生物形态多孔氮化钛陶瓷的碳热氮化法制备

研究了以生物模板(木炭)浸渍TiO2溶胶,高温碳热-氮化制备TiN陶瓷的工艺过程.应用热力学原理计算了经溶胶浸渍后形成的TiO2/C复合体系的氮化条件,确定了N2,CO分压对氮化温度的影响.采用碳热氮化法,在高浓度的氮气压力下反应烧结制备了具有生物形貌的多孔TiN/C陶瓷.结果表明在1400℃,4 h,0.5 MPa氮气压力下,得到了具有立方晶体结构的TiN/C多孔陶瓷,并保留了木材模板的显微结构.     

NOTE ON MAGNETIC PROPERTIES OF GRAIN ORIENTED 4％Si-Fe

<正> 现将近年来在4％Si-Fe合金冷轧成带的加工塑性和二次再结晶方面的研究中所取得的主要结果介绍如下: (1) 4％Si-Fe合金的物理性能 3—4％Si-Fe的饱和磁感(B_■),电阻率(ρ),比重(D),膨胀系数()和导热系数(λ)的实测结果示于表1。     

Vision-based detection of MAG weld pool

Weld pool contains significant information about the welding process. The weld pool images of MAG welding are detected by LaserStrobe system. An algorithm for extracting weld pool edge is proposed according to the characteristics of MAG weld pool images. The maximum weld pool length and width are calculated. The measurement data can be used to verify the results of welding process simulation and to provide a good foundation for automatic control of MAG welding process.     

车铣加工硬铝合金微细轴技术

车铣加工能实现以铣代车加工回转体零件的外圆表面。它从切削原理上解决了微细轴类零件车削加工时切削速度低的问题。通过车铣加工微细轴试验,从切削速度和加工质量两个主要方面分析了车铣技术在解决微细轴加工中的特点。结果表明,车铣加工技术在实现微细轴的高速切削和保证零件加工质量方面都具有独特优势,是一种非常适合于微细轴类零件加工的技术。     

全焊接阀门的焊接温度场拟合分析

建立了一种基于试验的非线性曲线拟合的新方法来分析焊接温度场。采用改进的温度场数学解析模型后，拟合得到与实测结果相当接近的温度-时间拟合曲线方程：根据不同条件下的拟合方程，对其回归系数进行了影响因素的分析。并考虑实际需要，得到了不同初始温度下全焊接阀体的密封圈安全位置范围，为阀门焊接工艺的制定提供了重要依据。     

基于机器视觉的气门杆几何参数测量方法研究

文章给出了机器视觉系统的基本组成及高精度视觉测量的实施对策,并以气门杆几何及形位参数检测为例,讨论了图像的采集、处理及达到亚像素边缘检测精度的软件设计,通过LOG算子、最小二乘线性估计等手段,使直线边缘定位精度达到亚像素级,在不增加硬件成本的前提下,达到了检测参数的精度设计要求.     

Effects of Ag addition on mechanical properties and microstructures of Al-SCu-0.5Mg alloy

The mechanical properties and microstructures of Al-8Cu-0.5Mg alloy with and without Ag addition were studied at both room- and elevated-temperatures. The results show that the alloy with Ag is strengthened by a homogeneous distribution of coexistent θ＇ and Ω precipitates on the matrix （001） and （111） planes, respectively, whereas the alloy without Ag by θ＇ precipitates only. The small size and high volume fraction of θ＇ and Ω precipitates in the Ag-containing alloy improve the tensile strength and yield strength, especially those at the elevated temperatures. However, it is also responsible for the decrease in elongation, compared with the alloy without Ag, which is due to the microcracks initiated from the inherent incompatibility between the particles and the AI matrix during deformation.     

聚苯胺-蒙脱土纳米复合材料的耐腐蚀性能

在聚合温度为25℃，蒙脱土质量含量为苯胺的0．5％，过硫酸铵和苯胺的摩尔比为1：1，掺杂剂磺基水杨酸摩尔浓度为0．03mol／L的实验条件下，运用插层聚合的方法制备出PAT—MMT复合纳米材料。电化学阻抗谱(EIS)表明：在NaCl质量含量为3．5％的腐蚀环境中，该复合纳米材料作为冷轧钢的涂层，耐蚀效果并不理想；与环氧树脂面涂料配合使用，耐蚀效果明显提高；在盐酸摩尔浓度为1mol／L的腐蚀环境中，沥青涂料是比环氧树脂更好的面涂料。浸泡试验表明：在上述两种腐蚀环境中，以聚苯胺一蒙脱土复合材料作为冷轧钢的底涂料，沥青涂料作为面涂料，45天后没有发现腐蚀现象。     

Effect of welding speed and electrode extension on the approximate entropy of welding current in short-circuiting GMAW

Based on the phase space reconstruction of welding current in short-circuiting transfer arc welding under carbon dioxide, the approximate entropy of welding current and its standard deviation have been calculated and analyzed at different welding speeds and different electrode extensions respectively. The experimental and calculated results show that at a certain arc voltage, wire feeding rate and gas flow rate, welding speed and electrode extension have significant effects not only on the approximate entropy of welding current, but also on the stability of welding process. Further analysis proves that when the welding speed and electrode extension are in an appropriate range respectively, the welding current approximate entropy attains maximum and its standard deviation minimum. Just under such circumstances, the welding process is in the most stable state.     

活性元素Ti在CBN与钎料结合界面的特征

通过扫描电镜、能谱仪、X射线衍射仪研究了Ag-Cu-Ti钎料中的活性元素Ti在钎料与立方氮化硼（CBN）磨粒高温钎焊结合界面的扩散现象，并运用动力学分析对界面反应层的生长过程及反应激活能进行了探讨。结果表明：钎焊过程中，钎料中的活性元素Ti明显向磨粒侧扩散偏聚并发生化学反应，实现了磨粒与基体材料的牢固结合；钎焊CBN磨粒表面生成的TiB2和TiN化合物形貌接近平衡状态下生长的理想形貌；界面反应层在钎焊温度1153K～1193K，保温时间5min～20min之间依据抛物线生长法则所得扩散激活能值表明其生长过程主要受新生TiN影响。