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91.
熔融-固相缩聚法中固相聚合对聚乳酸合成的影响 总被引:2,自引:0,他引:2
以L 乳酸单体为原料 ,熔融 -固相缩聚法合成了聚乳酸 ,重点研究了固相聚合的工艺条件。结果表明 ,绝对压力 60Pa ,氯化亚锡为催化剂 ,分段控温 ,可使聚乳酸的粘均分子量提高到固相聚合反应前的 5 3倍。通过对固相聚合产物的结晶度和熔点的分析 ,探讨了固相聚合的机理。 相似文献
92.
Yanqiu Shao Jiqing Han Ting Liu Yongzhen Zhao 《International Journal of Speech Technology》2007,10(1):45-55
In real speech, not like lexical words (LWs), prosodic words (PWs) are basic rhythmic units. The naturalness of a Text-to-Speech
(TTS) system is directly influenced by the segmentation of the PWs. Most of the PWs are the combination of several LWs. In
this paper, three Lexical Combination Models are proposed to combine LWs into PWs, including a Directed Acyclic Graph Model,
a Segmentation Model and a Markov Model (MM). To cope with the situation where some long LWs should be segmented into two
or more PWs, a Lexical Split Model (LSM) is applied to the long LWs. Experimental results prove that relatively constant results
with various training data can be obtained from a MM. The Transformation-Based Error Driven Learning (TBED) algorithm, for
its high performance of individual property, is applied in combination with the MM to improve the precision of PW segmentation.
Experiments show that among the three proposed models, the MM combined with TBED and LSM, leads to the best performance, in
which a precision of 93.00% and a recall of 93.23% are achieved. The perception test indicates that by using PWs as the lowest
prosodic units a speech sounds more natural and acceptable than by using LWs.
This paper is supported by NSFC Project (60503071); 973 Natural Basic Research Program of China (2004CB318102); Postdoctor
Science Foundation of P. R. China (20070420275). 相似文献
93.
Y. G. Wang H. Q. Ye K. H. Kuo X. J. Feng S. Z. Long G. L. Lao 《Journal of Materials Science》1991,26(23):6325-6330
The microstructures of unhydrated calcium aluminosulphate Ca4Al6SO16 and Ca3SrAl6SO16 have been studied by high-resolution electron microscopy (HREM). The results showed that twinning and twinned slabs could be introduced taking the [1 1 2] direction as the twin axis so that it seems to be coincident with the law of twinning formed in body-centred cubic structures. A previously reported superlattice with a repeat period twice that of the fundamental structure along the 〈1 1 0〉 direction has also been found in both matrix and twin variants. The close intergrowth of Ca3SrAl6SO16 and another phase, possibly Sr3Al2O6 existing as an inclusion between these two twin variants, was determined and clearly revealed by electron diffraction and HREM images. The coherent interphase boundaries and orientation relationship between them can also be deduced. 相似文献
94.
A novel series of temperature‐sensitive poly[(N‐isopropylacrylamide)‐co‐(ethyl methacrylate)] (p(NIPAM‐co‐EMA)) microgels was prepared by the surfactant‐free radical polymerization of N‐isopropylacrylamide (NIPAM) with ethyl methacrylate (EMA). The shape, size dispersity and volume‐phase transition behavior of the microgels were investigated by transmission electron microscopy (TEM), ultraviolet–visible (UV–Vis) spectroscopy, dynamic light scattering (DLS) and differential scanning calorimetry (DSC). The transmission electron micrographs and DLS results showed that microgels with narrow distributions were prepared. It was shown from UV–Vis, DLS and DSC measurements that the volume‐phase transition temperature (VPTT) of the p(NIPAM‐co‐EMA) microgels decreased with increasing incorporation of EMA, but the temperature‐sensitivity was impaired when more EMA was incorporated, causing the volume‐phase transition of the microgels to become more continuous. It is noteworthy that incorporation of moderate amounts of EMA could not only lower the VPTT but also enhance the temperature‐sensitivity of the microgels. The reason for this phenomenon could be attributed to changes in the complicated interactions between the various molecules. Copyright © 2004 Society of Chemical Industry 相似文献
95.
Carboxyl‐terminated butadiene‐acrylonitrile rubber (CTBN) has often been used to improve the toughness of cyanate ester (CE) resin while sacrificing modulus and thermostability. In this paper, the addition of the appropriate amount of epoxy resin (EP) to the CE/CTBN system is shown to not only increase the modulus and thermostability of the blend, but also improve the toughness. The values of impact strength showed a maximum for the CE/CTBN/EP 100/5/5 blend. The temperature of 10 % weight loss (T10) improves from 376 °C for CE/CTBN 100/5 to 407 °C for the CE/CTBN/EP 100/5/2.5 blend. It is proposed that addition of the appropriate amount of EP can decrease the mobility and increase the stability of CTBN via the reaction between the terminal carboxyl group of CTBN and the hydroxyl group of EP. But a very high EP concentration will decrease the crosslinking density of CE, consequently reducing the mechanical properties and thermostability of the blends. Copyright © 2004 Society of Chemical Industry 相似文献
96.
97.
Most algorithms on receiver autonomous integrity monitoring (RAIM) are under the assumption of a single-satellite fault, because there is an extremely small probability that significant simultaneous multiple-satellite faults may occur. However, after the implementation of the Galileo system in a few years, there will be more satellites in view for the user to utilise together with GPS satellites, and a combination of them will bring better performance for RAIM. On the other hand, with the help of wide area augmentation system and the use of dual-frequency operation, pseudo-range errors will be reduced greatly. Thus, tighter alert limits are required for RAIM, and formerly `small' errors should not be neglected. All of those factors make it necessary to consider simultaneous multiple-satellite faults. A detailed theoretical analysis of RAIM under the condition of two-satellite faults for both vertical and horizontal directions is presented. The characteristic/max slopes for every pair of satellites are then deduced in order to calculate the tighter vertical/horizontal protection level for RAIM 相似文献
98.
99.
100.
An efficient algorithm for the random packing of spheres can significantly save the cost of the preparation of an initial configuration often required in discrete element simulations. It is not trivial to generate such random packing at a large scale, particularly when spheres of various sizes and geometric domains of different shapes are present. Motivated by the idea of compression complemented by an efficient physical process to increase packing density, shaking, a new approach, termed compression algorithm, is proposed in this work to randomly fill any arbitrary polyhedral or cylindrical domains with spheres of various sizes. The algorithm features both simplicity and high efficiency. Tests show that it takes 181 s on a 1.4-GHz PC to complete the filling of a cylindrical domain with a total number of 26,787 spheres, achieving a packing density of 52.89%. 相似文献