活性纳米ZnO的制备

用成本低廉的锌焙砂为原料 ,通过直接沉淀法首先合成前驱物碱式碳酸锌 ,然后烘干分解得到活性纳米ZnO粉体。TG -DTA表明前驱物为碱式碳酸锌 ,XRD估测颗粒尺寸为 90nm ,产品气敏度为 17.8。     

Fe掺杂A-TiO_2在溴甲酚绿中的可见光催化活性及动力学

以FeCl_3·6H_2O为Fe源,采用水热法制备了Fe掺杂锐钛型TiO_2(A-Ti O2)光催化剂。以溴甲酚绿为降解对象,考察溴甲酚绿的初始浓度、催化剂用量、掺Fe量等因素对自制催化剂可见光催化降解反应的动力学方程的影响。结果表明:在40 W白炽灯照射下,当溴甲酚绿初始浓度为10 mg/L(pH=7)、催化剂的用量为0.6 g/L、掺Fe量为4%(摩尔分数)、室温下反应时间为3 h时,溴甲酚绿的降解率最大为76.05%。溴甲酚绿光催化降解曲线符合一级反应动力学方程,于上述最佳条件下其表观反应速率常数k达到最大值,为0.389 7 h-1。     

Measurement and modeling solubility of bioactive coumarin and its derivatives in supercritical carbon dioxide

To design a supercritical fluid extraction process for the separation of bioactive substances from natural products, a quantitative knowledge of phase equilibria between target biosolutes and solvent is necessary. How-ever, mostly no such information is available in literature to date. Thus in the present study, illustratively the solubility of bioactive coumarin and its various derivatives (i.e., hydroxy-, methyl-, and methoxy-derivatives) in supercritical CO₂ were measured at 308.15–328.15 K and 10–30 MPa. Also, the pure physical properties such as normal boiling point, critical constants, acentric factor, molar volume and standard vapor pressure for coumarin and its derivatives were estimated. By these estimated information, the measured solubilities were quantitatively correlated by an approximate lattice equation of state proposed recently by the present authors.     

垃圾焚烧管式布风流化床的冷态实验

在床截面为300mm×300mm、床高为4. 4m的管式布风流化床实验台上,分别对宽筛分下不同颗粒粒度、不同床层高度、不同截面流速、布风的均匀性以及非平衡布风时颗粒流化特性进行实验研究,为未来垃圾衍生燃料的流化燃烧实验提供基础数据。管式布风流化床的开孔方向与夹角大小对床层压降变化影响明显,向下开孔角度越小,动能消耗越大,但床层稳定性能好。随着料层高度增加,各布风管间的布风更趋于平衡,流化的稳定与均匀性能也越好。管组压降失衡时,床层压降不平衡明显增加,波动幅度增大,不稳定性明显高于正常流化状态。     

纳米SiO_2表面改性及其在水性涂料中的应用

通过正交实验筛选出最隹分散工艺,将改性后的纳米级多孔SiO2加入到水性苯丙乳液涂料中配制出水性纳米涂料,并对其涂料进行了性能测试。     

纯低温余热电站项目介绍

山东东华水泥有限公司是隶属于淄博矿业集团有限责任公司的子公司，东华水泥5000t／d新型干法水泥熟料线是淄矿建设“煤、电、材”产业链的建材板块龙头项目，第一条5000t／d水泥熟料生产线已于2005年2月投产，目前生产稳定，产品质量优良。配套200万吨粉磨站于2005年11月顺利投产。东华公司根据本公司的实际情况，结合国家资源综合利用的产业政策，委托天津水泥工业设计院设计，利用5000t／d水泥熟料生产线的余热配套一座纯低温余热电站（同时对2号5000t／d水泥熟料生产线配套余热电站进行规划）。     

Annotating korean text documents with linked data resources

Semantic annotation approaches link entities from a knowledge base to mentions of entities in text to provide additional content-related information. Recently increasing use of resources from the Linked Open Data (LOD) Cloud has been made to annotate text documents thanks to the network of machine-understandable, interlinked data. While existing approaches to semantic annotation in the LOD context have been proven to be well performing with the English language, many other languages in general and the Korean language in particular are still underrepresented. We investigate the applicability of existing semantic annotation approaches to the Korean language by adapting two popular approaches in the semantic annotation field and evaluating those approaches on an English-Korean bilingual sense-tagged corpus. Further, general challenges in internationalization of annotation approaches are summarized.     

Speech driven photo realistic facial animation based on an articulatory DBN model and AAM features

This paper presents a photo realistic facial animation synthesis approach based on an audio visual articulatory dynamic Bayesian network model (AF_AVDBN), in which the maximum asynchronies between the articulatory features, such as lips, tongue and glottis/velum, can be controlled. Perceptual Linear Prediction (PLP) features from audio speech, as well as active appearance model (AAM) features from face images of an audio visual continuous speech database, are adopted to train the AF_AVDBN model parameters. Based on the trained model, given an input audio speech, the optimal AAM visual features are estimated via a maximum likelihood estimation (MLE) criterion, which are then used to construct face images for the animation. In our experiments, facial animations are synthesized for 20 continuous audio speech sentences, using the proposed AF_AVDBN model, as well as the state-of-art methods, being the audio visual state synchronous DBN model (SS_DBN) implementing a multi-stream Hidden Markov Model, and the state asynchronous DBN model (SA_DBN). Objective evaluations on the learned AAM features show that much more accurate visual features can be learned from the AF_AVDBN model. Subjective evaluations show that the synthesized facial animations using AF_AVDBN are better than those using the state based SA_DBN and SS_DBN models, in the overall naturalness and matching accuracy of the mouth movements to the speech content.     

硫代磷酸三(4-氨基苯酯)的合成及应用进展

介绍了硫代磷酸三(4-氨基苯酯)的国内外研究现状、各种合成方法以及它在聚氨酯、涂料、照相乳剂等方面的应用进展。     

高支模施工安全管理问题与对策

高支模工程安全管理不仅需要很高的技术,而且安全管理本身也具有较大的随机性,这就导致相关人员在开展安全管理工作时具有一定的难度。面对这一问题,相关监理人员必须从施工方案的审批、应急预案的落实、质量安全作业的施工技术交底和施工过程中所需要的各种原材料进场前的检验等方面加强管理。