Ozonation of CI Reactive Black 5 using rotating packed bed and stirred tank reactor

This study investigates the ozonation of CI Reactive Black 5 (RB5) by using the rotating packed bed (RPB) and completely stirred tank reactor (CSTR) as ozone contactors. The RPB, which provides high gravitational force by adjusting the rotational speed, was employed as a novel ozone contactor. The same ozone dosage was separately introduced into either the RPB or the CSTR for the investigation, while the experimental solution was continuously circulated within the apparatus consisting of the RPB and CSTR. The decolorization and mineralization efficiencies of RB5 in the course of ozonation are compared for these two methods. Moreover, the dissolved and off‐gas ozone concentrations were simultaneously monitored for the further analysis. As a result, the ozone mass transfer rate per unit volume of the RPB was significantly higher because of its higher mass transfer coefficient and gas–liquid concentration driving force. Furthermore, ozonation kinetics was found to be independent of the gravitational magnitude of an ozone gas–liquid contactor. Therefore, the results suggest employing RPBs as ozone‐contacting devices with the advantage of volume reduction. The experimental results, which can be used for further modeling of the ozonation process in the RPB, also show the requirement of correct design for the RPB. Consequently, the present study is useful for the understanding of practical application of RPBs. Copyright © 2004 Society of Chemical Industry     

Tensile and flexural creep rupture tests on partially-damaged concrete specimens

Three series of novel tensile and flexural creep tests on partially-damaged concrete specimens were carried out in order to gain some insight into creep crack growth and failure of strain-softening materials. In the tests, each specimen was initially loaded to a given point in the descending branch and thus had a lower load-carrying capacity than that at the peak-point. Then, the specimen was unloaded and reloaded to sustain a load which was from 70% to 95% of its current load-carrying capacity. Experimental creep curves display a three-stage process, consisting of primary, secondary and tertiary stages, with a decreasing, constant and increasing creep rate, respectively. The secondary stage dominates the whole failure lifetime, whereas both the secondary and tertiary stages are important in terms of creep deformation. Failure life-time seems to be more sensitive to the change of load level in flexural tests rather than in tensile tests. The decrease in load-carrying capacity due to damage tends to result in a shorter failure lifetime and a lower critical load level for creep rupture. The descending branch of the static load-deflection or load-CMOD curve may be used as an envelope criterion for creep fracture.     

烧成及热处理工艺对钛酸锶铅基热敏材料性能及显微结构的影响

研究了烧成及热处理工艺对钛酸锶铅基热敏材料的阻温特性及显微结构的影响。通过扫描电镜（ＳＥＭ）和能量分散仪（ＥＤＡＸ）分析了材料的显微结构及不同形貌晶粒的成份。通过对组成、烧成及热处理工艺的控制，可得到具有Ｖ型ＰＴＣＲ特性的热敏材料。     

正交双频光栅CCD系统剪切干涉测量二维温度场

以半导体激光器为光源，利用正交双频光栅（ＯＤＦＧ）ＣＣＤ系统剪切干涉对带平板边界的半圆柱体热源的二维温度场进行实时诊断，分析剪切干涉图时，用柱函数系作为拟合基底，给出二维自然对流温度场的定量分布。     

改善磁盘阵列性能的方法

磁盘阵列是解决计算机Ｉ／Ｏ瓶颈问题的有效方法之一，通过对现有磁盘阵列结构的研究，提出了４种改善磁盘阵列性能的方法，即良分利用磁盘带宽，平衡多盘的负载，减少奇偶检验数据存取时间和磁盘阵列Ｃａｃｈｅ技术等，分析结果表明：在事务处理应用领域，利用Ｃａｃｈｅ来把小写转化为大写可大大改善目前一般情况下，以一道数据大小来作为磁盘的基本存取大小是合适的选择，磁盘阵列负载平衡设计不足是指正常模式下系统请求在多盘间     

GIS技术与微机制图

地理信息系统（ＧＩＳ）随着信息社会的发展愈发显示出强大的生命力。本文简要叙述ＧＩＳ的重要作用及其发展进程中涌出出来的四个设计模型，总结了运用ＧＩＳ国产软件平台ＭＡＰＧＩＳ制作遥感地质构造解译图的工作步骤和技术方法。     

浅谈托辊的开发与实践

本钢１７００连轧机应用的托辊原由外企业制作，为了减少公司资金外流，公司技术人员和工人结合现有的生产条件，先后攻克了辊身铸造和加工，托辊装配等工艺方面的难关，研制成功了合格的产品，年创经济效益８０万元。     

高性能各向异性Sm2Fe17Nx磁粉的制备

本文研究了高性能各向异性Ｓｍ２Ｆｅ１７Ｎｘ磁粉的制备工艺路线与工艺参数。优化了制备与工艺参数。已制备出磁性能达到：Ｂｒ＝１．３９Ｔ，Ｈｃｉ＝８５０ＫＡ／ｍ和（ＢＨ）ｍ＝２３６ＫＪ／ｍ＾３的各向异性Ｓｍ２Ｆｅ１７Ｎ２．８８磁粉，该磁粉的各向异性场ＨＡ达到２０Ｔ。