Micro- and nano-scale deformation behavior of nylon 66-based binary and ternary nanocomposites

The primary aim of this paper is to provide an insight on the effect of the location of organoclay on the micro- and nano-scale deformation processes in melt-compounded nylon 66/organoclay/SEBS-g-MA ternary nanocomposites prepared by different blending sequences. In addition, the deformation processes of the ternary nanocomposites were compared to the binary nanocomposites (nylon 66/organoclay and nylon 66/SEBS-g-MA) and neat nylon 66. The incorporation of SEBS-g-MA particles toughened nylon 66 markedly; but the flexural modulus and strength were both reduced. Conversely, the use of organoclay increased the modulus but decreased the fracture toughness of nylon 66. Nylon 66/SEBS-g-MA/organoclay ternary nanocomposites exhibited balanced elastic stiffness and toughness. Stress-whitening studies of the fracture surfaces in terms of gray level were also performed and an attempt was made to correlate the optical reflectivity characteristics with fracture toughness. It was concluded that the capability of SEBS-g-MA particles to cavitate was decreased by the presence of organoclay in the SEBS-g-MA phase, resulting in reduced toughening efficiency. The best micro-structure for toughness and other mechanical properties is thus to maximize the amount of exfoliated organoclay in the nylon 66 matrix rather than to have it embedded in the finely dispersed SEBS-g-MA particles.     

零电压零电流开关全桥PWM变换器的研究

文本通过分析全桥ZVZCS PWM变换器的工作原理,得出其与传统的全桥ZVZCS PWM变换器的不同之处,然后具体分析对于变化的负载电流,电路环流是如何自我调节以实现ZCS的,并给出了一些影响实现ZVZCS的关键元器件的参数设计公式。最后样机的试验波形证了本文的分析研究。     

数字水印演化设计

数字水印算法中相关参数的选择是水印算法设计的一个关键问题。不同的参数选取，将直接影响到算法的有效性。该文给出一种采用演化计算进行水印参数有效选择的方法，实验结果表明，这种方法在提高水印健壮性的同时保证保真度。     

4Cr5MoSiV1热作模具钢锻造加热工艺的改进

攀长钢生产的4Cr5MoSiV1热作模具钢锻材存在超声波探伤合格率较低的问题。分析认为主要原因是沿用较低的锻前加热温度，钢锭加热程度不足造成锻造时大锻材中心没有充分锻透。笔者对4Cr5MoSiV1钢锻造加热工艺进行了递进式改进，逐步调整钢锭加热制度从1180℃最终提高到1270℃．1290℃，同时相应调整退火工艺制度，基本解决了上述问题，探伤废品大幅降低，锻造火次也明显减少，并避免高温加热引起的粗晶降低钢材使用性能，取得了显著的工艺改进效果。另外，采用高温加热也使钢中的显微偏析明显减轻，获得了部分的均匀化扩散退火的效果：一次碳化物减少，尺寸变小，没有尖锐的棱角，冲击韧性比工艺改进前有明显提高。     

特高压通道降压运行时安徽500kV西通道建设必要性分析

根据华东1000kV特高压输电通道初期降压运行的统筹安排，结合淮南煤电基地电源、平圩电厂二期及蚌埠电厂等电源的装机进度，通过对各电源接入系统方案的计算分析，最后得出结论：为保证江北地区电力送出，安徽500kV西路过江通道在“十一五”期间建成是有必要的。     

Characterization of (Y,Gd) BxV1-xO4-x:Eu Phosphor Prepared by Coprecipitation Reaction

White body-color (Y, Gd)BxV1- xO4-x :Eu3 phosphors were prepared by coprecipitation reaction. Under VUV excitation at 147 nm, the red emission colorimetric purity of (Y, Gd)BxV1- xO4-x :Eu3 phosphor is much better than that of commercial PDP (plasma display panels) phosphor (Y, Gd)BO3:Eu3 . But its relative emission intensity is only about 90% of the commercial phosphor.     

住宅小区智能化系统工程初探

文章对住宅小区智能化的概念和功能进行了详细介绍,重点阐述了计算机、通信与网络、自控、IC卡技术在以住宅小区为代表的数字化人居环境发展中的作用与意义,并针对建设与管理存在的问题提出了合理化建议。     

压水堆一回路模拟腐蚀氧化物的溶解去污试验

本文介绍了对两种压水反应堆一回路模拟腐蚀氧化物（铁镍铬氧化物和铁镍氧化物）的溶解去污试验结果。选择的去污剂为0.3%草酸、0.1%柠檬酸和0.1%高锰酸钾。结果表明，实验温度为95℃、去污时间在6－48h范围内，0.3%草酸对铁镍铬氧化物和铁镍氧化物的溶解率分别为24.1%-65.3%和4.9%-64.4%；0.1%柠檬酸对二者的溶解率分别为2.2%-4.4%和0.37%-1.55%；0.1%高锰酸钾对二者几乎没有溶解作用。采用在草酸或柠檬酸去污前使用高锰酸钾去污剂的二步去污法，对两种氧化物的溶解度小于单独使用草酸或柠檬酸去污的一步法。     

Rare earth elements in CO_2-fluid inclusions in mantle Iherzolite

Trace elements including REE (Rare Earth Elements) in fluid inclusions in Iherzolite, olivine, orthopyroxene, and clinopyroxene have been determined by heating-decrepitation and ICP-MS (Element Type Inductively Coupled Plasma-Mass Spectrometry) method. Normalized CO2 fluid/chondrite data show that mantle fluids are rich in REEs, especially LREEs (Light Rare Earth Elements), several times or dozen times higher than mantle rocks and mantle minerals. There are close relationships among the REE data of olivine, orthopyroxene, clinopyroxene and 1herzolite. Compared to the data of chemical dissolution method, it is believed that REE data obtained from heating-decrepitation and ICP-MS technique are contributed by CO2 fluid inclusions. About 60% (mass fraction) of tiny inclusions are observed not to be decrepitated above 1000℃, so REE data obtained are only contributed by decrepitated inclusions. Mantle fluids rich in LREE play an important role in mantle metasomatism, partial melting and mineralization.