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141.
142.
Tingfang Hu Jinpeng Chen Haiyan Wang Jun Min Wei 《Petroleum Science and Technology》2006,24(12):1477-1484
Etherification reaction of FCC light gasoline over Hβ zeolite was investigated to decrease the light olefins in motor gasoline while enhancing octane. Etherification activity of several molecular sieve catalysts for FCC light gasoline was studied in a fixed-bed reactor. The influence of pore-enlarging agent (PEG) with different molecular weight, binder (γ-Al2O3), and peptizing agent (HNO3) in the shaping process on etherification activity of Hβ zeolite was studied. The impregnating ways of precursor of oxides and the order of extruding and impregnating were also investigated. The results show that the activity of extruded Hβ zeolite before impregnating precursor of oxides is higher than the reverse order. The best shaping condition obtained was PEG-4000 10%, γ-Al2O3 20%, and HNO3 10%. At the optimal reaction condition, the conversion of tert-olefins reached the peak. 62.93%, the yield of TAME, is also high and the technology can be applied to industry as well. 相似文献
143.
以3-碘苯甲酸为原料,在浓硫酸作用下与乙醇反应制得3-碘苯甲酸乙酯(1),再以无水乙醇为溶剂,在105℃化合物1与80%的水合肼反应8 h,制得3-碘苯甲酰肼(2)。在无水乙醇中,在90~95℃化合物2分别与4-甲基苯甲醛、2-氯苯甲醛、4-氯苯甲醛、4-羟基苯甲醛、2,4-二氯苯甲醛、4-甲氧基苯甲醛、3-硝基苯甲醛、4-硝基苯甲醛和4-二甲氨基苯甲醛反应得到相应的酰腙[3(a~i)]。最后化合物3(a~i)分别与丙酸酐脱水环化成了3-N-丙酰基-2-芳基-5-(3-碘苯基)-1,3,4-(口恶)唑啉类化合物[4(a~i)],收率分别为86.2%,70.5%, 80.1%,68.2%,62.4%,75.2%,73.2%,70.5%和63.2%。并通过元素分析,IR,1H NMR和MS对化合物4(a~i)的结构进行了表征。 相似文献
144.
This paper highlighted the use of X-ray diffraction, scanning electron microscopy and X-ray fluorescence spectroscopy to investigate the changes on the surface composition of high-sulfur coal and pyrite before and after ultrasonic conditioning. The results showed that ultrasonic conditioning resulted in a decrease in the contents of iron and sulfur in coal, an increase in the content of element carbon, and an increase in the purity of the coal. Conversely, ultrasonic conditioning led to an increase in the content of iron and sulfur in pyrite, a decrease in the impure content of calcium, and a relative increase in the purity of the pyrite after ultrasonic conditioning. This study verified that on the one hand, ultrasonic conditioning can promote the pyrite separation from the high-sulfur coal, with the separated pyrite taking the form of FeS; on the other hand, it can produce a cleaning effect on the surface of coal and pyrite with the consequent increase both in hydrophobicity of coal and hydrophilicity of pyrite. The paper introduced ultrasonic pre-treatment of the slurry and stepped froth removal tests of high-sulfur coal and the study on the yield, ash and sulfur content of clean coal in different phases. The results gave further evidence of the increases both in the rate and the selectivity of flotation. This study shows that ultrasonic conditioning can enhance the performance of de-sulphurization of high-sulfur coal flotation. 相似文献
145.
146.
Stock market forecasting has been a challenging financial research topic for decades. In the literature, there are numerous
results based on point methods. However, poor forecasting quality has been a continuous problem. Motivated by the fact that
financial data varies within intervals, we apply interval methods on a well known stock pricing model [3] to predict stock
market variability as intervals. Empirical results obtained with a few different approaches in this paper consistently suggest
that interval forecasts have better overall quality than traditional point forecasts. 相似文献
147.
分析了建筑陶瓷企业实施精益生产的条件和当前推行精益生产的主要障碍,对应用中存在的问题进行了分析并提出了相关建议。 相似文献
148.
149.
SL Nyberg HJ Mann MY Hu WD Payne WS Hu FB Cerra RP Remmel 《Canadian Metallurgical Quarterly》1996,24(6):643-648
OBJECTIVE: The initially well-fixed implants of total hip replacement (THR) are in the long-term subject to aseptic loosening. Many cytokines can contribute to osteolysis due to osteoclast recruitment and/or activation. However, in this respect tumor necrosis factor-alpha (TNF-alpha) plays a pivotal role, because it upregulates interleukin-1 and 6 and granulocyte-macrophage colony stimulating factor. The aim of this study was to assess the eventual presence, cellular localization and extent of expression of TNF-alpha in the synovial-like membrane at the implant or at the cement to bone interface compared to control synovial membrane. METHODS: Twenty samples from the synovial-like membrane of the periprosthetic tissues were compared to control samples. TNF-alpha containing cells were visualized using an avidin-biotin-peroxidase complex (ABC) method and analyzed by light microscopy, double labelling and image analysis. RESULTS: TNF-alpha was found in the periprosthetic tissues in fibroblasts and vascular endothelial cells, but mainly in the macrophages was it found to coincide with areas containing implant-derived debris. TNF-alpha containing cells were more numerous in the synovial-like membrane in the interface tissue from the proximal stem area (2816 +/- 318 cells) than in the control synovial membrane (565 +/- 93 cells, p < 0.01). Interestingly, similarly high TNF-alpha expression (3452 +/- 582 cells) was also seen in the synovial-like membrane of the pseudocapsule. CONCLUSION: These findings suggest that the foreign body-type host reaction caused by THR is characterized by the high expression of TNF-alpha. Because such expression occurred in the interface tissue between the implant and surrounding bone, TNF-alpha, due to its pivotal direct and indirect role in the activation and recruitment of osteoclasts, may contribute to periprosthetic osteolysis and to the loosening of THR. 相似文献
150.
砼受压损伤力学本构模型的研究 总被引:15,自引:1,他引:14
本文利用MTS公司815.02型电液伺服试验系统对砼进行了等应变速率加载控制的应力一应变全曲线试验,应用不可逆热力学和内变量理论的成果建立了砼损伤力学模型,并用概率统计的观点分析了损伤的演化规律。由于考虑了不可逆变形的影响,本文所建本构模型与实验吻合较好。 相似文献