基于DSP／BIOS的数字滤波器设计与实现

用可编程DSP芯片实现数字滤波可以通过修改滤波器的参数十分方便的改变滤波器的特性。本文以TMS320F2812数字信号处理器为核心,用DSP／BIOS来实现滤波器的算法任务,介绍了基于DSWBIOS的滤波器开发过程,在DSK2812平台上实现了数字滤波器的功能,同时本文方法可推广用于需要进行数字信号处理的多任务软件开发。     

基础素描课程“启发性教学”的研究

针对素描教学中存在的实际问题,通过素描色调训练、构成组合训练、绘画材料表现等3方面研究教学中的启发性素描的教学训练模式,使学生具备较好的绘画表现能力,提高学生的艺术感受能力．     

混合H2／H∞控制问题的降阶控制器

考虑混合H2／H∞控制问题的降阶控制器的设计问题．基于线性矩阵不等式（LMI）,分别‘给出了连续和离散情形下混合H2／H∞问题的降阶控制器的设计．     

基于FPGA的光栅尺位置速度反馈模块设计

利用FPGA的高速运算能力,建立一个数据采集处理模块,该模块的任务是采集光栅尺输入信号,对采集到的信号进行分析处理,得出速度、位移、方向等物理量.并对该模块进行了仿真,结果表明模块可以很好地完成预定任务.     

2-巯基-5-甲氧基咪唑并[4,5-b]吡啶的合成

以2,6-二氯吡啶为原料,经过硝化、氨解、甲氧基取代、还原和环化5步反应制得泰妥拉唑重要中间体2-巯基-5-甲氧基咪唑并[4,5-b]吡啶,总收率达40.2%.通过红外光谱、核磁共振氢谱对部分中间体及最终产品的结构进行表征,证明结果正确.     

Tests and numerical simulation on curved blade of super-critical adjust stage

Tests and numerical simulations of super-critical adjust stage blade were carried out and the effect of bowed blade on flow characteristics and the secondary flow were analyzed. The simulation and test results show that the adjust stage blade with aft-loading and big front-edge radius has good flow characteristics by meridian shrink. The numerical studies were carried out with software of NUMECA in order to investigate the aerodynamic characteristics of adjust stage blades,which include prototype blade(tested blade) ,positive curved blade (15°) and negative curved blade(-15°) . The simulation results show that the positive curved blade forms a negative static pressure gradient in the lower region of the cascade along the blade height and a positive static pressure gradient in the upper region. This leads to the reduction of the streamwise vortices intensity and the aerodynamic load on both sides of the blade and the endwall. Therefore,the crosswise secondary flow losses of endwall can be decreased considerably.     

含砷废水砷铁分离的研究

以氢氧化钠作为沉淀剂,对含砷废水进行选择性沉淀研究,考察了pH值、搅拌速度、温度等因素对砷、铁分离效果的影响,确定了合适的工艺条件：温度25℃,pH=13.5,搅拌速度500 r/min.此工艺条件下铁的回收率达到99.9%以上,实现了砷、铁的有效分离.     

Sensor placement for structural damage detection with modal data

A new method is presented for prioritizing sensor locations for structural health monitoring (SHM). In view of the needs of SHM and damage detection,sensor locations are optimized for the purpose of both sensitivity for local damages and independence of the target mode. However,the two different optimization criterions lead to an inconsistency of the optimal result. Considering the structural response changes that result from damage,the relationship between the structural response and damage is deduced from the structural motion equation by a quasi-analytical mode. Based on the harmony between damage identifiability and mode observability,an object function is set up,including the information of mode independence and damage sensitivity. Utilizing the technique of singular value decomposition,an interior algorithm for the optimum sensor placement is proposed with the multiple objective criterions of minimizing the condition number of coefficient matrix and maximizing the fisher information matrix. A numerical example shows that this approach can effectively avoid the contradiction between the two different optimization criterions. Comparing with the result of single object,the result of damage detection from the optical sensor locations is much more accurate.     

反相液相色谱法测定(反)-4-环已基-L-脯氨酸和(反)-4-苯基-L-脯氨酸

采用反相高效液相色谱法分离和测定(反)-4-环已基-L-脯氨酸和(反)-4-苯基-L-脯氨酸.在选定的色谱条件下,(反)-4-环已基-L-脯氨酸、(反)-4-苯基-L-脯氨酸和杂质之间具有较好的分离效果.该方法具有操作简单、快速、准确度和精密度较好,对同一(反)-4-环已基-L-脯氨酸试样多次测定,(反)-4-环已基-L-脯氨酸的日内、日间相对标准偏差(RSD)分别1.55%和0.09%;(反)-4-苯基-L-脯氨酸的日内、日间相对标准偏差(RSD)分别1.94%和1.79%.(反)-4-环已基-L-脯氨酸和(反)-4-苯基-L-脯氨酸的回收率分别为99.80%~100.40%和97.28%~100.00%.     

AZ91D镁合金表面复合涂层的微观形貌与性能

为了提高AZ91D镁合金的耐腐蚀性和耐磨性,用硅酸盐体系溶液和以乙酸镍为主盐的镀液在AZ91D镁合金表面制备了等离子体电解氧化和化学镀镍复合涂层.SEM分析结果表明,复合涂层表面呈典型的胞状结构,复合涂层中的镀镍层自氧化膜的紧密层和疏松层的交界处向外生长,镀镍层和氧化膜之间呈"机械咬合"式结合.XRD分析结果表明,复合涂层外层和内层的相组成主要为非晶态Ni-P合金和Mg2SiO4、MgAl2O4等.与AZ91D镁合金相比,复合涂层的显微硬度为基体的6倍;自腐蚀电位提高了约1.2 V,自腐蚀电流密度降低了2个数量级.制备复合涂层之后,AZ91D镁合金的性能得到显著的改善.