Facile synthesis of nanocrystalline zinc ferrite via a self-propagating combustion method

Macroporous nanocrystalline zinc ferrite with single spinel-phase was prepared by a facile self-propagating combustion method using zinc nitrate, iron nitrate and glycine. The as-prepared ZnFe₂O₄ were characterized by X-ray diffraction (XRD) analysis, N₂ adsorption, scanning electron microscopy (SEM), high-resolution transmission electron microscopy (HRTEM), selected area electron diffraction (SAED) and energy dispersive X-ray spectrum (EDS). The magnetic properties of the prepared ZnFe₂O₄ were also studied.     

单壁碳纳米管的制备及生长特性研究

采用Fe/MgO作为催化剂 ,催化裂解CH4制备了较纯的单壁碳纳米管 ,用TEM和Raman对碳纳米管进行了表征 ,对不同生长温度下制备的碳纳米管Raman径向呼吸振动峰 (RBM)进行了分析 ,研究了生长温度对单壁碳纳米管生长特性和结构特性的影响     

中碱值硫化烷基水杨酸钙的制备及性能研究

介绍了一种碱值达170mgKOH／g以上、硫含量大于3．0％、钙含量大于6．0％的硫化烷基水杨酸钙盐润滑油添加剂的制备过程及其性能。实验中重点考察了促进剂及硫磺加入量对产品碱值及硫含量的影响；通过冷冻蚀刻电镜法观察了含碳酸盐的胶体粒子结构及粒度分布情况；应用凸轮挺校、四球试验机等考察了硫化烷基水杨酸钙盐产品的极压抗磨性能。结果表明，硫化烷基水杨酸钙产品不但具有良好的高温洁净性、抗氧化安定性、胶体稳定性，而且具有突出的极压抗磨性及热稳定性。     

多部件设备维修问题研究及遗传算法求解

合理组织设备维修，缩短设备维修时间是生产运营管理的一个重要环节。本文探讨了多部件设备维修的有效组织问题。考虑到维修工人对拆分后设备的不同部分具有不同的维修效率，提出了一种基于维修时间优化的决策方法，将其与经典指派方法进行了比较；进一步地，对这一NP-hard问题设计了遗传算法，通过数值例子讨论了其求解有效性。     

Convergence of simultaneous perturbation stochastic approximation for nondifferentiable optimization

We consider simultaneous perturbation stochastic approximation for function minimization. The standard assumption for convergence is that the function be three times differentiable, although weaker assumptions have been used for special cases. However, all work that we are aware of at least requires differentiability. We relax the differentiability requirement and prove convergence using convex analysis.     

自蔓延高温合成TiNi多孔体合金

为了开发新型的生体材料，本文对自蔓延高温合成TiNi多孔体合金——人造骨材料进行了研究。以单质钛粉和镍粉作原料，在氩气保护条件下，采用预热点燃模式和热爆模式制得了不同形态的多孔TiNi形状记忆合金。采用SEM和XRD分析了样品的孔洞特征和相组成，测试了其力学性能，并研究了合成条件参数与样品表面形貌和孔隙状态之间的关系。结果表明，用SHS法制备TiNi多孔体合金是可行的。     

Competitiveness of Inexperienced and Experienced Contractors in Bidding

This paper tests the assertion that experienced contractors are more competitive than inexperienced contractors by measuring the effect of experience on bidding competitiveness for building contracts procured by a regular client. Contractors are grouped into experienced and inexperienced contractors, and two levels of contractors’ experience are identified: (1) bidding experience only and (2) bidding plus construction experience. Results of two-sample t tests show that experienced contractors are more competitive than inexperienced contractors. Contractors’ competitiveness in respect of school contracts and other contracts are further compared in evaluating the relationship between the project type and experience effect. Experienced contractors are, on average, more competitive in competing for school contracts. It emerges that the factor of project type familiarity amplifies the experience effect. A comparison of experienced contractors’ competitiveness in bidding for (1) new building works and (2) alteration and extension works shows that the effect of experience would be more significant when contract works packages are highly standardized.     

钼酸铵溶液深度净化工艺探索

对传统的钼酸铵溶液净化工艺及文献介绍工艺进行了较为详细的分析 ,并与实验数据对比分析 ,找到了较为合理的工艺方案     

阻燃沥青的研究进展与建议

介绍了对沥青进行阻燃处理的必要性、沥青的阻燃机理、常用阻燃剂的特性及其作用模式;参照塑料材料阻燃性能的测试手段介绍了常用的沥青材料阻燃性能的测试方法;最后分析了我国沥青阻燃的研究现状,指出了该领域存在的主要问题,并给出了相应的建议。     

GIS中矢量图形的结构分析与VC++中的实现

简要讨论了GIS各类矢量图形元素间的空间拓朴结构及基位置关系 ,并用VC 6 . 0及MFC具体分析了圆弧与多边形区域的相交关系及实现。为利用VC开发专用图形软件提供了有用帮助。