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91.
92.
93.
Yu‐Qing Cao Zhan Zhang Yan‐Xin Guo 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2008,83(10):1441-1444
A new efficient method for synthesising nitriles, important organic reagents, is reported in this paper. In an environmentally benign solvent‐free system, aryl carboxylic acids were converted into the corresponding nitriles via one‐pot reactions, by amidation with ethyl carbamate followed by dehydration with thionyl chloride, in excellent yields. The results showed that the method has the advantages of lower cost, higher yield, less pollution and greater ease of work‐up. Copyright © 2008 Society of Chemical Industry 相似文献
94.
95.
采用微软公司Microsoft Excel的规划求解功能,可以快速准确地进行玻璃料方的计算,从而大大提高工作效率.本文以平板玻璃料方为例,对玻璃料方的电子计算机计算原理作介绍,并对利用Excel电子表格的规划求解功能进行玻璃料方计算的过程进行介绍. 相似文献
96.
Poly[2‐methoxy‐5‐(2′‐ethyl‐hexyloxy)‐para‐phenylene vinylene] (MEH‐PPV)/silica nanoparticle hybrid films were prepared and characterised. Three kinds of materials were compared: parent MEH‐PPV, MEH‐PPV/silica (hybrid A films), and MEH‐PPV/coupling agent MSMA/silica (hybrid B films), in which MSMA is 3‐(trimethoxysilyl) propyl methacrylate. It was found that the hybrid B films could significantly prevent macrophase separation, as evidenced by scanning electron and fluorescence microscopy. Furthermore, the thermal characteristics of the hybrid films were largely improved in comparison with the parent MEH‐PPV. The UV‐visible absorption spectra suggested that the incorporation of MSMA‐modified silica into MEH‐PPV could confine the polymer chain between nanoparticles and thus increase the conjugation length. The photoluminescence (PL) studies also indicated enhancement of the PL intensity and quantum efficiency by incorporating just 2 wt% of MSMA‐modified silica into MEH‐PPV. However, hybrid A films did not show such enhancement of optoelectronic properties as the hybrid B films. The present study suggests the importance of the interface between the luminescent organic polymers and the inorganic silica on morphology and optoelectronic properties. Copyright © 2004 Society of Chemical Industry 相似文献
97.
Ying Ding Chunqing Wang Yanhong Tian Binbin Zhang 《Metallurgical and Materials Transactions A》2006,37(12):1017-1025
in-situ transmission electron microscopy (TEM) tensile tests on as-cast and aged 63Sn37Pb solder alloys were conducted, and the fracture
behavior in nanometer scale ahead of the crack tip was inspected and discussed. Results show that the fracture was completed
by connecting the discontinuous cracks or voids. Dislocation behavior was concentrated along the grain boundaries for as-cast
samples, and displayed mainly as dislocation climb. The crack was intergranular dominated under the lower strain rate. While
remarkable mutual dislocation emission was detected in the aged solder. Transgranular cracks were dominant in the fractured
area, and they propagated by linking up with the nanometer scale cracks ahead of the crack tips under the effective promotion
of the inverse dislocation emission. At the same time, the partial interphase or intergranular cracks in the thinned area
were also found. Under this condition, a new critical stress intensity factor K
c
′ to define the mutual dislocation emission was proposed. 相似文献
98.
Wang Xuegang Yan Fengjie Yan Qian Li Xingeng 《Frontiers of Materials Science in China》2007,1(2):225-227
An iron-based amorphous foil (FeNiCrSiB) was used as an interlayer for the amorphous diffusion bonding of low carbon steel
pipes under argon flux. The microstructure and mechanical properties of the joint were analyzed using an electron probe micro-analyzer
(EPMA), tensile test, bending test and impact test. The results show that the joint microstructure resembles that of the base
metal and no precipitates form at the joint. Melting point depressants (B, Si) diffuse far away from the joint and the base
metal element is homogenous across the joint. The joint impact toughness is greater than the base metal toughness and the
mechanical properties of the joint are similar around the pipe. 相似文献
99.
压密注浆及其在地基加固中的应用 总被引:1,自引:0,他引:1
在简单介绍了压密注浆工法的加固机理、影响被加固土体强度的因素的基础上,结合工程实例介绍了压缩注浆工法的工程应用情况。 相似文献
100.
A photochromic nanocomposite based on Keggin structure phosphomolybdic acid (PMoA) well dispersed in polyethyleneglycol (PEG) was fabricated. TEM image showed that PMoA nanoparticles with narrow size distribution were finely dispersed in polymer matrix. FT-IR results showed that the Keggin geometry of polyoxometalates was still preserved inside the composites and strong coulombic interaction was built between PMoA and polymer matrix. Under UV irradiation, the film was reduced photochemically to yield a blue species, which was in accordance with a charge-transfer mechanism. 相似文献