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41.
Susan Walter Thomas Herzog Henning Heuer Hagen Bartzsch Daniel Gloess 《Microsystem Technologies》2012,18(7-8):1193-1199
We investigated the potential of the aluminum nitride films to excite ultrasonic waves at frequencies >50?MHz. The deposition process of the aluminum nitride thin film layers on silicon substrates was investigated and optimized regarding their piezoelectric behavior. Large single element transducers were deposited on silicon substrates with aluminum electrodes, under different parameters for the magnetron sputter process, like pressure and bias voltage. Special test setup and a measuring station were created to characterize the sensors. Acoustical measurements were carried out in pulse echo mode up to 500?MHz and the values of piezoelectric charge constant (d33) were determined. As a result, two parameter sets were found for the sputtering process to obtain an excellent piezoelectric charge constant of about 7.2?pC/N maximum. Then the sputtering process with these parameters was used to deposit sensors on various substrate materials and with different electrode sizes. 相似文献
42.
Exergy analysis of incremental sheet forming 总被引:1,自引:0,他引:1
M. A. Dittrich T. G. Gutowski J. Cao J. T. Roth Z. C. Xia V. Kiridena F. Ren H. Henning 《Production Engineering》2012,6(2):169-177
Research in the last 15 years has led to die-less incremental forming processes that are close to realization in an industrial
setup. Whereas many studies have been carried out with the intention of investigating technical abilities and economic consequences,
the ecological impact of incremental sheet forming (ISF) has not been studied so far. Using the concept of exergy analysis,
two ISF technologies, namely single sided and double sided incremental forming, are investigated and compared to conventional
forming and hydroforming. A second exergy analysis is carried out with the purpose of examining the environmental impact of
different forming technologies from a supply chain perspective. Therefore, related upstream activities (die set production,
aluminum sheet production and energy conversion and supply) are included into the exergy analysis. The entire supply chain
is modeled with Matlab/Simulink. The results of both analyses suggest that ISF is environmentally advantageous for prototyping
and small production runs. 相似文献
43.
Reduction of the elongation at break of thermoplastic polyolefins through melt blending with polylactide and the influence of the amount of compatibilizers and the viscosity ratios of the blend components on phase morphology and mechanics
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Carolin Vogt Hans‐Josef Endres Jürgen Bühring Henning Menzel 《Polymer Engineering and Science》2016,56(8):905-913
The objective of this work is the synthesis of a polypropylene/ethylene‐propylene‐rubber (TPO)/polylactide (PLA)/compatibilizer (PVM) blend to reduce the elongation at break of TPO by blending TPO with brittle PLA. Three TPO types with different viscosities were melt blended with PLA and an ethylene/n‐butylacrylate/glycidyl methacrylate terpolymer (PVM) as reactive compatibilizer. All blends had a constant PLA amount of 30 wt%. Two parameters were varied in the experiments, viscosity of the TPO types, and amount of PVM used in the blends. Both parameters played important roles in reducing the nominal elongation at break compared to pure TPO foils and influencing the phase morphology of extruded blend foils. The nominal elongation at break could be reduced by 100‐150% through blending TPO with PLA and PVM. Characterization regarding the blend morphology, especially the size and shape of the dispersed PLA phase in the TPO matrix was done by Environmental Scanning Electron Microscopy (ESEM) images. Investigations of the morphology showed that size and shape of dispersed PLA phases are dependent on the viscosity ratios of the blend components and on the amount of compatibilizer in the blend. AFM images of the polymer blends reveal soft rubbery layers around the dispersed PLA phases. POLYM. ENG. SCI., 56:905–913, 2016. © 2016 Society of Plastics Engineers 相似文献
44.
Analyses of structurally modified quasi‐solid‐state electrolytes using electrochemical impedance spectroscopy for dye‐sensitized solar cells
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Seok‐Jun Seo Andreas Hinsch Welmoed Veurman Henning Brandt Moon‐Sung Kang Sung‐Hee Shin Seung‐Hyeon Moon 《应用聚合物科学杂志》2014,131(1)
Electrochemical properties of structurally modified quasi‐solid‐state electrolytes were examined using porous substrates (PSs). The PS was prepared into two categories by a phase inversion method with a brominated poly(phenylene oxide) (BPPO): the sponge and finger types. Effects of the humidification and cosolvent compositions on the morphology of the PS were analyzed by scanning electron microscopy. In all cases of the PSs, a higher VOC was observed of about 0.1 V than that of a liquid electrolyte owing to a suppressed back electron charge transfer. In addition, the PS prepared by the polymer solution of 1 : 4 : 1 (BPPO : N‐methyl‐2‐pyrrolidone : butyl alcohol) with the humidification process showed better photovoltaic properties in terms of the current density and conversion efficiency owing to the appropriate combinations of pore size, tortuosity, and interconnectivity. Effects of the pore structures were intensively examined using electrochemical impedance spectroscopy. The impedance results revealed that large pores at the surface layers are advantageous for a lower RS and RTiO2. Meanwhile, the straight inner structure is beneficial for the facile I?/I3? diffusion, thus lowering RPt. © 2013 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2014 , 131, 39739. 相似文献
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48.
J. Fuhrmann H. Kppel K.-D. Schleinitz H.-G. Henning 《Advanced Synthesis \u0026amp; Catalysis》1982,324(4):664-666
Applications of the Nuclear Overhauser Effect. I. Investigations of the Structure of Z/E Isomeric 2,3-Diarylazetidin-3-oles The relative configurations of Z/E-isomeric 2,3-diaryl-azetidin-3-oles are determined by mass spectrometry and 1H-n.m.r.-NOE-measurements. The increase of the C(2)-H line intensity by saturation of the OH-signals demonstrates the Z-position of the 2,3-diaryl groups in the isomers 2a . 相似文献
49.
The objective of the present study was to determine if application of microfiltration (MF) or raw milk lactoperoxidase system (LP) could reduce the risk of foodborne illness from Escherichia coli in raw milk cheeses, without adversely affecting the overall sensory acceptability of the cheeses. Escherichia coli K12 was added to raw milk to study its survival as a non-pathogenic surrogate organism for pathogenic E. coli. Five replications of 6 treatments of Cheddar cheese were manufactured. The 6 treatments included cheeses made from pasteurized milk (PM), raw milk (RM), raw milk inoculated with E. coli K12 (RME), raw milk inoculated with E. coli K12 + LP activation (RMELP), raw milk inoculated with E. coli K12 + MF (MFE), and raw milk inoculated with E. coli K12 + MF + LP activation (MFELP). The population of E. coli K12 was enumerated in the cheese milks, in whey/curds during cheese manufacture, and in final Cheddar cheeses during ripening. Application of LP, MF, and a combination of MF and LP led to an average percentage reduction of E. coli K12 counts in cheese milk by 72, 88, and 96%, respectively. However, E. coli K12 populations significantly increased during the manufacture of Cheddar cheese for the reasons not related to contamination. The number of E. coli K12, however, decreased by 1.5 to 2 log cycles during 120 d of ripening, irrespective of the treatments. The results suggest that MF with or without LP significantly lowers E. coli count in raw milk. Hence, if reactivation of E. coli during cheese making could be prevented, MF with or without LP would be an effective technique for reducing the counts of E. coli in raw milk cheeses. The cheeses were also analyzed for proteolysis, starter and nonstarter lactic acid bacteria (NSLAB), and sensory characteristics during ripening. The concentration of pH 4.6 soluble nitrogen at 120 d was greater in PM cheese compared with the other treatments. The level of 12% trichloroacetic acid-soluble nitrogen at 120 d was greater in RM, RME, and RMELP cheeses compared with PM, MFE, and MFELP cheeses. This could be related to the fact that cheeses made from raw milk with or without LP (RM, RME, and RMELP) had greater levels of NSLAB compared with PM, MFE, and MFELP cheeses. Cheeses at 60 d, as evaluated by 8 trained panelists, did not differ in bitterness, pastiness, or curdiness attributes. Cheeses at 120 d showed no differences in acid-taste, bitterness, or curdiness attributes. Sensory analysis at 60 d showed that PM and MFELP cheeses had greater overall sensory acceptability than RM and RME cheeses. The overall sensory acceptability of the cheeses at 120 d showed that PM, MFE, and MFELP cheeses were more acceptable than RM and RME cheeses. 相似文献
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