表明这些断裂在五龙金矿成矿过程中起着重要作用。将EH4音频大地电磁方法应用于五龙金矿控矿构造及成矿预测研究中,取得了良好的效果,矿区东、西部和深部均具有良好的找矿潜力,为矿区下一步地质找矿指明了方向。     

甘肃某金矿选矿试验研究

根据国内某金矿载体矿物的性质,进行了详细的选矿条件试验,获得了较优的工艺参数,最终确定了“一粗两精两扫,中矿顺序返还”的工艺流程。闭路试验结果表明：在磨矿细度为一0．074mm占70％的条件下,可获得产率2．89％、品位85．16g／t、回收率82．17％的金精矿。     

含氟铍矿石冶炼过程中氟的分离工艺研究

对含氟铍矿石冶炼过程中的氟分离工艺进行了研究。当矿石F/BeO=20%～40%时,采用沉淀分离法可以控制氢氧化铍的F/BeO=10%～12%。氢氧化铍经二次除铝、碱洗,可使产品中杂质Al2O3达到低于0 7%的要求。与矿石预处理工艺相比,沉淀法可使每吨氧化铍总成本降低约5000元左右。     

浇注过程的防下渣技术

消除汇流旋涡是防下渣技术开发的首要目标。已有的浇注过程防下渣方法大体可分为3类,即上躲、下藏与抑制。看来抑制法最为积极、有效,特别是用于中间包的名种控流、分渣双功能装置具有显著的综合优势;这类装置的逐步完善与普及,似乎是今后提高连铸水主要技术走向之一。     

Effect of rare earth addition on Cu-Fe/AC adsorbents for phosphine adsorption from yellow phosphorous tail gas

Phosphine(PH3) is a highly toxic air pollutant,commonly produced in phosphorous chemical industry.But it has received less research attention due to its handling difficultly.CO is the main content of the phosphorous chemical industry tail gas,the concentration of which is always more than 80 vol.%,and it can be the feed gas to produce various valuable products such as formate,oxalate,and methanol and so on.But,PH3 is one of the important barriers,which is harmful to the following chemical process.In order to make use of the tail gas,PH3 should be removed firstly,and CO should be covered in the whole purified procedure at the same time.In this work,the modified activated carbon(MAC) was used as the adsorbent to separate PH3 from the mixture tail gas.Series of MAC adsorbents were prepared for the adsorption of PH3,which loaded Cu-Fe and Ce(La),or separately.The PH3 adsorption capacities,chemical and physical properties of MAC were all investigated.The results showed that over 99% PH3 adsorption efficiency was achieved when used MAC adsorbents.The removal efficiency and PH3 adsorption capacity of the Cu-Fe-Ce/AC(20:1:0.4) were both much higher than those modified activated carbons.The maximum PH3 adsorption capacity was 71 mg of PH3/g of MAC on the Cu-Fe-Ce/AC,which were much higher than literature data using CuO only for adsorbing hydride gases.     

Re-determination of the crystal structure of Ca₂Y₈Si₆O₂₆ and study on the luminescent properties of Ca₂Y₈Si₆O₂₆:Tb³⁺

The crystal structure of silicate oxyapatite Ca2Y8Si6O26 was indexed as hexagonal,space group P63/m,a=0.93515 nm,c=0.67872 nm,α=β=90°,γ=120°,V=0.5138692 nm3.Three strong peaks located at 32.079o,32.595o,and 50.104o with d=2.7903,2.74649,1.8194 was in accordance with,(112),and(213) planes.The optimum concentration of Tb3+ in Ca2Y8Si6O26 to yield highest photoluminescence intensity was 10 mol.% of Y3+.The corresponding excitation spectrum consisted of an intense broad band from 220 to 260 nm.The photoluminescence measurements showed that the green emission originated from 5D4-7F5 was predominant in the measured range with strong doublet lines at 543 and 549 nm.