改性低毒脲醛树脂的固化研究

研究了非等温过程中改性低毒脲醛树脂固化体系和未改性脲醛树脂固化体系的固化行为，并研究了不同固化剂施用量对改性树脂固化的影响，对不同树脂体系固化后的结构进行了表征。结果表明，改性的UF树脂固化后的交联度大于未改性树脂固化后的交联度。     

基于动态硼酸酯键改性黄原胶的性能

基于苯硼酸聚合物可以与存在于黄原胶糖环单元结构中的伯、仲醇羟基通过硼酸酯键形成动态共价微交联结构的性质对黄原胶进行改性。以偶氮二异丁基脒二盐酸盐（AIBA）为引发剂，通过水相自由基聚合，制备了不同共聚比的丙烯酰胺（AM）、N-(3-二甲氨基丙基)丙烯酰胺（DMAPAM）和3-丙烯酰胺基苯硼酸（AMBB）的三元共聚物P(AM-co-DMAPAM-co-AMBB)。通过1H NMR、FTIR、元素分析和光散射对聚合物结构及相对分子质量进行了表征，并对其与黄原胶复配体系的增黏性、流变性、抗老化性及抗干扰性进行了评价。结果表明：P(AM-co-DMAPAM-co-AMBB)与黄原胶复配后对黄原胶溶液具有明显的增黏性，其中苯硼酸单体的摩尔比为1.0 mol%的聚合物对黄原胶溶液的增黏幅度达43.8%，在8074 mg/L的矿化水中增黏幅度高达56.4%，且复配体系具有良好的抗老化降解性，对乙二醇和1,3-丙二醇具有较强的抗干扰性。     

涡轮轴疲劳试验器控制系统设计

在航空发动机研制过程中,对涡轮轴进行模拟加载疲劳试验是一项重要的工作。该试验用于验证涡轮轴设计、加工是否具有足够的强度和在寿命期具有足够的疲劳寿命。试验器电气控制系统采用计算机加数据采集控制多功能卡模式组成核心控制系统。电气控制系统采用NI公司的虚拟仪器软件LabWindows/CVI作为控制和人机界面(HMI)的编程软件。     

Prevention from Soft Errors via Architecture Elasticity

Due to the decreasing threshold voltages, shrinking feature size, as well as the exponential growth of on-chip transistors, modern processors are increasingly vulnerable to soft errors. However, traditional mechanisms of soft error mitigation take actions to deal with soft errors only after they have been detected. Instead of the passive responses, this paper proposes a novel mechanism which proactively prevents from the occurrence of soft errors via architecture elasticity. In the light of a predictive model, we adapt the processor architectures h01istically and dynamically. The predictive model provides the ability to quickly and accurately predict the simulation target across different program execution phases on any architecture configurations by leveraging an artificial neural network model. Experimental results on SPEC CPU 2000 benchmarks show that our method inherently reduces the soft error rate by 33.2% and improves the energy efficiency by 18.3% as compared with the static configuration processor.     

An Elastic Architecture Adaptable to Various Application Scenarios

The quantity of computer applications is increasing dramatically as the computer industry prospers. Meanwhile, even for one application, it has different requirements of performance and power in different scenarios. Although various processors with different architectures emerge to fit for the various applications in different scenarios, it is impossible to design a dedicated processor to meet all the requirements. Furthermore, dealing with uncertain processors significantly aggravates the burden of programmers and system integrators to achieve specific performance/power. In this paper, we propose elastic architecture （EA） to provide a uniform computing platform with high elasticity, i.e., the ratio of worst-case to best-case performance/power/performance-power trade-off, which can meet different requirements for different applications. It is achieved by dynamically adjusting architecture parameters （instruction set, branch predictor, data path, memory hierarchy, concurrency, status~zcontrol, and so on） on demand. The elasticity of our prototype implementation of EA, as Sim-EA, ranges from 3.31 to 14.34, with 5.41 in arithmetic average, for SPEC CPU2000 benchmark suites, which provides great flexibility to fulfill the different performance and power requirements in different scenarios. Moreover, Sim-EA can reduce the EDP （energy-delay product） for 31.14% in arithmetic average compared with a baseline fixed architecture. Besides, some subsequent experiments indicate a negative correlation between application intervals＇ lengths and their elasticities.     

在线红外检测仪在头孢噻肟酸合成中的应用

利用在线红外检测仪ReactIRTM4000在线监测以7-氨基头孢烷酸(7-ACA)与2-甲氧亚氨基-2-(2-氨基-4-噻唑基)-硫代乙酸苯并噻唑酯(MEAM)为原料,用二甲基乙酰胺(DMA)作催化剂,一步合成头孢噻肟酸的实验过程,主要考察了反应时间对反应的影响。在最佳反应条件下(催化剂用量、反应物用量、结晶pH已经优化)头孢噻肟酸的合成摩尔收率超过98%。     

新型空穴传输材料N,N′-二苯基-N,N′-二(3-甲苯基)-4,4′-联萘胺的合成、薄膜发光与能级比较

将有机电致发光中最常用的空穴传输材料N,N′-二苯基N,N′-二(3甲苯基)-4,4-′联苯胺(TPD)中的联苯以联萘代替,合成了新型空穴传输材料N,N′-二苯基N,N′-二(3-甲苯基-)4,4′-联萘胺(PMPN)。与TPD在熔点、薄膜发光、量子效率和电化学行为上进行了比较。PMPN比TPD(m.p.175℃)有稍低的熔点、稍高的电离势,更高的薄膜荧光量子效率。联萘的引入可以增大体系的共轭作用,对载流子传输有益。通过构效关系的分析,可以对进一步合成高性能空穴材料进而得到高性能的有机电致发光器件有所借鉴。     

CaCO3/natural rubber latex nanometer composite and its properties

Calcium carbonate/natural rubber (NR) latex nanometer composites were prepared by adding nanometer CaCO₃ whose surface had been treated to natural rubber latex (NRL) before sulfuration. The physical, thermooxidative aging, and thermal degradation properties and the ultra‐microstructure were analyzed with a multipurpose material testing meter, a thermal analysis meter and a Philips XL‐30 SEM, respectively. The results showed that the structures and properties of nanometer composites could be clearly improved by NRL mixed with surface‐treated nanometer CaCO₃. The physical properties of the nanometer composites were best when the content of surface treatment agent was 2.5% (to nanometer CaCO₃), the nanometer CaCO₃/NRL content was 3:100, and the stirring time for treating the surface of the nanometer CaCO₃ was 20 min. Simultaneously, the thermooxidative aging resistance of the nanometer composites also was significantly improved. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 101: 3442–3447, 2006     

基于Fisher 准则和最大熵原理的SVM核参数选择方法

针对支持向量机(SVM)核参数选择困难的问题,提出一种基于Fisher准则和最大熵原理的SVM核参数优选方法.首先,从SVM分类器原理出发,提出SVM核参数优劣的衡量标准;然后,根据此标准利用Fisher准则来优选SVM核参数,并引入最大熵原理进一步调整算法的优选性能.整个模型采用粒子群优化算法(PSO)进行参数寻优.UCI标准数据集实验表明了所提方法具有良好的参数选择效果,优选出的核参数能够使SVM具有较高的泛化性能.     

加强协调促进甲烷氯化物企业健康有序发展

回顾了我国甲烷氯化物行业的发展概况，着重介绍了甲烷氯化物下游产品对该行业的影响。提出促进甲烷氯化物行业健康有序发展的建议。