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991.
992.
Chunnuan Ji Rongjun Qu Cheng Bo Cao Huo Chen Qiang Xu Changmei Sun Chunhua Wang Huafang Yuan Jun Zhou 《应用聚合物科学杂志》2006,102(6):6054-6059
A novel chelating resin containing sulfoxide and diethylene glycol, poly{4‐vinylbenzyl‐[2‐2‐(hydroxyethyl)ethoxyl]sulfoxide} (PVESO) was synthesized using chloromethylated polystyrene (PS‐Cl) as material. Its structure was characterized by elemental analysis, infrared spectra, and scanning electron microscopy (SEM). The adsorption capacities of the resin for Hg2+, Ag+, Cu2+, Zn2+, and Pb2+ at various pH values were determined. The maximum adsorption capacities for Hg2+ and Ag+ were 1.56 and 0.75 mmol g?1 respectively. The resin had high selectivity for Hg2+ and Ag+ over the pH range 1.0–7.0. The adsorption capacities for Hg2+ and Ag+ under competitive condition were also determined by batch experiment method. In addition, the adsorption kinetics of the resin towards Hg2+ at different temperatures was also investigated. The results showed that the adsorption rate was governed by film diffusion at 20°C and 25°C, by particle diffusion at 30°C and 35°C. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 6054–6059, 2006 相似文献
993.
本文利用易于控制流速的旋转圆盘电极研究了SiC微粒与Cu的共沉积。得出了在不同镀液流动速度下镀得的复合镀层中微粒含量与镀液中微粒浓度以及与电流密度之间的关系曲线,进而探讨了镀液流速对Cu-SiC共沉积的影响。镀液流速通过影响微粒与阴极之间的弱吸附影响微粒在阴极表面的停留,从而对Cu-SiC复合电沉积过程产生很大影响。 相似文献
994.
Boron-based metal-free catalysts for oxidative dehydrogenation of propane (ODHP) have drawn great attention in both academia and industry due to their impressive activity and olefin selectivity. Herein, the SiO2 and B2O3 sequentially coated honeycomb cordierite catalyst is designed by a two-step wash-coat method with different B2O3 loadings (0.1%-10%) and calcination temperatures (600, 700, 800 ℃). SiO2 obtained by TEOS hydrolysis acts as a media layer to bridge the cordierite substrate and boron oxide via abundant Si-OH groups. The welldeveloped straight channels of honeycomb cordierite make it possible to carry out the reactor under high gas hourly space velocity (GHSV) and the thin wash-coated B2O3 layer can effectively facilitate the pore diffusion on the catalyst. The prepared B2O3/SiO2@HC monolithic catalyst exhibits good catalytic performance at low boron oxide loading and achieves excellent propylene selectivity (86.0%), olefin selectivity (97.6%, propylene and ethylene) and negligible CO2 (0.1%) at 16.9% propane conversion under high GHSV of 345,600 ml·(g B2O3)-1·h-1, leading to a high propylene space time yield of 15.7 g C3H6·(g B2O3)-1·h-1 by suppressing the overoxidation. The obtained results strongly indicate that the boron-based monolithic catalyst can be properly fabricated to warrant the high activity and high throughput with its high gas/surface ratio and straight channels. 相似文献
995.
996.
Zhi-Ping Jiang Wei Xi Xiangyang Li Shaojie Tang Ji-Zhong Zhao Jin-Song Han Kun Zhao Zhi Wang Bo Xiao 《计算机科学技术学报》2014,29(4):589-604
Numerous indoor localization techniques have been proposed recently to meet the intensive demand for location-based service (LBS). Among them, the most popular solutions are the Wi-Fi fingerprint-based approaches. The core challenge is to lower the cost of fingerprint site-survey. One of the trends is to collect the piecewise data from clients and establish the radio map in crowdsourcing manner. However the low participation rate blocks the practical use. In this work, we propose a passive crowdsourcing channel state information (CSI) based indoor localization scheme, C2IL. Despite a crowdsourcing based approach, our scheme is totally transparent to the client and the only requirement is to connect to our 802.11n access points (APs). C2IL is built upon an innovative method to accurately estimate the moving speed solely based on 802.11n CSI. Knowing the walking speed of a client and its surrounding APs, a graph matching algorithm is employed to extract the received signal strength (RSS) fingerprints and establish the fingerprint map. For localization phase, we design a trajectory clustering based localization algorithm to provide precise real-time indoor localization and tracking. We develop and deploy a practical working system of C2IL in a large office environment. Extensive evaluations indicate that the error of speed estimation is within 3%, and the localization error is within 2 m at 80% time in a very complex indoor environment. 相似文献
997.
998.
甲酸甲酯合成与转化的催化技术 总被引:3,自引:0,他引:3
本文评述了甲酸甲酯(MF)合成与转化的催化技术,展示了从MF出发发展C_1化学的可能途径,在MF的合成方面详细地分析了从甲醇出发的羰化法、脱氢法和氧化法催化技术,简介了我们的有关研究工作。 相似文献
999.
Stephen Q. Zhou Liming Wang Xiugao Liao Georges Manuel William P. Weber 《Journal of Inorganic and Organometallic Polymers and Materials》1991,1(2):199-210
High molecular weight poly(1,1-dimethyl-1-germa-cis-pent-3-ene), poly(1,1-diphenyl-1-germa-cis-pent-3-ene), poly(1,1-dimethyl-1-sila-cis-pent-3-ene), and poly(1-methyl-1-phenyl-1-sila-cis-pent-3-ene) have been prepared. The thermal stability of these polymers is found to increase with their molecular weight. 相似文献
1000.
进行了充气压力对充气工况载重斜交轮胎影响的有限元分析.结果表明,充气工况下,充气压力对斜交轮胎外形轮廓尺寸影响明显,其外直径、断面宽度均随充气压力的增大而增加;充气压力的大小对胎圈接触应力分布影响很小,但胎圈最大接触应力随充气压力的增加而增大. 相似文献