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91.
氟碳铈矿/直氟碳钙铈矿混层结构中新规则混层矿物的超微结构研究 总被引:4,自引:0,他引:4
用电子衍射和晶格像技术研究了钙稀土氟碳酸盐矿物中的氟碳铈矿(B)/直氟碳钙铈矿(S)混层结构,发现并确定了B_4S_4、B_8S_6、B_1S_6、B_7S_4和B_2S_15种新规则混层矿物的对称性、晶胞参数及理论晶体化学式。根据所获得的高分辨晶格像真实而直观地揭示出该类B_mS_n(m>n)型新规则混层矿物的长周期有序堆垛结构特征及变化规律。 相似文献
92.
用微机计算电子衍射径向分布函数 总被引:1,自引:0,他引:1
本文介绍用微机计算非晶态高聚物电子衍射径向分布函数(RDF)。运用二次样条函数分段拟合及傅氏积分的数学方法,通过 BASIC 程序,只要输入初始实验数据即可自动解算且连续得到与各运算阶段相应的曲线图及其运算结果. 相似文献
93.
脉冲激光LGA法钛表面氮化及其XRD和SEM微观分析 总被引:1,自引:0,他引:1
用调Q-YAG和XeCl脉冲激光在钛表面以激光气体合金化方法生成氮化钛层,用X射线衍射仪分析了不同激光能量、不同N2气压不同作用脉冲数等条件下TiN的结晶取向、结晶形态、氮化程度,用扫描电镜观察了它们的微观结构,对脉冲激光的LGA法机理进行了探讨,也发现了用LGA法对Mo的氮化生成Mo2N. 相似文献
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95.
Chan C.C. Zheng Ming Zhao Qian C. Meng S. 《Industrial Electronics, IEEE Transactions on》2002,49(6):1342-1344
Based on the concepts of cascade multilevel converters and one-cycle technique, comparisons are conducted to characterize the distortion of the pulsewidth modulation (PWM) and one-cycle control methods that were applied to converters. Simulation results for the different control schemes are obtained in PSIM software initially to see the effect of one-cycle control different from that of PWM control. Through the comparisons, the advantages and disadvantages are identified for each method. The one-cycle scheme is better than PWM control in reducing undesirable harmonics and tracing dynamic waveforms. Simulation and experimental results are also provided to verify the conclusions. 相似文献
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98.
A series of polyurethane microcapsules containing a phase change material (PCM) of n‐octadecane was successfully synthesized by an interfacial polymerization in aqueous styrene‐maleic anhydride (SMA) dispersion with diethylene triamine (DETA) as a chain extender reacting with toluene‐2,4‐diisocyanate (TDI). The average diameter of microPCMs is in the range of 5–10 μm under the stirring speed of 3000–4000 rpm. Optical and SEM morphologies of microPCMs had ensured that the shell was regularly fabricated with the influence of SMA. FTIR results confirmed that the shell material was polyurethane and the SMA chains associated on core material reacted with TDI forming a part of shell material. The shell thickness was decreasing in the range of 0.31–0.55 μm with the molar ratio of DETA/TDI from 0.84 to 1.35 and the weight of core material increasing from 40 to 80% (wt %). By controlling the weight ratio of PCM as 40, 50, 60, 70, and 80% in microPCMs, it was found using DSC that the Tm and Tc of microPCMs were in the range of 29.8–31.0oC and 21.1–22.0°C and an obvious phase change had been achieved nearly the same temperature range of that of PCM. The results from release curves of microPCM samples prepared by 1.4, 1.7, and 2.0 g of SMA indicated the release properties were affected by the amount of the dispersant, which attributed to the emulsion effect and shell polymerization structure. The above results suggest that the shell structure of microPCMs can be controlled and the properties of microPCMs determined by shell will perform proper practical usage. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 4996–5006, 2006 相似文献
99.
孟政军 《石油化工安全环保技术》2006,22(2):3-7
运用危险性分析和工作危害分析法,对一套常减压装置适应性改造的危险性进行分析, 找出主要影响因素,制订对策,确保装置改造和生产安全。 相似文献
100.
YAG:Ce Phosphors for WLED via Nano-Pesudoboehmite Sol-Gel Route 总被引:5,自引:0,他引:5
The sub-micron sized YAG : Ce phosphors were synthesized via a modified sol-gel method by peptizing nano-pesudoboehmite particulate. It is found that YAG phase from the dried gel powders appears at 1000 ℃ then the pure YAG phase exists at a relatively lower sintering temperature of 1400 ℃. The smaller sizes of phosphors in the ranges of 1 - 3 μm are obtained due to the contribution of seeding effects of nano-sized alumina particles to strengthen each step of the processes. Both the excitation and emission spectra of photoluminescence of the phosphor obtained at 1400 ℃ meet well with the spectroscopic requirements of the WLED phosphors. 相似文献