溶胶-凝胶法合成硬质合金用Ni基纳米粉末

采用溶胶-凝胶法与自蔓延燃烧法相结合,研究一种Sol-gel自燃烧法合成Ni基纳米粉末的制备方法。用DTA-TG方法研究凝胶的燃烧过程,测定粉末的粒径。结果表明,采用柠檬酸络合法可形成稳定的Ni基干凝胶,具有自蔓延燃烧特性,可不经煅烧直接合成粒度为40~50 nm的纳米级Ni基合金粉末。     

On the Catalytic Activity of Sn Monomers and Dimers at Graphene Edges and the Synchronized Edge Dependence of Diffusing Atoms in Sn Dimers

In this study, in situ transmission electron microscopy is performed to study the interaction between single (monomer) and paired (dimer) Sn atoms at graphene edges. The results reveal that a single Sn atom can catalyze both the growth and etching of graphene by the addition and removal of C atoms respectively. Additionally, the frequencies of the energetically favorable configurations of an Sn atom at a graphene edge, calculated using density functional theory calculations, are compared with experimental observations and are found to be in good agreement. The remarkable dynamic processes of binary atoms (dimers) are also investigated and is the first such study to the best of the knowledge. Dimer diffusion along the graphene edges depends on the graphene edge termination. Atom pairs (dimers) involving an armchair configuration tend to diffuse with a synchronized shuffling (step-wise shift) action, while dimer diffusion at zigzag edge terminations show a strong propensity to collapse the dimer with each atom diffusing in opposite directions (monomer formation). Moreover, the data reveals the role of C feedstock availability on the choice a single Sn atom makes in terms of graphene growth or etching. This study advances the understanding single atom catalytic activity at graphene edges.     

基于STM32的医疗康复室智能家居系统

本文提出一种基于红外通信互联的、可无线操控的医疗康复室智能家居系统设计.此系统一方面实现了家居设施的智能控制,同时可由护士及病患通过红外、语音两种方式对各类家居进行遥控,另一方面红外无线通信具有低功耗、低电磁干扰等优点,减轻了环境中辐射对病人的伤害.这分担了护士的工作,让护士专注于病人病情的诊查,还有利于病人的康复.     

Brine Refrigerants for Low-cost,Safe Aqueous Supercapacitors with Ultra-long Stable Operation at Low Temperatures

Traditional aqueous energy storage devices are difficult to operate at low temperatures owing to the poor ionic conductivity and sluggish interfacial dynamics in frozen electrolytes. Herein, the low-cost brine refrigerants for food freezing and preservation as electrolytes, and unexpectedly realize high ionic conductivity and stable operation of an aqueous storage device at low temperatures are demonstrated. A CaCl₂ brine refrigerant electrolyte (BRE) with a low freezing point −55 °C and high ionic conductivity (10.1 mS cm⁻¹ at −50 °C) is developed for supercapacitors (SCs), which retains 80% of the room temperature capacity at −50 °C and exhibits ultra-long cycle life with excellent capacity retention of 92% over 98,500 cycles, outperforming the other SCs which can be operated below −40 °C in literature. Moreover, the SCs with MgCl₂ and NaCl BREs can also be operated successfully with excellent cycle stability and high-capacity retention at low temperatures of −30 and −20 °C, respectively. Fundamental correlation between various cations and their effect on the freezing point reduction of aqueous electrolytes is revealed via Raman investigation and molecular dynamics simulations. This study provides a rational design strategy for green, inexpensive, and safe low-temperature aqueous electrolytes for energy storage devices.     

Regulation and Reconstruction of Cell Phenotype Gradients Along the Tendon-Bone Interface

Tendon–bone interface is prevalent in the human body. It is divided into four zones: tendon (soft tissue), unmineralized fibrocartilage, mineralized fibrocartilage, and bone (hard tissue). Tendon–bone interface is characterized by a cell phenotype gradient that appears in the different zones. The cell phenotype gradients at the tendon–bone interface are orchestrated by specific intracellular molecular mechanisms, extracellular factors, immune signals, and neurovascular factors. These features have inspired scientists to design systems that mimic natural cell phenotype gradients. These biomimetic systems include the construction of cell sheets, regulation of cellular microenvironments, and the design of gradient functional scaffolds. Exploration of methods to mimic cell phenotype gradients is instructional for future clinical applications in reconstituting the tendon–bone interface. The present review elucidates the gradient composition of the tendon–bone interface. The associated regulatory mechanisms and applications are discussed, with the anticipation of creating a mise en scène for future research in interface tissue engineering.     

An 8-Bit Digitally Controlled Programmable Phase Shifter Circuit for Sinusoidal Signals with 252∘ Phase Control Range

In this paper, the synthesis, design, and implementation of a programmable phase shifter circuit for sinusoidal signals is presented. The proposed circuit, built-up herein with operational amplifiers (OPAMPs), high precision resistors and low voltage switches, consists of a digitally controlled amplitude attenuator in combination with a single-tone orthogonalizer. Experimental results agree with theoretical background: the attained phase range was 252^° in 256 steps with a median step of 0.9^°. The inaccuracy of the circuit was determined to be of 0.03 %. Contrary to other OPAMP approaches for sinusoidal signals reported in the literature and based on a first-order all-pass filter structure, the approximation suggested in this work is based on a different concept. The achieved results demonstrate the functionality of the system for the case of a sinusoidal signal with frequency of 1 kHz. Notwithstanding, the proposed architecture can be extended to operate at higher frequencies by using different building blocks with larger bandwidth. Furthermore, it can be extended as well to work out with other periodic input waveforms, like triangular shapes or square waves, with the use of an appropriate orthogonalizer.     

一种基于热释电传感器p7187的人体测温仪的设计

人体测温仪的设计主要为适应人体体温快速无接触测量的需要。主要介绍热释电红外传感器的工作原理以及最适宜人体红外线检测的热释电传感器p7187的结构和等效电路,阐述了基于热释电传感器p7187的红外测温仪的工作原理,讨论了该系统的设计与实现方法,简单介绍了该测温仪系统的适用条件。应用表明该设计有广泛的临床实用性。     

SaaS技术的发展和演进

分别从表现层、接口层和应用实现层分析SaaS,可以看到SaaS是一种业务模式、一种接口要求和一种软件能力;分析了电信运营商与SaaS的关联,明确了SaaS的发展方向和演进目标,以实现SaaS模式的成功。     

制药工厂洁净室的压差控制

分析介绍了制药工厂洁净室压差控制的目的和作用以及制药工厂相关规范标准中压差控制的目标要求;结合中国新版GMP中压差控制的要求,对制药工厂洁净室压差控制的方法与措施进行了探讨。     

有机显示浮出水面

介绍了有机显示技术的优势及其应用领域。