Hydrothermal Synthesis of Acicular Lead Titanate Fine Powders

A pure, acicular lead titanate (PbTiO₃) fine powder with a white color has been prepared by hydrothermal synthesis. It is a new phase of PbTiO₃ with I 4 symmetry, cell parameters of a = 12.358 Å and b = 14.541 Å, and a density of 6.80 g.cm⁻³. The influences of pH (12.5 to 14.4), Pb/Ti ratio (1.0 to 1.6) in the feedstock, reaction temperature (130° to 230°C), time (0.25 to 4 h), starting materials, and additives on the formation of acicular PbTiO₃ under hydrothermal conditions have been investigated. The acicular PbTiO₃ with I 4 symmetry, referred to as the PX phase, can be converted to the perovskite-type (PE phase) of PbTiO₃ at about 605°C while its acicular morphology is essentially unchanged. The preferable conditions for preparing pure acicular PX-phase PbTiO₃ are that the pH is 13.0 to 14.0, Pb/Ti ratio is >1.3, reaction temperature is 170° to 200°C, time is 0.5 to 1.0 h, titanium butoxide (Ti[O(CH₂)₃CH₃]₄) is the starting material, and poly(vinyl alcohol) is an additive. The acicular grain of the PX phase is usually less than 100 nm in diameter and more than 1000 nm in length.     

火电机组运行优化系统的现状与展望

简单回顾了国内外在火电机组运行优化领域的研究历程，列举了目前国内外市场上针对火电机组的各种主流运行优化产品的功能特点和应用情况，分析了国外引进产品和国内自主研发产品在中国当前市场环境下各自的优势和劣势。介绍了当前运行优化系统在国内电站机组的应用现状，阐述了国内外运行优化系统在实际应用中存在的问题，并提出了相应的改进意见。对机组运行优化系统的未来发展进行了展望，指出机组运行优化系统将利用先进技术设备和信息平台，与电站管理紧密结合，在日益规范的市场中不断发展完善，为提高电站经济性发挥更大的作用。     

光隔离器及其相关的磁光材料

本文简要介绍了磁光隔离器的理论、结构和分类 ,并提出了该器件今后发展的几个问题 ,最后介绍了几种磁光材料     

微合金钢模拟焊接热影响区组织和韧性研究

采用焊接模拟试验方法，研究了不同峰值温度（Tmax）和不同冷却时间（t8/5），对合Ti-N、TI-NB-N两种微合金钢热影响（HAZ）显微组织、奥氏体晶粒度、冲击韧性影响。试验结果表明：Ti-N钢焊接热影响区比Ti-Nb-n钢具有更高的冲击韧性、更适用于大线能量的焊接条件。     

Hydrolysis of Milk Fat with Lipase in Reversed Micelles

Enzymatic hydrolysis of milk fat was studied in a reversed-micelle system consisting of lecithin, water (1% total volume) and butteroil. Candida cylindracea lipase entrapped in the water pools of reversed micelles hydrolyzed surrounding triglycerides. The optimum temperature for enzyme activity was 55°C with an activation energy of 15.4 kcal/mole, while maximum enzyme activity was observed between pH 4 to 6. The molar ratio of water to surfactant (R value) in the system influenced enzyme activity with maximum activity at R = 10. Enzyme activity also increased with increasing surfactant or enzyme concentration.     

宁夏引黄灌区渠道防渗衬砌技术研究

对宁夏引黄灌区渠道防渗衬砌的形式、防渗衬砌效果、渠道防渗衬砌工程的技术指标、冻害特征、防治措施进行了综合应用分析与研究,提出了不同级别渠道适宜的衬砌形式、推广渠道防渗衬砌的技术要求,供灌区节水工程改造、渠道衬砌工程参考。     

数字通信系统设计中FPGA的仿真

在大规模的FPGA设计中，由于逻辑过于复杂，给仿真与调试工作带来很大难度。本文结合“实用化综合接入系统”边缘路由器子系统的设计，结合仿真软件提供的接口，提出用测试程序自动生成测试向量，自动完成仿真结果检查的方法，大大降低了仿真与调试的工作量。     

MOISTURE TRANSFER PROPERTIES of WILD RICE

Working isotherms for processed wild rice and desorption isotherms for unprocessed wild rice were determined at temperatures ranging from 10 to 43.5°C. the constants for the Guggenheim-Anderson-DeBoer (GAB), Day and Nelson, Chen and Clayton and modified Halsey equations were determined by using a nonlinear optimization technique. the GAB equation showed extremely good fit to the experimental data (less than 5% error). the diffusion coefficients for moisture transport in both broken and whole processed wild rice and for unprocessed wild rice samples were determined at room temperature. the processed broken wild rice kernels had an effective diffusion coefficient of 2.66 × 10^?9 m²/h, whereas the effective diffusion coefficient was 7.08 × 10^?10m²/h for the processed whole wild rice kernels. Unprocessed wild rice had moderate effective diffusivity (1.4 × 10^?9 m²/h). These results predicted quite well the equilibrium water activities and time to equilibrium of wild rice-white rice mixtures using both analytical methods and the finite element method. the transfer of moisture to or from packaged wild rice was also illustrated for different distribution systems.     

迁安精矿粉高碱度烧结矿试验研究

对迁安地区磁选精矿粉添加磷石粉和Ｂ２Ｏ３，生产二元碱率为２．０左右的高碱度烧结矿，在实验室和现场进行了试验。结果表明：加入少量磷灰石粉或硼即可完全抑制烧结矿冷却过程中的自然粉化现象；ＭｇＯ含量对烧结矿质量影响明显；烧结矿的冶金性能良好。     

虚拟仪器技术在直升机主减速器平台检测中的应用

虚拟仪器技术是基于计算机技术和硬件系统的支持,应用数字化和软件技术进行检测,可以极大地提高测量的灵活性和可扩展性.基于虚拟仪器技术的直升机主减速器的检测可实时掌握装备的动态变化,了解装备的技术状况,具有便捷和低成本等优点.