新型涂料增稠剂的化学成分鉴定

本文用红外光谱法对一种新型涂料增稠剂进行了化学成分鉴定,其主要成分为羟丙基甲基纤维素与蒙脱土。     

气敏材料的研究进展

从气敏材料种类，制备方法，改善气敏材料缺陷的手段等方面介绍了气敏材料的研究进展，论述了气敏材料研究中的新动向，展望了它的未来发展。     

化工离心泵的可靠性分析

对石油化工设备安全性和维修技术的研究,需要设备运行故障率等可靠性数据。探讨了如何应用传统可靠性理论知识,并结合国内外相关标准规范和运行数据的统计分析来确定离心泵的可靠性数据的方法。     

工程建设项目职业健康安全和环境管理机构的主要职责

工程建设项目要实施健康、安全和环境管理,文章阐述了工程建设项目职业健康安全和环境管理机构设置的必要性,该机构是项目职业健康安全和环境管理体系及其管理网络的管理者,是完成项目职业健康安全和环境保护管理目标的第一责任部门。该机构的主要职责有:编制作业文件,组织培训教育,进行监测、检查和监督,审核不符合项的整改、纠正和预防工作,记录及其管理,项目职业健康安全和环境管理评审。组织精悍、职责明确的管理机构并通过严密有序的工作,是实现项目健康、安全、环境管理目标的重要保证。     

高压乙烯压缩机出入口管线振动分析及改造

为减轻高压乙烯压缩机出入口管线的振动,采用有限元建模方法,对管线结构固有频率及各阶振型进行分析计算,详细讨论了在管线同一位置加不同约束和在不同位置加同一约束的情况对管线振动的影响.最后,结合测试数据和现场实际情况提出了改造方案.实际使用结果证明改造措施有效,达到了预期的防振效果.     

A segmentation-based fine-grained peer sharing technique for delivering large media files in content distribution networks

Delivering large media files over the Internet is a challenging task because it has some unique features that are different from delivering conventional Web documents. In this paper, we propose a fine-grained peer sharing technique for dealing with the problem in the context of content distribution networks. The key difference of the technique from conventional peer-to-peer systems is that the unit of peer sharing is not a complete media file, but at a finer granularity. By doing so, we improve the flexibility of replica servers for handling client requests. We analyze the storage requirement at replica servers and design a scheduling algorithm to coordinate the delivery process from multiple replica servers to a client. Our simulations show that the fine-grained peer sharing approach can reduce the initial latency of clients and the rejection rate of the system significantly over a simple peer sharing method.     

Formation of mushroom-like ZnO microcrystals through a solution calcination process

Mushroom-like ZnO microcrystals have been prepared via a solution calcination route, using Zn(NO₃)₂ as Zn source in the absence of any surfactants, templates or catalysts. This is the first example to prepare mushroom-like crystals as semiconductors, which are expected to show particular physical properties. The ZnO products were investigated by X-ray powder diffraction (XRD), scanning electron microscopy (SEM), Raman spectroscopy and photoluminescence (PL) spectrum measurements. A suitable concentration of Zn(NO₃)₂ solution was important for the growth of the mushroom-like products. The reported synthetic procedure is straightforward and inexpensive, and thus can be readily adopted to produce large quantities of mushroom-like ZnO microcrystals.     

静压下ZnS：Te中Te等电子陷阱的发光

研究了4块ZnS：Te薄膜样品(Te组分从0．5％到3．1％)的光致发光谱在常压下的温度特性．对于Te组分较小的2块样品观察到2个发光峰，分别来自Te1和Te2等电子陷阱；而对Te组分较大的2块样品则只观察到1个来自Te2等电子陷阱的发光．我们还研究了这些发光峰在低温1．5K下的流体静压压力行为．观察到与Te1有关的发光峰压力系数比ZnS带边的要大很多，而与Te2有关的发光峰压力系数则比带边小．根据Koster-Slater模型，价带态密度半宽随压力的增加是Te1中心有较大压力系数的主要原因，而Te1和Te2中心的不同压力行为则是由于压力对两者缺陷势增强的不同效果引起的．     

支持下一代无线宽带应用自适应QoS模型的研究

作为真正完整的下一代网络 ( NGN,Next Generation Network)解决方案 ,NGN需要在固定通信领域和移动通信领域都能够支持综合多媒体特性。NGN中的新一代移动通信网承载在开放式、层次化结构的分组交换网络之上 ,能够为用户提供端到端的 Qo S解决方案。本文分析了下一代移动通信系统中多媒体宽带应用的 Qo S问题 ,从无线通信系统的多层次结构出发 ,建立了业务流的 Qo S指标评判体系 ,为下一代网络中的无线宽带应用提供了一种自适应Qo S控制模型     

Sol-gel Preparation and Preliminary in vitro Evaluation of Fluorapatite／Hydroxyapatite Solid Solution Films

Fluorapatite/hydroxyapatite solid solution has better biological properties than other apatites, especially used as films or coatings. In this work, sol-gel preparation and in vitro behavior of fluorapatite/hydroxyapatite solid solution films on titanium alloy were investigated. Ca(NO3)2-4H20 and PO(OH)x(OEt)3-x were selected as precursors, and hexafluorophosphoric acid (HPFo) was used as a fluorine containing reagent. The Ca and P precursors were mixed with HPFo to keep the Ca/P molar ratio 1.67. The mixtures refluxed for 12 h were used as dipping sols for the preparation of the films. The phase of the films obtained at 600℃ was apatite. The F contents in the films increased with the concentrations of HPF6 in the dipping sols. The solid solution films were shown to have better stability than hydroxyapatite films, and a reasonably good bioactivity in the in vitro evaluation.