工艺参数对直流磁控溅射法制备氧化铝薄膜的试验研究北大核心

采用直流磁控溅射法在载玻片和不锈钢基底上制备某设计要求的氧化铝薄膜,首先采用单因素法分别分析溅射功率、氧气流量、工作压强、负偏压及本底真空度等制备参数对薄膜沉积速率的影响;在此基础上设计正交试验,研究优化范围内溅射功率、氧气流量、工作压强对沉积速率的影响,并进行极差与方差分析。结果表明,在一定工艺参数范围内,随着溅射功率的增加,薄膜的沉积速率不断增大;氧气流量增加时薄膜的沉积速率不断下降;随着工作压强的增大,薄膜的沉积速率先增大后减小,在1.0 Pa时达到最大速率;加载的负偏压增加时,薄膜的沉积速率不断降低;本底真空度提高时薄膜的沉积速率不断增大;通过使用XRD衍射仪对制备的薄膜进行物相检测,研究结果表明,常温下不同氧气流量制备的氧化铝薄膜均为非晶态;获取了制备所需薄膜的较优的制备工艺。     

Corrosion mechanism and corrosion model of Mg-Y alloy in NaCl solution

Corrosion of Mg–Y alloy was studied using electrochemical evaluations, immersion tests and SEM observations. Corrosion mechanisms of Mg-(0.25 and 2.5) Y alloy and Mg-(5, 8, and 15) Y alloy were uniform corrosion and pitting corrosion respectively, and the content of Mg_(24)Y_5 phases determined its effect acting as cathode to accelerate the corrosion or corrosion barrier to inhibit the corrosion. Corrosion resistance of Mg-(0.25, 2.5, 5, 8, and 15) Y alloys was as follows: Rt(Mg-0.25Y) Rt(Mg-8Y) Rt(Mg-15Y) Rt(Mg-5Y) Rt(Mg-2.5Y). Y could significantly improve the corrosion resistance of the Mg-Y alloy, but the excess of Y deteriorated the corrosion resistance of the Mg-Y alloy. The optimum content of Y in the studied alloys was 2.5%.     

饶阳凹陷武强地区沙二、沙三段储层成岩作用分析

为明确饶阳凹陷武强地区沙二、沙三段有效储层的成因和分布规律,通过岩心观察、镜下薄片鉴定分析储层的岩石学特征、储集空间类型和成岩作用类型;结合物性测试和镜质体反射率测试等资料,研究该区储层的成岩阶段和成岩演化过程及其对物性的影响.结果表明:长石砂岩和岩屑长石砂岩是研究区主要的砂岩类型,结构和成分成熟度为中等;储集空间主要为次生溶蚀孔隙,此外发育少量原生孔隙和裂缝;储层埋藏深度大,整体以中—低孔、中—低渗储层为主;储层成岩阶段主要处于早成岩B期—中成岩A期,受烃源岩成熟过程的影响,垂向上次生孔隙主要发育深度为2 400~2 800m.该研究对武强地区的油气勘探和开发具有指导意义.     

Superplastic behavior of Al-Cu-Li based alloy

The superplastic behavior was studied in an Al-4Cu-ILi-0.4Mg-0.4Ag-0.1Zr alloy. The alloys were manufactured both by＂ a conventional rolling route and a thermo-mechanical treatment route. The superplastic properties were evaluated as a function of temperature, strain rate, and processing history. Prior to thermo-mechanical processing, the alloys have elevated-temperature ductilities of 94% to 130%, strain rate sensitivities of about 0.25, and activation energies corresponding to lattice diffusion. After thermo-mechanical processing, the alloys have ductilities of 200% to 630%, strain rate sensitivity of about 0.42, and activation energies corresponding to grain boundary diffusion or a mixture of grain boundary diffusion and lattice diffusion. Skipping rapid recrystallization annealing can supply a higher value of elongation-to-failure.     

Effect of Zr content on quench sensitivity of AlZnMgCu alloys

The effect of Zr content on quench sensitivity of AlZnMgCu alloys was investigated by mechanical properties testing and microstructure observations. The results show that with the increase of Zr the quench sensitivity relative to hardness and strength increases, while that relative to elongation decreases. From hardness and strength viewpoints, the low quench sensitivity is observed for the Zr-free and 0.05% Zr-containing alloys, which is quite quench sensitive from the ductility viewpoint. The largest quench sensitivity relative to hardness and strength is observed for 0.1% Zr-containing alloy, this is mainly due to large amount of high angle grain boundaries and incoherent Al3Zr dispersoids caused by recrystallization, which may efficiently promote heterogeneous precipitation during air quenching. More than 0.05% Zr can significantly decrease the quench sensitivity relative to ductility, which can be primarily attributed to recrystallization inhibiting and grain refining effects of Zr.     

Synthesis and thermal decomposition kinetics of LiNiO2

A layered LiNiO2 with high crystallinity was synthesized by sintering the finely prepared mixture of lithium hydroxide and nickel hydroxide in the oxygen atmosphere. The electro-chemical properties of LiNiO2 show that it has a reversible capacity of more than 168mA*h*g-1. It was found that with increasing temperature, LiNiO2 decomposed in air followed with three reaction stages, the apparent activation energies were 747.18±1.0kJ*mol-1, 932.46±1.0kJ*mol-1 and 1126.97±1.0kJ*mol-1 respectively, and the kinetic equations of the three reaction stages were obtained.     

电测法在离合制动器动作时间调整中的应用

电测法在离合制动器动作时间调整中的应用１６１００５齐齐哈尔第二机床厂张新，蔡子牛摩擦离合器制动器脱开结合过程的正确性是影响其使用寿命和生产效率的关键。离合器制动器的正确工作状态应该是：离合器的结合滞后制动器脱开，制动器的结合滞后离合器脱开。滞后时间，...     

浅谈博州气象局网络实时监控系统的设计

随着网络技术的迅猛发展,对网络运行状态的实时监控显得十分重要。通过综合分析我局整个网络拓扑结构,开发了基于delphi语言环境的实时网络监控系统,介绍了该系统的实现必要性、功能、设计原理和实现流程。投入业务应用的实践表明,该系统实用性强,对网络系统实时监控效果很好,大大提高了网络的有效性和可靠性。     

“数字海洋”原型系统设计与实现初步

基于现有数字海洋的概念及其相关研究,结合对我国数字海洋建设战略部署的分析,设计了中国数字海洋原型系统框架;另外,根据用户类型和应用需求的不同,设计了数字海洋原型系统公众版和管理版的功能模块;并从数据处理流程和信息服务需求角度分析了数字海洋原型系统数据处理及信息服务模式;最后给出了原型系统实现的初步进展。     

行波型超声电机基于神经网络的逆模型辨识

行波型超声电机的动态特性受定子压电陶瓷迟滞和接触层非线性摩擦力的影响,表现出复杂的多值映射特征.通过引入动态迟滞逆算子,将存在于超声波电机逆系统中的多值映射在新的扩张输入空间上,转换为一一映射;然后使用神经网络建立超声波电机的逆模型,对迟滞和非线性摩擦力的影响进行补偿.所建立的模型结构简单,可以在线调整适应电机参数的非线性变化.实验仿真结果验证了该方法的有效性.