溶胶-凝胶法制备PDMS/SiO2杂化材料

采用sol-gel工艺,以正硅酸乙酯(TEOS)为无机组分前驱物,以含端羟基的聚二甲基硅氧烷(PDMS)为有机组分,分别采用盐酸、草酸、氨水、三乙醇胺为催化剂,合成了PDMS/SiO2杂化材料,讨论了催化剂、共溶剂对杂化材料的影响,考察了杂化材料收缩率及透光率.结果表明:采用草酸作催化剂合成了块状、透明的杂化材料,PDMS/SiO2杂化材料的收缩率随共溶剂用量的增加和PDMS用量的减小而增加,采用羟基含量为4%的PDMS合成的杂化材料的透明性较好.     

氢氧化锌浆体抗菌材料-抗菌涂料一体化制备技术研究

采用氢氧化锌浆体抗菌材料-抗菌涂料一体化制备技术,能缩短工序,不排放废物,节约能耗,降低成本.氢氧化锌浆体加入量和粉磨时间对涂料的基本性能有影响,合适的加入量折算的锌含量为1%,粉磨时间为40min;氢氧化锌粉体和氧化锌粉体对涂料基本性能没有影响;锌型抗菌涂料有明显的抗菌效果,氢氧化锌浆体型涂料比氢氧化锌和氧化锌粉体型涂料抗菌性能更好.     

铁系氧化物纳米晶粉/环氧树脂杂化材料的制备

采用硬脂酸凝胶法制备铁系氧化物Ba2Co2Fe2sO46纳米晶粉,并通过表征和制备机理的探讨,确定600℃、2h后处理为制备Ba2Co2Fe28O46纳米晶粉合适的条件.以此为基础制备铁系氧化物纳米晶粉/环氧树脂杂化材料,并研究了团聚现象对吸波性能的影响.     

改性纳米金刚石增强增韧医用口腔复合树脂的研究

以爆轰法合成的纳米金刚石作为填料,加入到双酚A型口腔用光固化复合树脂中,研究了纳米金刚石对树脂性能的影响.金刚石用硅烷偶联剂进行表面改性.结果发现:偶联剂化学接枝到金刚石表面,改性后的金刚石在乙醇中的分散稳定性得到提高;加入0.2%(质量分数)的改性纳米金刚石后,复合树脂的挠曲强度和硬度分别提高35.4%和29.8%,改性金刚石的增强作用明显优于未经改性的金刚石;同时金刚石的加入也改善了树脂的韧性.     

面向多无人车的目标点分配和协同路径规划算法

针对多智能体路径搜索算法在非指定式多车协同路径规划问题中路径冗长,计算效率低等缺陷,提出协同目标点分配 路径规划算法 Nutcracker-CBS。 首先构建紧耦合目标点分配 MAPF 框架,实现目标点分配和路径构建的联合寻优;针对目标点 分配模块,提出改进的星鸦优化算法,增量式求解分配问题,缩短模块用时;针对路径构建模块,提出改进的 MAPF 算法,通过回 退式约束构建机制,引入避碰路径估计的绕道机制和数据共享底层路径规划机制,提升效率和路径质量。 数据集实验中, Nutcracker-CBS 时耗相比 SOTA 算法减少 90. 37% ;目标点分配模块求解耗时减少 86. 76% ;MAPF 模块 6 s 内构建 100 辆无人车 路径,平均路径长度缩短 6. 058% 。 实际实验中路径总和与系统运行时长分别减少 55. 26% 和 61. 29% ,提升了多机器人系统的 效率,降低了路径长度。     

确保FF现场总线仪表系统开车一次成功的重要措施

信息化、数字化、网络化,已与人们的日常生活息息相关,倍受青睐。在化工厂实现网络化管理、信息化管理是工业企业发展的趋势,基于基金会现场总线技术的自控仪表在石油化工装置以其独特的技术上的特点和其它诸多的优越性,在化工自动化控制领域占据了很重要的位置。为此,在新技术、新材料、新工艺的使用上,更要认真对待,在施工的各个环节中如何确保现场总线仪表系统的正常运行尤为关键。     

Analysis and optimization of high-power pulse transformer for SXFEL

Longitudinal injection is a promising on-axis injection scheme for diffraction-limited storage rings. In the latest version of the Hefei advanced light source(HALS), both the dynamic aperture and momentum aperture have been optimized. A longitudinal injection scheme was investigated on the HALS using a doublefrequency radio frequency system. To evaluate the injection performance, various errors were considered. A series of tracking simulations were conducted, and the injection efficiency was obtained under different error levels.     

铁矿烧结过程微细颗粒物排放行为

 采用ELPI+设备(荷电低压撞击器)对铁矿烧结过程微细颗粒物进行在线检测与采样,利用场发射扫描电子显微镜(FESEM EDS)对采集的颗粒物形貌特征进行分析,研究铁矿烧结过程中微细颗粒物的排放行为。研究结果表明,PM10大量释放集中在烧结升温段,且颗粒物质量浓度与数目浓度在粒径分布上有较大差异,其中质量浓度峰值区间为5.37～10.00 μm,数目浓度峰值区间为0.10～0.16 μm;形貌特征上,微细颗粒物呈规则的球形、方块形和片状;不同粒径物质组成差异明显,其中颗粒物中的K、Na主要以KCl和NaCl的形式存在,含量随颗粒物粒级的增大而略有降低。     

基于OSPF的ASON路由的一种加密方案

自动交换光网络(ASON)控制协议采用通用多协议标签交换(GMPLS)控制协议族,其路由部分主要为开放式最短路径优先(OSPF)协议.文章分析了OSPF协议加密措施存在的安全隐患,并对现有的加密方案进行了改进.针对OSPF协议的安全模式,提出了一种可以应用于ASON中路由技术的新的安全性方案.基于数论算法,实现S盒动态调整,通过动态产生的子密钥,在迭代过程中对分组进行加密.     

An experimental study on the choked flow characteristics of CO2 pipelines in various phases

High pressure pipeline transportation has been an established technology for economically transporting large amounts of CO_2. However, there are still issues and associated risks that have to be effectively addressed and adequately understood. It is well known that a strong Joule-Thomson Cooling effect can occur when pressurized CO_2 flows through a choke valve. Thus, to investigate the choking characteristics especially the temperature drop of high pressure CO_2, a new laboratory scale experimental setup(total length of 14.85 m and the inner diameter of 15 mm) was constructed. Steady choked flow and transient choked flow tests were carried out respectively for pressurized CO_2 in various initial phases. The phase transitions and temperature drop characteristics were then studied following the choked flow and the results show that the phase transitions in steady choked flow differs significantly from that in transient choked flow. For transient choked flow of various initial phases, all the flows downstream would transfer from single phase to gas–liquid two-phase flow. Furthermore, the effect of water on transient choked flow of supercritical CO_2 pipeline was investigated, and the phenomena of solid particles deposition was captured which was paramount importance of ensuring the safety operation of CO_2 pipelines when throttling by the choke valves.