数码辅助方法在毛细管流变仪测量粘度的应用

讨论了传统流变仪测量粘度上存在的问题，提出了改进的方案测量粘度，以减少误差。试验方案主要体现在用数码方法采集数据。     

Study on Sintered Synthetic Hercynite Clinker

Special grade bauxite and roll scale were used as raw materials to investigate the influences of reducing atmosphere and firing temperature on sintering clinker. The results showed that: 1) The mixture of the materials could be sintered enough to synthesise hercynite under reducing atmosphere by adding reducing reagent ; 2) The hercynite dinker could be sintered to high density and the content of FeAl2O4 may attain 80～90% under the firing tempera-ture of 1550℃.     

燕化660 kt/a乙烯冷区设备布置

主要介绍了大型乙烯改扩建的冷区设备布置的主要特点，分析了设备布置的思路，及与土建等各专业的关系，强调了设备布置方案利旧的方法。     

Measurement and Correlation for Solubility of (S)-(+)-2,2-Dimethyl-cyclopropane Carbox Amide in Different Solvents

1 INTRODUCTION (S)-(+)-2,2-dimethylcyclopropane carbox amide [(+)-DMCPCA, Fig.1] is a key intermediate of Cilas- tatin, an inhibitor of dehydropeptidase-I. As the syner- gist of imipenem (an antibiotic drug), cilastatin is widely used in clinical applications and has prosper- ous prospects[1]. In industrial manufacture[2―6], as the optical intermediate, the chemical and optical purity of (+)-DMCPCA would affect the quality of cilastatin. So, the separation and purification are impo…     

An Investigation of Error Sources in Computational Fluid Dynamics Modelling of a Co-current Spray Dryer

The paper is focused on identifying error sources in computational fluid dynamics(CFD) predictions of a spray drying process. Seven groups of drying and atomisation parameters were selected for analysis and 13 simulation trials were performed. The theoretical results were compared with experimental data and sensitivity of the simulation results to the analysed factors was determined. The following parameters affecting the accuracy of CFD spray modelling were found: gas turbulence model, particle dispersion, atomising air, initial parameters of atomisation and heat losses to the environment. A major difference in the errors committed during modelling of spray drying process for fine and coarse sprays was observed.     

新型液压胀合有缝不锈钢管衬里复合管的制造技术

针对目前液压生产复合管方法的不足，研制开发了一种新型不锈钢衬里复合管液压胀合装置。介绍了该装置的工作原理和结构特点及液压胀合复合管的制造技术。     

以设计为中心的虚拟制造技术及在化工过程装备中的应用

简述了虚拟制造技术的内涵、关键技术及应用现状。在分析化工过程装备特点基础上 ,对过程装备虚拟制造技术平台的体系结构进行了探讨 ,以典型过程装备螺旋片导流式气液分离器为例 ,对其数字化建模方法、数值仿真技术、虚拟设计和制造环境进行了研究。初步结果表明 :以设计为中心的虚拟制造技术的应用 ,可以有效地减少产品开发的时间和成本 ,提高产品质量     

The Desalting Property of Ion-Exchange Resins in Organic Solvent

The desalting property of ion-exchange resins in organic solvent is reported by using potassium acetate as a model compound. The experimental results show that the solvability of the solvent stirring speed, and temperature are the factors which influence the ion-exchange rate. The increase of solvability, stirring speed and temperature will speed up the ion-exchange process.     

Study on Jet Coflow Packing Tray

Experimental study on hydrodynamics and mass transfer efficiency of jet coflow packing tray (JCPT) was conducted in a φ285 mm column and a φ200 mm column, respectively. Compared with new vertical sieve tray which has been applied in the petrochemical industry since 1968, the JCPT has lower pressure drop, higher capacity and higher mass transfer efficiency, and seems promising in commercial application.