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991.
Wettability of polyimide (PI) and polypropylene (PP) films have been improved using SiOx-like thin layers deposited from a mixture of hexamethyldisiloxane (HMDSO) and oxygen in a microwave distributed electron cyclotron resonance plasma reactor. The films wettability evolution behaviors were evaluated through the results of contact angle measurements, atomic force microscopy (AFM) and X-ray photoelectron spectroscopy (XPS). The plasma depositions of SiOx thin layers in presence of VUV radiation induce a contact angle decrease to about 7° and 35° for PI and PP films, respectively. XPS data showed that such difference in wettability is attributed to the increase of hydrophilic group's proportion at the surface of coated PI films due to VUV irradiation. AFM images showed that the PI surface topography remains relatively smooth when coated in presence of VUV radiation. However, in the case of PP films, AFM images revealed the growth of irregular structure due to a substrate etching effect supported by VUV radiation. For polymers coated without VUV irradiation, the deconvolution of the C1s peaks showed a significant decrease of CO bonds for both PI and PP substrates. 相似文献
992.
La doping effects on intergrowth Bi2WO6–Bi3TiNbO9 ferroelectric ceramics were studied by X-ray diffraction, electron probe microanalysis and dielectric spectroscopy. It was found that the La3+ distribution, ferroelectric phase transition and dielectric relaxation behavior are apparently affected by La doping. With increasing La3+ content, the site of dopant ion varies, the grain growth of Bi5TiNbWO15 is restrained, the Curie temperature is reduced and broadened. Furthermore, two dielectric relaxation loss peaks were observed both in temperature and frequency spectra. The calculated relaxation parameters revealed the oxygen vacancy related to the relaxation process. 相似文献
993.
Observation of calcium aluminate inclusions at interfaces between Ca-treated,Al-killed steels and slags 总被引:1,自引:0,他引:1
B. Coletti B. Blanpain S. Vantilt S. Sridhar 《Metallurgical and Materials Transactions B》2003,34(5):533-538
The evolution of Al2O3-CaO inclusions on molten steel surfaces and at molten steel/slag interfaces was observed in-situ through a confocal scanning laser microscope (CSLM) equipped with a gold-image furnace. Depending on the slag chemistry,
some of the initially liquid inclusions evolved into irregular Al2O3 or SiO2-enriched inclusions during the separation across the interface. Inclusions were found to cluster at specific locations at
the steel/slag interface. Unlike capillary-depression-driven clustering, which is observed on molten steel surfaces, a weak
repulsive force opposes fluid-flow-driven clustering at the steel/slag interface. After clustering, the irregular solid inclusions
were observed to agglomerate to form large aggregates.
This article is based on a presentation given in the Mills Symposium entitled “Metals, Slags, Glasses: High Temperature Properties
& Phenomena,” which took place at The Institute of Materials in London, England, on August 22–23, 2002. 相似文献
994.
I. Egli L. Davidsson M.-A. Juillerat D. Barclay R. Hurrell 《Journal of food science》2003,68(5):1855-1859
Complementary foods based on cereals and legumes often contain high amounts of phytic acid, a potent inhibitor of mineral and trace element absorption. The possibility to degrade phytic acid during the production of complementary foods by using whole grain cereals as the phytase source was investigated. Whole grain rye, wheat, or buckwheat (10%) were added to cereal‐legume‐based complementary food mixtures, and phytic acid was shown to be completely degraded in a relatively short time (1.5 to 3 h) when incubated at optimal conditions for cereal phytase. The potential usefulness of the method for industrial production was demonstrated with a complementary food based on wheat and soybean. 相似文献
995.
An optimal control problem with nonsmooth performance criterion described by a system of ordinary differential equations is considered. Necessary first-order optimality conditions are obtained. 相似文献
996.
D. D. Avrov S. I. Dorozhkin Yu. M. Tairov A. Yu. Fadeev A. O. Lebedev 《Semiconductors》2008,42(13):1469-1474
The problem of the appearance of carbon inclusions in single-crystal silicon carbide ingots grown by the modified Lely method (the so-called graphitization of the ingot) is analyzed. It is shown that the process of graphitization of the ingot is not related to a deficit of silicon in the growth cell; in contrast, it is excess of silicon at the growth surface that inhibits the ingot growth rate and gives rise to intense corrosion of the graphite fittings. 相似文献
997.
998.
I. N. Ishchuk 《Measurement Techniques》2007,50(10):1081-1086
A three-dimensional solution of the direct problem of heat conduction when a linear pulsed heat source acts in the plane of
contact of two semibounded bodies is presented. The solution is obtained by the method of finite differences. An example of
the modeling is considered.
__________
Translated from Izmeritel’naya Tekhnika, No. 10, pp. 42–45, October, 2007. 相似文献
999.
L. Serra-Majem L. Bassas R. Garcí a-Glosas L. Ribas C. Ingl s I. Casals P. Saavedra A. G. Renwick 《Food Additives & Contaminants》2003,20(12):1097-1104
Cyclamate and its metabolite cyclohexylamine affect male fertility in high dose animal studies, but this affect has not been investigated in epidemiological studies. This paper reports the first epidemiological study designed to investigate the possibility of a relationship between cyclamate and cyclohexylamine and male fertility in humans, in which 405 cases of clinically defined infertility in men and 379 controls were surveyed. Semen evaluation, urine analysis for cyclamate and cyclohexylamine and dietary questionnaires were compared between cases and controls. No evidence was found of a significant association between cyclamate intake and male infertility; neither high cyclamate nor high cyclohexylamine excretion were associated with elevated risk. The lack of association remained after adjusting by age, area of residence, education, total energy intake and other variables. No significant correlations were observed between cyclamate intake, metabolism or excretion, and sperm count and motility. The results demonstrate no effect of cyclamate or cyclohexylamine on male fertility at the present levels of cyclamate consumption. 相似文献
1000.
Bing Q. Han Farghalli A. Mohamed Enrique J. Lavernia 《Metallurgical and Materials Transactions A》2003,34(1):71-83
In the present study, the mechanical properties of Fe processed via severe plastic deformation (equal-channel angular pressing (ECAP)) at room temperature were investigated for the first time.
The grain size of annealed Fe, with an initial grain size of about 200 μm, was reduced drastically during ECAP. After eight passes, the grain size reaches 200 to 400 nm, as documented by means of
transmission electron microscopy (TEM). The value of microhardness during pressing increases 3 times over that of the starting
material after the first pass and increases slightly during subsequent pressing for higher-purity Fe. Examination of the value
of microhardness after eight passes as a function of post-ECAP annealing temperature shows a transition from recovery to recrystallization,
an observation that resembles the behavior reported for heavily deformed metals and alloys. The tensile and compression behaviors
were examined. In tension, a drop in the engineering stress-engineering strain curve beyond maximum load was observed both
in the annealed Fe and the ECAP Fe. This drop is related to the neck deformation. The fracture surface, examined by scanning
electron microscopy (SEM), shows vein patterns, which is different from the dimples found on the fracture surface of annealed
Fe. In compression, an initial strain-hardening region followed by a no-strain-hardening region was observed in the ECAP Fe.
The yield strength in tension of the ECAP Fe was observed to be higher than that in compression. The strengthening mechanisms
and softening behavior are discussed. 相似文献