纳米粒度测量方法浅析

本文介绍了多种纳米颗粒粒度的测量方法。主要讨论了X射线小角散射法、光子相关谱法和透射电镜-图像分析法的原理、适用范围及其优缺点。     

不同控制策略的小功率Boost-APFC性能研究

为了使用于小功率场合的功率因数校正电路的综合性能最优化,本文研究了采用电流断续模式或临界断续模式和电流连续模式的小功率Boost-APFC的各项性能。通过仿真分析和实验比较相结合的方法,定量给出了各电路在输入电流特性、效率、EMI滤波等性能上的具体差异,并且考虑了使用SiC二极管后对电路性能的影响。     

Flume Experiment on Stream Blockage by the Debris Flow From Tributary

Stream blockage by the debris flow from tributary valleys is a common phenomenon in mountainous area,which takes place when large quantities of sediment transported by debris flow reaches a river channel causing its complete or partial blockage.The dam formed by debris flow may causes upstream and downstream flooding,and presents great threat to people and property.Because of the catastrophic influence on people and property,debris-flow dam has attracted many attentions from the researchers and local administration.But,lit- tle attention has been given to the quantitative interrelationships of the potential influential factors.In this pa- per,the interrelationships of important influential factors caused the stream blockage by debris flow were ana- lyzed through flume experiment,and a model to predict the blockage was presented.     

Strain rate sensitivity of tensile properties in high Nb containing TiAl alloys

The effect of strain rate on the yield strength of high Nb containing TiAl alloy was studied. The results show that the strain rate sensitivity varies with the test temperature, and the yield strength is not sensitive to the strain rate at room temperature but significantly sensitive to the strain rate at high temperature. An increase of the strain rate or a decrease of the temperature results in an obvious change of fracture mode. It is found that the strain rate sensitivity of this alloy varying with temperature is due to the dislocation climb generated at high temperature.     

铝箔轧机排烟系统防火设计改进措施

铝箔轧机发生火灾时常引燃轧机排烟系统。本文简要介绍了铝箔轧机排烟系统，对排烟系统着火的原因进行了分析，在此基础上提出了排烟系统防火、灭火的改进措施。     

表征PAN纤维和炭纤维微细结构的HRTEM样品制备方法

为用高分辨透射电子显微术(HRTEM)表征聚丙烯腈(PAN)纤维和炭纤维的微细结构，从纤维性能出发，探讨研碎、离子束减薄和超薄生物切片三种制备方法及其工艺步骤，结合实验结果，对比了三种制备方法的原理、优缺点，提出了制备方法的适用范围和选择原则，并推断适于表征预氧化纤维微细结构的样品制备方法。与生物样品的制备方法类似，把超薄生物切片法引入到纤维材料HRTEM样品制备领域，为系统研究炭纤维微细结构的演变提供了线索。     

263电子邮件客户端软件的安全性分析

本文通过分析263电子邮件客户端软件的安全漏洞，揭示了该软件在用户信件安全方面的脆弱性。     

DWT－Based Watermarking Scheme for Digital Images

A watermarking scheme for digital images is introduced. This method is based on discrete wavelet transform and spread spectrum technique. A discrete wavelet transformed binary signature image is expanded by an m-sequence and added to the large wavelet coefficients of a host image with a scale factor. Good balance be-tween transparency and robustness is achieved by the selection of the scale factor. In addition, the spread spec-trum technique is adopted to increase the robustness of this watermarking scheme. The experimental results show that the proposed method is of good performance and robustness for common image operations such as JPEG lossy compression, etc.     

土壤样品的微波消解及其痕量铀的分析

对3个土壤样和2个放射性河床沉积物的国家标准物质进行了微波消解，又采用TOPO萃取和液体荧光法分析了样品中的铀含量，并将分析结果与国家标准方法GB11220．2-89的分析结果进行了比较。结果表明，微波消解法与国家标准方法一样，均不能实现土壤的全部消解，但与国家标准方法相比较，微波消解速度快，所需试剂量少，且易于实现定量控制，铀回收率高，分析精度高。对不溶物进行X射线能谱分析发现，其主要组成为铝、钛及过渡金属的氟化物或氧化物。同位素质谱分析表明，国家标准物质GBW08304中的^234U，^235U均比天然丰度低，另一个国家标准物质GBW08304a中铀的同位素分布与天然组成基本一致。     

用同步辐射X荧光分析血浆蛋白质的微量元素

用同步辐射X荧光(SRXRF)分析技术与凝胶色谱生化分离相结合，分析了用抗肿瘤药物顺铂处理过的和未处理过的小鼠血浆的大分子蛋白质。对以轻元素为基体的小量样品，用X荧光谱中的康普顿散射强度作为质量的因子，获得了在大于22ku分子量的蛋白质中Pt、S、Ca、Fe、Ni、Cu、Zn、Se、Br和Sr等元素含量在不同样品问的相对变化。由此推测，经顺铂处理后，Pt元素可与血浆中的大分子蛋白结合，含CM和S的大分子蛋白含量明显升高，而含Zn的减少。