IRIS/AP型电感耦合等离子体光谱仪激发光源常见故障分析

本文介绍IRIS/AP型ICP的激发光源(炬管),并较为全面地阐述和分析其不能正常激发点燃的常见故障及其原因。     

大孔径石蜡加氢精制催化剂的制备

采用氨吸附-程序升温脱附(NH3-TPD)、低温N2吸附(BET)、压汞法以及加氢精制活性评价等技术,探索SiO2-Al2O3载体在制备过程中孔结构和表面性质的变化。实验结果表明,采用特殊扩孔剂制备载体,当焙烧温度为700℃时,平均孔径可达到17.3nm,其中孔径大于20nm的孔占总孔体积的13.2%;同时载体表面上的中、强酸中心也全部丧失,均为弱酸中心。采用该载体制备的MoNiP/SiO2-Al2O3石蜡加氢精制催化剂,在MoO3用量减少了约1/4的情况下,比目前工业上使用的催化剂具有更高的脱金属能力和加氢精制活性。     

One-to-Many and Many-to-One Optical Chaos Communications Using Semiconductor Lasers

A theoretical construction of one-to-many (OTM) and many-to-one (MTO) chaos synchronization communications using semiconductor lasers is presented. One center laser provides strong injections (strong link) to other side lasers, and the side lasers also provide weak injections (weak link) to the center one. Simulation results show that the side lasers synchronize with the center laser through injection-locking. In addition, messages transmitted via the strong links or the weak links experience strong chaos pass filtering, enabling us to realize OTM and MTO communications.     

Estimation for the number of components in a mixture model using stepwise split-and-merge EM algorithm

The main difficulty with EM algorithm for mixture model concerns the number of components, say g. This is the question of model selection, and the EM algorithm itself could not estimate g. On the contrary, the algorithm requires g to be specified before the remaining parameters can be estimated. To solve this problem, a new algorithm, which is called stepwise split-and-merge EM (SSMEM) algorithm, is proposed. The SSMEM algorithm alternately splits and merges components, estimating g and other parameters of components simultaneously. Also, two novel criteria are introduced to efficiently select the components for split or merge. Experimental results on simulated and real data demonstrate the effectivity of the proposed algorithm.     

基于DTW算法的语音识别系统实现

动态时间归整(DTW)算法的实现简单有效,在孤立词语音识别系统中得到了广泛的应用.介绍了将DTW算法移植到TMS320VC5402上实现孤立词语音识别的原理、系统硬件组成和软件设计.研究结果表明,系统能满足实时性能要求,识别效果良好.     

Application of piece‐wise linear weight functions for 2D 8‐node quadrilateral element in contact problems

The present study is a continuation of our previous work with the aim to reduce problems caused by standard higher order elements in contact problems. The difficulties can be attributed to the inherent property of the Galerkin method which gives uneven distributions of nodal forces resulting in oscillating contact pressures. The proposed remedy is use of piece‐wise linear weight functions. The methods to establish stiffness and/or mass matrix for 8‐node quadrilateral element in 2D are presented, i.e. the condensing and direct procedures. The energy and nodal displacement error norms are also checked to establish the convergence ratio. Interpretation of calculated contact pressures is discussed. Two new 2D 8‐node quadrilateral elements, QUAD8C and QUAD8D, are derived and tested in many examples, which show their good performance in contact problems. Copyright © 2004 John Wiley & Sons, Ltd.     

核磁共振谱的岩石孔喉结构分析

刘堂宴 ,王绍民 ,傅容珊 ,周明顺 ,李艳华 ,罗曼 .核磁共振谱的岩石孔喉结构分析 .石油地球物理勘探 ,2 0 0 3,38(3) :32 8～ 333岩心核磁共振 T2 谱和压汞分析数据均在一定程度上反映了岩石的孔喉结构 ,理论分析表明 ,这两组数据具有相关性。应用岩心核磁共振 T2 谱研究岩石孔喉结构 ,关键是确定 T2 与 Pc的转换系数。但以前的方法在 T2与 Pc 的转换过程中 ,需要涉及某些岩石特性参数 ,实用中有一定困难。本文直接利用岩心核磁共振 T2 谱和压汞分析数据之间的相关性 ,客观地确定 T2 与 Pc之间的转换系数 ,避免了确定岩石特性参数的困难。应用本文方法 ,对 6块岩心的多种核磁共振分析数据进行了对比分析 ,做出了 NMR (Nuclear Magnetic Resonance,简称NMR) T2 毛管力曲线和孔喉半径分布 ,并将这些结果与压汞分析的结果进行了对比。结果表明 ,岩心 NMR T2谱在实用性和评价精度上均略显优势 ;至少是在饱含油的条件下 ,岩心的 NMR T2 谱可以用于研究孔喉结构分布 ,油气的弛豫特性作为影响背景值存在 ,对于评价结果没有明显的影响 ;在全部 6块岩心中 ,T2 与 Pc 的转换系数位于 2 5 0 0～ 4 0 0 0μs· MPa之间。     

汽车代用燃料的应用和发展

评述了汽车代用燃料的现状和未来，压缩天然气和液化石油气将率先大量使用，其次是醇燃料，合成燃料和二甲醚将主要用于某些混合动力车，燃料电池因为能源效率高是最有吸引力的车用能源，将于2010-2015年开始在汽车上实际使用，我国石油工业在提升汽油和柴油质量的同时，应与汽车工业联手开发代用燃料，特别要注意发展燃料电池技术。