元明青花红绿彩的研究与考证

青花红绿彩作为加彩器的一种,比传统的观点早一个朝代,根据明中青花红绿彩盖罐结合最新的窑址考古成果,得出元代的窑炉设计和釉面配方的缺陷,使元代青花红绿彩的生产和存世极少,明官窑中由于斗彩的出现,青花红绿彩在民间一直沿烧。与元代风格相近,只是到了后期风格才大变。     

非晶态NiB配位催化2-亚丁基环己酮的选择加氢动力学研究

以超细非晶态NiB为催化剂、乙醇为溶剂 ,研究了常压条件下 2 -亚丁基环己酮的选择催化氢化反应。确定了反应对 2 -亚丁基环己酮的反应级数n =1,80℃下准一级反应的速率常数为k =3.4× 10 -3 min-1。同时考察了氢化过程中外扩散的影响以及温度、催化剂用量对反应的影响。求得反应的活化能Ea =16 .391kJ/mol。     

Two-dimensional bilinear preserving projections for image feature extraction and classification

Two-dimensional locality preserving projections (2DLPP) was recently proposed to extract features directly from image matrices based on locality preserving criterion. A significant drawback of 2DLPP is that it only works on one direction (left or right) to reduce the dimensionality of the image matrices and thus too many coefficients are needed for image representation in low-dimensional subspace. In this paper, we propose a novel method called two-dimensional bilinear preserving projections (2DBPP) for image feature extraction. We generalized the image-based (2D-based) feature extraction techniques into bilinear cases, in which 2DLPP is a special case of our proposed method. In order to obtain the bilinear projections, we proposed an iteration method by solving the corresponding generalized eigen-equations. Moreover, analyses show that 2DBPP has stronger locality preserving abilities than 2DLPP. By using the label information and defining different local neighborhood graphs, the proposed framework is further extended to supervised case. Experiments on three databases show that 2DBPP and its supervised extension are superior to some other image-based state-of-the-art techniques.     

高分子铁盐絮凝剂制备及其应用研究

研究了以废铁屑和工业硫酸亚铁为原料,在常压和加热条件下,用氯酸钾作为氧化剂制取聚合硫酸铁(PFS)的工艺条件,并在PFS制备的基础上,合成了聚磷硫酸铁(PPFS)和聚氯硫酸铁(PFCS)。将所制备的聚铁用于污水处理实验,结果表明:用该方法制备的聚铁絮凝剂对实际水样具有较好的混凝处理效果,且制备工艺简单、速度快,从根本上消除了用NaNO_2催化氧化法制备聚铁对环境造成的二次污染。     

基于先验知识的肝脏轮廓线提取算法研究

准确有效地提取肝脏CT序列的轮廓线是腹部软组织三维模型重建与可视化的关键问题之一。针对肝脏轮廓线提取准确性不高的问题, 提出了一种基于先验知识的肝脏轮廓线提取算法。首先利用拉普拉斯算法进行CT图像增强, 再利用基于边缘先验知识的套索模型对感兴趣区域进行半自动的初始化, 最后通过改进的Snake算法准确地提取肝脏CT图像的边缘。针对序列CT肝脏的边缘提取, 提出根据CT图像序列之间的相关性, 将上一幅图像的轮廓线提取结果作为下一幅CT图像边缘提取的初始化点, 接着批处理地提取CT序列的肝脏边缘。实验结果表明：该算法大大减少了手动初始化结果对目标边缘轮廓准确提取的依赖性, 并有效地解决了肝脏轮廓线的提取问题。     

An Intra-Server Interconnect Fabric for Heterogeneous Computing

With the increasing diversity of application needs and computing units, the server with heterogeneous pro- cessors is more and more widespread. However, conventional SMP/ccNUMA server architecture introduces communication bottleneck between heterogeneous processors and only uses heterogeneous processors as coprocessors, which limits the efficiency and flexibility of using heterogeneous processors. To solve this problem, this paper proposes an intra-server inter- connect fabric that supports both intra-server peer-to-peer interconnection and I/O resource sharing among heterogeneous processors. By connecting processors and I/O devices with the proposed fabric, heterogeneous processors can perform direct communication with each other and run in stand-alone mode with shared intra-server resources. We design the proposed fabric by extending the de-facto system I/O bus protocol PCIe （Peripheral Computer Interconnect Express） and implement it with a single chip cZodiac. By making full use of PCIe＇s original advantages, the interconnection and the I/O sharing mechanism are light weight and efficient. Evaluations that have been carried out on both the FPGA （Field Programmable Gate Array） prototype and the cycle-accurate simulator demonstrate that our design is feasible and scalable. In addition, our design is suitable for not only the heterogeneous server but also the high density server.     

The adsorption of dyes from aqueous solution using diatomite

Raw diatomite was calcined at 450 °C for dyes removal from aqueous solution. SEM and FTIR analysis show that the raw diatomite contains organic impurities, which are removed after the calcination. The impurities removal decreases the specific surface area and increases the average pore diameter of raw diatomite, while improves its adsorption capability of dyes. The adsorption isotherm and kinetics experiments of methylene blue onto calcined diatomite were then carried out to investigate the adsorption property. It shows that the adsorption capacity of methylene blue is about 50 mg/g. The adsorption isotherm was fitted by the Langmuir, Freundlich and Redlich-Peterson models, which reveals that the Redlich-Peterson isotherm is the best one. Two kinetic models, pseudo-first order and pseudo-second order, were rearranged for expediently investigating the adsortpion mechanisms. Fitting results show that the pseudo-first-order model is better in describing the adsorption process.     

邻氟苯甲腈的合成研究

以邻甲苯胺为原料 ,采用四步反应法合成邻氟苯甲腈。 (1)邻甲苯胺经西曼反应合成邻氟甲苯 ,收率 6 5 % ;(2 )邻氟甲苯经氯化、水解得到邻氟苯甲醛 ,以过氧化苯甲酰为氯化引发剂 ,氧化锌为水解催化剂 ,收率 80 % ;(3)邻氟苯甲醛经肟化反应得到邻氟苯甲醛肟 ,收率 87% ;(4)肟用乙酸酐脱水合成出邻氟苯甲腈 ,收率 76 % ,产品质量分数大于 99%。     

离子膜电解槽阴极系统两次轻微爆炸事故分析

分析离子膜电解槽开停车过程中在阴极系统发生的轻微爆炸事故,找到了爆炸发生的主要部位在阴极总管系统,找出其原因是漏入的空气与氢气接触,并提出了预防事故发生的措施。     

GOR-C降烯烃催化剂的工业应用

大庆炼化公司林源生产指挥部催化裂化装置原料油为典型石蜡基原油的常压渣油，生产的催化汽油中的烯烃含量较高，为此试用长岭炼化公司催化剂厂生产的降烯烃催化剂GOR-C。结果表明，降烯烃效果明显，产品分布无明显变化，能满足现有生产要求，经济效益显著。