Preparation and photochromism of nanocomposite thin film based on polyoxometalate and polyethyleneglycol

A photochromic nanocomposite based on Keggin structure phosphomolybdic acid (PMoA) well dispersed in polyethyleneglycol (PEG) was fabricated. TEM image showed that PMoA nanoparticles with narrow size distribution were finely dispersed in polymer matrix. FT-IR results showed that the Keggin geometry of polyoxometalates was still preserved inside the composites and strong coulombic interaction was built between PMoA and polymer matrix. Under UV irradiation, the film was reduced photochemically to yield a blue species, which was in accordance with a charge-transfer mechanism.     

提高小样试织质量的措施

介绍了纺织品小样试织时，为了提高试织质量在经纬纱准备及织造工序时所采取的一些措施。     

爆震室内混合物填充特性研究

爆震室内混合物的填充过程是PDE工作循环中的重要一环.为了研究爆震室内的燃料和氧化剂的填充特性,采用大型计算流体力学仿真软件对爆震室内燃料和空气的填充过程进行了数值模拟.计算结果表明,在设定的计算条件下,填充距离随填充时间的增加近似线形增大,填充完毕所需的填充时间约0.125s,且从距封闭端250mm开始,填充后的乙炔质量分数稳定在0.11.     

3Cr-3Mo二次硬化钢的回火组织和力学性能

研究了3cr—3Mo二次硬化钢淬火回火后的组织和力学性能。结果表明：随回火温度的升高，试验钢中先后析出M3c、M2c和M7C3等碳化物，在575℃回火时硬度达到峰值；400一575℃回火后试验钢的抗拉强度约为l600MPa，冲击韧性为30J／cm^2；回火温度高于600℃时，强度和硬度迅速下降，冲击韧性增加；640℃回火时，以M2C型碳化物为主，抗拉强度为1100MPa，冲击韧性增加至55J／cm^2。     

珠海市地下管线管理工作的具体措施

在建设部令第136号《城市地下管线工程档案管理办法》颁布前后,珠海馆从思想着手,从立法、宣传、教育、调研协调、具体措施等方面,将工作落到实处,为珠海市科学管理城市地下管线奠定了基础。     

Controlled Synthesis of Ag2S,Ag2Se,and Ag Nanofibers by Using a General Sacrificial Template and Their Application in Electronic Device Fabrication

Nanofiber bundles of Ag₂S, Ag₂Se, and Ag have been successfully synthesized by making use of Ag₂C₂O₄ template nanofiber bundles, utilizing both anion‐exchange and redox reactions. The obtained bundles were polycrystalline nanofibers composed of nanoparticles in which the precursor morphology was well‐preserved, indicating that Ag₂C₂O₄ nanofiber bundles acted as a general sacrificial template for the synthesis of silver‐based semiconductor and metal nanofibers. Dispersing media and transforming reactants were found to be key factors influencing the chemical transformation in the system. In particular, separate single‐crystalline Ag nanofibers were obtained via a nontemplate route when ascorbic acid was used as a relatively weak reductant. An electrical transfer and switching device was built with the obtained Ag₂S and Ag nanofiber bundles, utilizing the unique ion‐conductor nature of Ag₂S and revealing their potential applications in electronics.     

负载型固体碱催化合成亚苄基丙酮

研究了用固体碱 KOH/Al_2O_3催化合成苯叉丙酮,确定了合成的最佳工艺条件:n(苯甲醛)∶n(丙酮)=1∶4.催化剂用量2g,催化剂最佳负载量12mmol/g,反应温度40～45℃,反应时间为3h,产率达88%以上。     

苏北-南黄海盆地构造演化

苏北及南黄海盆地是由多期、多类盆地叠加的复合残留盆地,地质概况基本相似,成因演化近同,自元古界下扬子板块形成后,主要经历了古-中生代地台、中生代前陆盆地、走滑拉分盆地时期以及新生代断陷、坳陷盆地时期.在古生代-中生代发展过程中是一个整体,晚白垩世盆地演化出现分化,发育伸展盆地群,形成一系列叠置在中、古生代盆地之上的箕状断陷,箕状断陷的发育及分布明显受中-古生界内部先存逆冲断裂的控制.     

新的启迪

说点心里的话，建筑设计对青年人来讲是一条漫长的道路。建筑是一个载体，有精神一面，也有物质一面。有些建筑师拿着模型或未建成的设计来炒作，为了求名，生怕别人不知道。这对个人是小事，但若贻误了青年学子，那就是不可取的。     

Structured optimal and robust control with multiple criteria: a convex solution

In this paper, the design of controllers that incorporate structural and multiobjective performance requirements is considered. The control structures under study cover nested, chained, hierarchical, delayed interaction and communications, and symmetric systems. Such structures are strongly related to several modern-day and future applications including integrated flight propulsion systems, platoons of vehicles, micro-electro-mechanical systems, networked control, control of networks, production lines and chemical processes. It is shown that the system classes presented have the common feature that all stabilizing controllers can be characterized by convex constraints on the Youla-Kucera parameter. Using this feature, a solution to a general optimal performance problem that incorporates time domain and frequency domain constraints is obtained. A synthesis procedure is provided which at every step yields a feasible controller together with a measure of its performance with respect to the optimal. Convergence to the optimal performance is established. An example of a multinode network congestion control problem is provided that illustrates the effectiveness of the developed methodology.