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871.
By means of 29Si and 27Al magic angle spinning nuclear magnetic resonance (MAS NMR) combined with deconvolution technique, X-ray diffraction (XRD), scanning electron microscopy (SEM) as well as energy dispersive X-ray system(EDX), the effect of 5 wt% corrosive solutions (viz. 5 wt% Na2SO4, MgSO4, Na2SO4+NaCl and Na2SO4+NaCl+Na2CO3) on C-S-H microstructure in Portland cement containing 30 wt% fly ash was investigated.The results show that, in MgSO4 solution, Mg2+ promotes the decalcification of C-S-H by SO 4 2- ,increasing silicate tetrahedra polymerization and mean chain length (MCL) of C-S-H. However, the substituting degree of Al3+ for Si4+ (Al[4]/Si) in the paste does not change evidently. Effect of Na2SO4 solution on C-S-H is not significantly influenced by NaCl solution, while the MCL and Al[4]/Si of C-S-H in fly ashcement paste slightly change. However, the decalcification of C-S-H by SO 4 2- and CO 3 2- attack, as well as the activation of fly ash by SO 4 2- attack will increase the MCL and Al[4]/Si, which are both higher than that under Na2SO4 corrosion, MgSO4 or Na2SO4 +NaCl coordination corrosion. 相似文献
872.
Corrosion of Mg–Y alloy was studied using electrochemical evaluations, immersion tests and SEM observations. Corrosion mechanisms of Mg-(0.25 and 2.5) Y alloy and Mg-(5, 8, and 15) Y alloy were uniform corrosion and pitting corrosion respectively, and the content of Mg_(24)Y_5 phases determined its effect acting as cathode to accelerate the corrosion or corrosion barrier to inhibit the corrosion. Corrosion resistance of Mg-(0.25, 2.5, 5, 8, and 15) Y alloys was as follows: Rt(Mg-0.25Y) Rt(Mg-8Y) Rt(Mg-15Y) Rt(Mg-5Y) Rt(Mg-2.5Y). Y could significantly improve the corrosion resistance of the Mg-Y alloy, but the excess of Y deteriorated the corrosion resistance of the Mg-Y alloy. The optimum content of Y in the studied alloys was 2.5%. 相似文献
873.
The effects of ultrasonic vibration temperature on the microstructure of semisolid Sn-52 Bi alloy and mechanical properties were investigated. The results show that the microstructure and mechanical properties are improved obviously after the ultrasonic treatment. Nearly round and uniformly distributed primary Sn phase particles were obtained under the cavitation and acoustic streaming caused by ultrasonic treatment. The best effects of ultrasonic treatment on microstructure and mechanical properties were obtained with the ultrasonic vibration for 120 s at 140 ℃. The elongation of semisolid Sn-52 Bi alloy treated by ultrasonic vibration for 120 s at 140 ℃ was 42% and increased by 156.09% compared to conventional liquid casting Sn-52 Bi alloy without ultrasonic vibration. It is a feasible and effective method to adopt the semisolid metal forming technology assisted with ultrasonic vibration to improve the ductility of Sn-Bi alloys. 相似文献
874.
The effects of winglet offset distance, winglet coverage, and winglet cross section on the over-tip leakage loss for the plane tip have been investigated experimentally in a turbine blade cascade for a tip gap height-to-span ratio of h/s = 1.36 %. The results show that the over-tip leakage loss for the full coverage winglet increases steeply with increasing the winglet offset distance. This loss generation is attributed to flow disturbances over the forward-facing and backward-facing steps within the tip gap. The winglet flush mounted to the tip surface provides the best result. With the leading edge winglet portion or without it, the both-side winglet always provides better aerodynamic performance than the corresponding pressure-side winglet or suction-side winglet. Longer coverage of the both-side winglet leads to lower loss. Therefore, the full coverage winglet performs best in the loss reduction for the plane tip. In general, thinner winglet leads to better aerodynamic result, and the winglet cross section having a slant bottom surface with the smallest thickness at its outer end is recommended. 相似文献
875.
Songlv Qin Mingjun Cui Zhendong Dai Shihui Qiu Haichao Zhao Liping Wang Afang Zhang 《Tribology Letters》2018,66(2):69
A facile method is proposed to prepare poly-o-phenylenediamine (PoPD) noncovalent functionalized graphene (G)-reinforced polyimide (PI) nanocomposites. PoPD-G exhibited excellent dispersibility in various organic solvents. The structures of PoPD-G were characterized by Raman and UV spectrum, which verified the π–π interactions between PoPD and G. The effective exfoliation of graphene nanosheets was investigated by observation of the morphology of PoPD-G with SEM, SPM, and TEM. Compared to PI/G composites, the interfacial adhesion between graphene nanosheets and PI matrices promoted efficient stress transfer from PI chains to PoPD-G nanofillers. Polyimide nanocomposites with different incorporations of PoPD-G exhibited outstanding thermal properties. It is interesting to note that only 0.5 wt% PoPD-G-reinforced PI composites increased by 20.8% in hardness, enhanced by 84.0% in storage modulus, and reduced by 72.8% in wear rate compared with neat PI. The eminent enhancement was attributed to the facile dispersion of graphene nanosheets and strong interface adhesion between PI and PoPD-G. 相似文献
876.
HongWei Fang DongChen Dai SongHeng Li GuoJian He Lei Huang WenQi Peng 《中国科学:技术科学(英文版)》2016,59(12):1856-1866
Identifying the underlying mechanisms that influence the spatial patterns in populations improves the forecasts of the alternative management strategies on the spatial dynamics of the populations, which are critical for assessing and managing the fisheries and improving the water resource management. This paper described a new approach of the numerical model for the prediction of the aquatic animal distribution in the flows. The model was developed based on the kinetic theory of gases, the mechanism of the aquatic animal movement and the flow hydrodynamic patterns. The model was validated using the available experimental data and an acceptable agreement was obtained. A comprehensive parameter study was then conducted to help understand the impact and the sensitivity of each parameter to the aquatic animal distribution. The promising results of the model reveal the prospect of applying this model to the reliable prediction of the aquatic animal distribution within a relatively large water area. 相似文献
877.
To balance the convergence rate and steady-state error of blind source separation (BSS) algorithms, an efficient equivariant adaptive separation via independence (Efficient EASI) algorithm is proposed based on separating indicator, which was derived from the convergence condition of EASI, and can be used to evaluate the separation degree of separated signals. Furthermore, a nonlinear monotone increasing function between suitable step sizes and separating indicator is constructed to adaptively adjust step sizes, and forgetting factor is employed to weaken effects of data at the initial stage. Numerical case studies and experimental studies on a test bed with shell structures are provided to validate the efficiency improvement of the proposed method. This study can benefit for vibration & acoustic monitoring and control, and machinery condition monitoring and fault diagnosis. 相似文献
878.
The dynamic observations of bainitic transformation in a Fe-C-Mn-Si superbainite steel were conducted on a high temperature laser scanning confocal microscope. It is indicated that the mutual intersection of bainite sheaves often occurs during growth of bainite ferrite, resulting in an interlocked bainite microstructure. Moreover, bainite transformation is promoted by higher austenization temperature and the longer and finer bainite platelets are obtained. Further, The average growth rate of bainite after austenization at 1 100 ° is calculated as 5.8 µm·s?1. In situ observation investigation makes it possible to identify bainite transformation in real time during isothermal holding. 相似文献
879.
New visible transparent, UV absorption, and high infrared reflection properties have been realized by depositing multilayer SiO2/ZnO: Al/CeO2-TiO2/SiO2 films onto glass substrates at low temperature by radio frequency magnetron sputtering. Optimum thickness of SiO2, ZnO: Al (ZAO) and CeO2-TiO2 (CTO) films were designed with the aid of thin film design software. The degree of antireflection can be controlled by adjusting the thickness and refractive index. The outer SiO2 film can diminish the interference coloring and increase the transparency; the inner SiO2 film improves the adhesion of the coating on the glass substrate and prevents Ca2+, Na+ in the glass substrate from entering the ZAO film. The average transmittance in the visible light range increases by nearly 18%-20%, as compared to double layer ZAO/CTO films. And the films display high infrared reflection rate of above 75% in the wavelength range of 10-25 μm and good UV absorption (> 98%) properties. These systems are easy to produce on a large scale at low cost and exhibit high mechanical and chemical durability. The triple functional films with high UV absorption, antireflective and high infrared reflection rate will adapt to application in flat panel display and architectural coating glass, automotive glass, with diminishing light pollution as well as decreasing eye fatigue and increasing comfort. 相似文献
880.
王发洲 《武汉理工大学学报(材料科学英文版)》2015,30(2):331-337
Microstructural features including pore size distribution, cell walls and phase compositions of magnesium oxychloride cement foams (MOCF) with various MgO powders and water mixture ratios were studied. Their influences on compressive strength, water absorption and resistance of MOCF were also discussed in detail. The experimental results indicated that moderate and slight excess MgO powders (MgO/MgCl2 molar ratios from 5.1 to 7) were beneficial to the formation of excellent microstructure of MOCF, but increasing water contents (H2O/MgO mass ratios from 0.9 to 1.29) might result in opposite conclusions. The microstructure of MOCF produced with moderate and slight excess MgO powders could enhance the compressive strength, while serious excess MgO powders addition (MgO/MgCl2 molar ratios = 9) would destroy the cell wall structures, and therefore decrease the strength of the system. Although MOCF produced with excess MgO powders could decrease the water absorption, its softening coefficient was lower than that of the material produced with moderate MgO powders. This might be due to the instability of phase 5, the volume expansion and cracking of cell walls as immersed the sample into water. 相似文献