国产耐火砖在德士古水煤浆气化炉的使用

分析气化炉耐火材料损蚀原因及国产耐火砖在德士古水煤浆加压气化炉中的使用情况，使用结果证明，国产耐火砖可以替代进口砖，每年节约设备投资600万元左右。     

塑料旋转成型用原料的特点、品种和发展

对塑料旋转成型用原料的特点和品种进行总结和讨论，并介绍了最新的发展情况。随着塑料旋转成型的工艺技术的发展，该项工艺可用的原料品种正在大大拓广，旋转成型在塑料加工工艺中的重要性日益增加。     

采用主监视窗扩展技术的增强现实三维注册方法

在增强现实三维注册中,采用重新检测策略时顿卡现象严重。提出一种采用主监视窗扩展技术的增强现实三维注册方法。在检测阶段,引入特征点可信度和主监视窗,并设计主监视窗的分割、扩展和调控策略,大幅提升了计算速度;在跟踪阶段,采用基于图像金字塔的光流算法进行特征点跟踪。实验证明,该方法不仅有效缓解了顿卡现象,也提升了系统整体的实时性。     

2，6－二氯－4－硝基苯胺的合成

以盐酸－过氧化氢为氯代试剂，由对硝基苯胺制备了２，６－二氯－４－硝基苯胺。结果表明，过氧化氢的比例、反应温度对收率有较大的影响。过氧化氢过量，反应温度在５０℃时，可缩短反应时间，提高收率。     

Structure and dynamics of a pentablock copolymer of polystyrene-polybutadiene in a butadiene-selective solvent

We have examined solutions of a polystyrene-polybutadiene pentablock copolymer in n-heptane, a strongly selective solvent for polybutadiene. Small angle neutron scattering from 7 to 15% samples reveals domains about 10 nm in radius formed by the association of 200 polystyrene blocks. Dynamic light scattering measurements on 8 and 9% samples showed three modes: a fast diffusive mode related to the collective diffusion in semidilute solutions/gels; a relaxational mode related to the local dynamics of polystyrene domains trapped in the gel formed by bridging the domains with the polybutadiene chains; and a very slow diffusive mode. The relaxational dynamics persisted over the entire temperature range, becoming faster with increasing temperature, indicating a decreased microviscosity at higher temperatures. The slow dynamics seems to be connected with heterogeneities in the physical gel due to microsyneresis and almost disappeared above 50 °C. Macroscopic phase separation into two liquid phases was observed in a dilute solution of the un-associated copolymer, and into a liquid and gel phase at higher concentrations. The absence of flower-like micelles in dilute solutions and the macroscopic phase seperation suggest that the gels in the pentablock are formed by random association of multiplet domains and not by bridging of micellar domains.     

Electrochemical copolymerization of carbazole and 3‐methylthiophene

The copolymerization of carbazole (CZ) and 3‐methylthiophene (3MeT) was successfully performed electrochemically in freshly distilled boron trifluoride diethyl etherate by direct anodic oxidation of the monomer mixtures, although the oxidation potentials of CZ and 3MeT were quite different. The electrochemical properties of the copolymers were studied with cyclic voltammetry. The influence of the applied polymerization potential on the synthesis of the copolymers was investigated. The higher potential favored the incorporation of 3MeT units into the copolymers. The insertion of 3MeT units into polycarbazole (PCZ) was helpful in improving the conductivity of PCZ. The novel copolymers had the advantages of both PCZ and poly(3‐methylthiophene), that is, good redox activity, good thermal stability, and high conductivity. The structure and morphology of the copolymers were investigated with ultraviolet–visible, infrared spectroscopy, thermal analysis, and scanning electron microscopy. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 1877–1885, 2006     

基于过程控制技术对轮胎硫化过热水主管道振动问题的解决

首先介绍过程控制系统的基本概念、控制模型、质量指标，结合过程控制系统理论分析轮胎硫化过热水制造的控制过程，找出原来控制不稳定的原因，进行被控参数的改变，消除输送管道振动的问题。     

乙苯/乙烯烷基化反应中EA-8402分子筛催化剂的失活动力学研究

用内循环无梯度反应器,在593～633K范围内考察了在乙苯/乙烯进行定向烷基化反应合成对二乙苯时,EA-8402分子筛催化剂的失活行为,建立了相应的失活动力学模型: -da/dt=0.3271exp(-12.94/T)P_(EB)~(0.02)P_(E(?))~(0.383)·α这一模型可作为该反应的宏观动力学模型的补充。由失活级数d=1,按Levenspiel判据推断:其失活机理应该是不受内扩散阻力控制的平行-连串失活。     

基于Nutch与元搜索引擎技术的高校网络舆情监测系统研究

针对高校网络舆情监测工作的不足,结合高校舆情信息的传播特点,提出了在校园网范围内基于Nutch搜索引擎技术进行信息检索,在互联网上采用元搜索引擎技术获取相关信息的舆情监测系统构建方案。采用关键词特征库匹配方式自动进行网络舆情监测,及时准确地发现网络舆情信息;探讨了高校对于网络舆情的监测、分析、引导和反馈等环节的处理方法,从而形成完善的应对机制。     

Investigation and improvement of reversible microfluidic devices based on glass–PDMS–glass sandwich configuration

Reversibly assembled microfluidic devices are dismountable and reusable, which is useful for a number of applications such as micro- and nano-device fabrication, surface functionalization, complex cell patterning, and other biological analysis by means of spatial–temporal pattern. However, reversible microfluidic devices fabricated with current standard procedures can only be used for low-pressure applications. Assembling technology based on glass–PDMS–glass sandwich configuration provides an alternative sealing method for reversible microfluidic devices, which can drastically increase the sealing strength of reversibly adhered devices. The improvement mechanism of sealing properties of microfluidic devices based on the sandwich technique has not been fully characterized, hindering further improvement and broad use of this technique. Here, we characterize, for the first time, the effect of various parameters on the sealing strength of reversible PDMS/glass hybrid microfluidic devices, including contact area, PDMS thickness, assembling mode, and external force. To further improve the reversible sealing of glass–PDMS–glass microfluidic devices, we propose a new scheme which exploits mechanical clamping elements to reinforce the sealing strength of glass–PDMS–glass sandwich structures. Using our scheme, the glass–PDMS–glass microchips can survive a pressure up to 400 kPa, which is comparable to the irreversibly bonded PDMS microdevices. We believe that this bonding method may find use in lab-on-a-chip devices, particularly in active high-pressure-driven microfluidic devices.