四倍频Nd：YAG激光在高压氢气中的喇曼频移研究

利用Nd:YAG固体激光器四倍频输出(266nm)在高压H₂中的受激喇曼散射获得多波长的激光输出。当泵浦能量一定时,通过改变H₂压力得到了最佳的能量输出,299nm波长的激光能量为3mJ,341nm波长的激光能量输出为6.1mJ,398nm波长的激光能量输出为2.8mJ,239nm波长的激光能量输出为0.8mJ,同时在477nm,595nm,218nm,200nm波段也有能量输出。     

KQl50潜孔钻机的改造

我公司矿山车间原有KQ150潜孔钻机4台,工作气压0.5～0.8MPa,单台耗气量15.4m3/min,配置低风压QCZ150型冲击器及钻头(钻孔直径Φ150mm),钻杆直径Φ108mm。供风设备为5L-40/8-Ⅰ型空气压缩机4台,供风管道2000余m。由于空压机至潜孔钻供风管路过长,管路维护困难,漏风多,管路压力损失大;钻杆采用插入式联接,密封性差,故障率高。以上情况造成潜孔钻实际工作风压低,冲击器冲击能力减弱,粉渣重复破碎,进尺效率低(8h进尺约35m),能耗高,冲击器、钻头、钻杆等配件消耗高,成本高。因此公司于2000年11月将KQ150潜孔钻机改造为高风压潜孔钻机,淘汰5L…     

Lutein and lutein esters in marigold flowers by high performance chromatography

Lutein and lutein esters in marigold flowers was quantitatively determined by high performance chromatography (HPLC) with ODS-C18 column. A mixture of CH3CN-CH3OH-CH3COOCH2CH2 with volume ratio of 55:1:44 was used as mobile phase at a flow rate of 1.0mL/min and detection was carried out at 480 nm. The column temperature was about 20℃. The contents of lutein and lutein esters were determined by analytical curve of lutein since lutein and lutein esters have the same spectral characteristics. Determination results of hexane extracts and saponified samples of lutein show that the saponification transforms the esters into free lutein. The increase of the content of dipalmitate and palmitate stearate reveals that the reaction includes transesterifications.     

MS方法的一个新证明及其结构优化算法

本文给出Ｍｉｌｎｅ－Ｓｉｍｐｓｏｎ（ＭＳ）预测─校正法新的导出方法，并以结构优化思想设计出通用性和可靠性较强的算法。     

锌合金压铸件古铜色钝化

介绍了锌合金压铸件古铜色钝化的工艺化影响因素。该工艺简单，成本低廉，钝化膜硬度高、耐磨、结合力和抗变色性能强。     

油井腐蚀因素探讨

对影响油井腐蚀的各种主要因素进行了系统的分析和探讨，为油井腐蚀的控制提供有效的理论依据。