Synthesis, structure and fluorescence properties of a highly stable indium(III)-2,5-pyridinedicarboxylate coordination polymer

The hydrothermal reaction of 2,5-pyridinedicarboxylic acid (H₂PDC), diethylene triamine and In(NO₃)₃·4.5H₂O gave rise to a two-dimensional (2D) coordination polymer In(OH)(2,5-PDC). This compound crystallizes in the orthorhombic space group Iba2, with cell parameters, a = 12.656(3) Å, b = 20.114(4) Å, c = 6.2216(1) Å, V = 1583.9(5) Å³ and Z = 8. Its structure contains one-dimensional In–O–In–O– chains, which are further linked by 2,5-PDC ligands into a 2D supramolecular neutral framework. The adjacent 2D layers are parallel with each other and construct a three-dimensional framework via hydrogen bands. At room temperature, the compound exhibits intense photoluminescence. On the basis of the results of TG/DTA analyses, the structure is thermally stable up to 390 °C.     

面向下一代网络的资源管理与服务开通解决方案

在向下一代网络演进的过程中，网络结构正经历一场深刻的变革。在这一背景下，新的业务种类和丰富多彩的增值服务大量涌现；同时，如何降低成本和改进服务水平也成为服务提供商越来越关注的问题。     

精密陶瓷部件近净成型技术的发展

重点介绍了近十年发展起来的陶瓷部件的近净成型技术 ,主要包括直接凝固注模成型、凝胶注模成型、陶瓷注射成型、陶瓷无模成型和微注入成型。对这些新的成型方法的原理、工艺过程及应用特点进行了较全面的分析与比较。     

码头建筑物对水位影响的模型试验及计算方法

河岸码头建筑物势必导致其上游水位壅高及对码头附近水流流态产生影响。以汉江沙洋河段为对象 ,通过定床概化物理模型试验研究了码头建筑物对河道水位与流速场的影响。并基于能量平衡原理 ,采用河道恒定非均匀流水面曲线基本方程 ,结合物理模型试验资料 ,计算了码头建筑物附近的水位变化值 ,并提出了码头建筑物产生的水位壅高值的计算方法。     

光纤专用网中基于DSP的Q值在线检测模块的设计

基于误码率与Q值的对应关系，本文介绍一种Q值在线检测方法，模块设计采用DSP技术，并讨论了该模块在光纤工业专用网（FIN）中的应用。     

基于CPX8216硬件平台的GPRS板间切换的实现

GPRS全称通用分组无线业务,它在改进了现有GSM系统后能实现高速的数据传输。首先对GPRS系统做了简单介绍,然后在此基础上详细介绍了GPRS的板间切换在CPX8216硬件平台上的实现方法。     

Adaptive predictive control algorithm based on Laguerre Functional Model

Laguerre Functional Model has many advantages such as good approximation capability for the variances of system time‐delay, order and other structural parameters, low computational complexity, and the facility of online parameter identification, etc., so this model is suitable for complex industrial process control. A series of successful applications have been gained in linear and non‐linear predictive control fields by the control algorithm based on Laguerre Functional Model, however, former researchers have not systemically brought forward the theoretical analyses of the stability, robustness, and steady‐state performance of this algorithm, which are the keys to guarantee the feasibility of the control algorithm fundamentally. Aimed at this problem, we introduce the principles of the Incremental Mode Linear Laguerre Predictive Control (IMLLPC) algorithm, and then systemically propose the theoretical analyses and proofs of the stability and robustness of the algorithm, in addition, we also put forward the steady‐state performance analysis. At last, the control performances of this algorithm on two different physical industrial plants are presented in detail, and a number of experimental results validate the feasibility and superiority of IMLLPC algorithm. Copyright © 2005 John Wiley & Sons, Ltd.     

小浪底3号灌浆洞辐射灌浆孔的成孔技术

辐射灌浆孔是基岩防渗灌浆处理中的一种特殊设计,一般因应特殊部位而设计,技术设计复杂,施工难度大,尤其是其成孔施工难度.小浪底3号灌浆洞辐射灌浆孔是为解决水工建筑物建成后,对可能存在的渗漏通道进行封堵而设计的,其不同角度和深度对成孔技术要求提出了新的课题.     

海上采油作业安全灭火措施--推广采用高倍泡沫灭火技术

对海洋石油平台火灾进行分析 ,提出采用高倍泡沫灭火技术与密集水流相结合的优化灭火措施建议 ,并介绍锦州 93平台应用实例