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81.
Yasushi Murakami Taki Matsumoto Kiyochika Yahikozawa Yoshio Takasu 《Catalysis Today》1995,23(4):383-389
The sol-gel process for the hydrolysis and polycondensation of tin tetra-n-butoxide in butanol was followed by viscosity measurements. The precipitation of tin-containing ultrafine particles was observed without any variation in the solution viscosity in the absence of diethylene glycols, while the viscosity increase was made without any precipitation by the addition of diethylene glycol. The induction period and the rate of the viscosity increase after the induction period was independent of the diethylene glycol content but depended upon the water content. The Monte Carlo simulation data were consistent with data for the viscosity experiment. The simulation was based on a kinetic model of the slow hydrolysis of tin tetra-n-butoxide, the reverse reaction of hydrolysis, and the polycondensation of the hydroxy derivatives. 相似文献
82.
T. Sato T. Murakami T. Endo M. Shimada K. Komeya T. Kameda M. Komatsu 《Journal of Materials Science》1991,26(7):1749-1754
Corrosion behaviour of Si3N4 ceramics containing Y2O3, Al2O3 and AIN as sintering aids was investigated under hydrothermal conditions at 200–300 C and saturated vapour pressures of water for 1–10 days. Hydrothermal corrosion resulted in the dissolution of the Si3N4 matrix and the formation of a product layer consisting of the original grain-boundary phases and hydrated silica. The dissolution rate of Si3N4 ceramics decreased with decreasing crystallinity of the grain-boundary phase. The dissolution rate could be adequately described by a parabolic plot in the initial stage of the reaction. The apparent activation energies were 83.5–108 kJ mol–1, and the bending strength of the corroded samples decreased from 600 to 400 MPa in the initial stage of the reaction upto a weight loss of 0.004 g cm–2, and then was almost constant up to a weight loss of 0.012 g cm–2. 相似文献
83.
Hiroki Matsuo Tatsuya Murakami Junichiro Otomo 《Journal of the American Ceramic Society》2021,104(11):5740-5749
In proton-conducting oxides, analyses for their electronic structure contribute to the understanding of interactions between defects in them. In this study, electronic band alignment of (1−x)BaZr0.8Y0.2O3−δ(BZY)–xSrZr0.95Y0.05O3−δ(SZY) proton-conducting solid-solution system (BSZY) which has high defect concentration and the deep valence band is experimentally investigated. By using thin-film specimens for optical absorption measurements, absorption edges derived from electron transition from the valence band to the conduction band which was insensitive to the proton incorporation were clearly observed in spite of the high defect concentration. The obtained optical band gap energy increased from 5.61 to 5.89 eV with increasing x, which was consistent with a composition dependence of Zr(Y)O6 octahedral tilting. Ultraviolet photon-yield spectroscopy (UV-PYS) measurements under vacuum condition revealed that BZY and SZY had ionization energy of 6.98 and 7.31 eV, respectively, and thus the absolute energy levels of the valence band maximum and the conduction band minimum of BSZY were experimentally clarified. We propose that the combination of the optical absorption measurements using thin-film specimens and the UV-PYS measurements under vacuum condition is effective in evaluating fundamental electronic structures of proton-conducting oxides. 相似文献
84.
Shinsuke Nagamine Yosuke Mizuno Yuta Hikima Kiyomi Okada Long Wang Masahiro Ohshima 《应用聚合物科学杂志》2021,138(7):49851
Cellulose microfibers (CMFs) having surfaces modified with polydopamine (PDPA) and octadecylamine (ODA) were prepared, and their reinforcing abilities for polypropylene (PP) were investigated. The PDPA coating was made via self-polymerization of dopamine (P-CMF), and subsequent alkylation was conducted by the reaction with ODA (OP-CMF). The modified CMFs exhibited improved dispersibility in the PP matrix due to the reduced hydrophilicity. The OP-CMF/PP composite prepared by batch mixing had a higher tensile modulus compared to that for the pure PP and composites with unmodified CMFs. However, excess alkylation lowered the tensile modulus, and the presence of an optimal degree of alkylation was demonstrated. The CMF/PP-IM composites fabricated by injection molding exhibited improved tensile properties compared to those prepared by batch mixing. Both the tensile modulus and yield stress were increased by increasing the CMF content and improved by the surface modification of the CMFs. 相似文献
85.
HiroyukiHoshino HiromitsuMurakami HideoYokota SatoshiSuda HidekiTsuge KoichiTerasaka ToshiakiWakabayashi 《材料热处理学报》2004,25(5):475-479
In quenching, the cooling uniformity is most important to diminish distortion occurring on work pieces. As a trial to accomplish uniform cooling, therefore, there exist various mixing methods of a quenchant and the quenchant circulation with an external pump has so far been the well accepted mixing method. However, this study proposes an advanced oscillation mixing method that can improve more the cooling uniformity in quenching. The proposed method includes a stirrer in oscillating motion, so that the simultaneous oscillating and mixing movements of the stirrer are considered to provide efecfively the uniform cooling characteristics for the quenchant. In comparison with the case of the circulation pump mixing, the investigation using the oscillation mixing method has demonstrated the following two experimental facts:(1) the short vapor blanket stage caused by the quick breakage of the oil vapor blanket and (2) the reduced variation of the quenching distortion. 相似文献
86.
87.
A. Ohmori Z. Zhou K. Inoue K. Murakami T. Sasaki 《Journal of Thermal Spray Technology》1996,5(2):134-138
The penetration phenomena of liquid manganese (Mn) alloy into porous ZrO2 (8 vvt % Y2O3) coating plasma sprayed on SS400 steel substrate was studied by heating in a vacuum atmosphere. The improvement in mechanical
properties of the coating by heat treatment with liquid Mn alloys was examined. Liquid Mn alloys, such as Mn-Cu, Mn-Sn, and
Mn-In, rapidly penetrated the coating and formed a chemical bond between the coating and the substrate. The densification
of the ZrO2 coating occurred when ZrO2 particles were sintered with liquid Mn alloys that penetrated the porous coating. The dense coating was free of porosity,
and its hardness increased after heat treatment with Mn alloys, compared with assprayed ZrO2 coating. Moreover, the fracture toughness of the coating reached the same levels as those of sintered yttria-stabilized PSZ. 相似文献
88.
Masahiro Hayashi Masahiko Jin Sutasn Thipprakmas Masao Murakawa Jung-Chung Hung Yu-Chung Tsai Ching-Hua Hung 《Journal of Materials Processing Technology》2003,140(1-3):30-35
In ultrasonic-vibration drawing, wires are drawn while ultrasonic vibration is applied to a drawing die. Prior studies provide experimental proof that ultrasonic-vibration drawing reduces drawing resistance, improves lubrication and prevents wire breakage. In the future, ultrasonic-vibration drawing is expected to contribute to the drawing of difficult-to-draw materials and operations, such as shaped wires, ultrafine wires, and the wire drawing operation in semidry or dry condition. However, a detailed analysis and understanding of the mechanism of improvement is not possible on the basis of conventional experimental observations because the ultrasonic-vibration processing phenomenon occurs at high speed. Therefore, we attempted to understand the processing mechanism of ultrasonic-vibration drawing using the finite element method (FEM). ABAQUS was used for the FEM. Drawing force and stress–strain distributions in drawn wires were analyzed. From these studies, we quantitatively clarified the mechanism of improved drawing characteristics, such as decreased drawing force. 相似文献
89.
Reo Matsumura Masahiro Shiomi Takahiro Miyashita Hiroshi Ishiguro Norihiro Hagita 《Advanced Robotics》2015,29(7):469-480
This study addresses a floor identification method for small humanoid robots that work in such daily environments as homes. The fundamental difficulty lays in a method to understand the physical properties of floors. To achieve floor identification with small humanoid robots, we used inertial sensors that can be easily installed on such robots, and dynamically selected a full-body motion that physically senses floors to achieve accurate floor identification. We collected a training data-set over 10 different kinds of common floors in home environments. We achieved 85.7% precision with our proposed method. We also demonstrate that our robot could appropriately change its locomotion behaviours depending on the floor identification results. 相似文献
90.
Hamid Noori Farhad Mehdipour Kazuaki Murakami Koji Inoue Morteza Saheb Zamani 《The Journal of supercomputing》2008,45(3):313-340
To improve the performance of embedded processors, an effective technique is collapsing critical computation subgraphs as
application-specific instruction set extensions and executing them on custom functional units. The problem with this approach
is the immense cost and the long times required to design a new processor for each application. As a solution to this issue,
we propose an adaptive extensible processor in which custom instructions (CIs) are generated and added after chip-fabrication.
To support this feature, custom functional units are replaced by a reconfigurable matrix of functional units (FUs). A systematic
quantitative approach is used for determining the appropriate structure of the reconfigurable functional unit (RFU). We also
introduce an integrated framework for generating mappable CIs on the RFU. Using this architecture, performance is improved
by up to 1.33, with an average improvement of 1.16, compared to a 4-issue in-order RISC processor. By partitioning the configuration
memory, detecting similar/subset CIs and merging small CIs, the size of the configuration memory is reduced by 40%. 相似文献