Synthesis and characterization of molybdenum disulphide formed from ammonium tetrathiomolybdate

An investigation has been carried out into the possibility of in situ formation of MoS2 within porous anodic films on aluminium, to improve subsequent tribological behaviour, by re-anodizing in thiomolybdate electrolyte. Acidification of thiomolybdate was employed to simulate the conditions for formation of the sulphide at the anodic film/electrolyte interface, followed by appropriate vacuum heat treatments to study possible temperature effects on the sulphide due to either friction or Joule heating during anodizing. The products of both acidification and heat treatment, characterized by X-ray powder diffraction and scanning electron microscopy, were compared with those formed by direct thermal decomposition of ammonium tetrathiomolybdate crystals. The precipitate formed by acidification was mainly amorphous molybdenum trisulphide (MoS3), which on heat treatment at 450 and 850°C yielded 3R-MoS2. 3R-MoS2 also formed by the thermal decomposition of thiomolybdate crystals. Thermogravimetric and differential thermal analyses showed that the decomposition of MoS3 to MoS2 occurred in the range 220–370°C and revealed the sequence of reaction steps. The findings suggest that mainly amorphous MoS3 is formed as a consequence of changes in the pH of the film/electrolyte interface during re-anodizing but the product is relatively easily transformed to crystalline MoS2 on moderate heating which may occur during wear processes.     

超薄SiO2层的热生长

隧道小孔中超薄ＳｉＯ２的生长是ＥＥＰＲＯＭ电路制造的关键工艺之一。采用ＳＵＰＲＥＭ－Ⅲ工艺模拟程序对超薄ＳｉＯ２的热生长进行了工艺模拟，经过大量的工艺实验及优化，确定了超薄ＳｉＯ２的最佳生长条件，生长出的ＳｉＯ２性能良好，完全可满足ＥＥＰＲＯＭ研制的要求。     

一种改进的共同进化遗传算法及其应用

将共同进化遗传算法应用于临床营养决策优化中,虽然取得了一定成果,但算法中仍存在早熟现象、局部搜索能量弱等问题,为此提出一种改进的共同进化模型。算法使用新的子群体划分方法和交叉算子,引入精英保留策略、信息交换原则和小生境技术。通过对糖尿病营养治疗的仿真表明,改进后的算法在保证群体多样性和避免早熟现象的前提下,提高了算法的局部和全局寻优能力,且膳食配方中营养素达标率符合要求,满足专家建议的糖尿病饮食需求。     

基于Dynaform的汽车液位传感器外壳拉深过程研究

针对拉深件在实际生产中所产生的拉裂、起皱等问题，利用有限元理论，运用Dynaform软件对汽车液位器外壳模型进行拉深的数值模拟，直观体现板材在拉深时的变化过程，对生产起到指导作用。     

缺血性糖尿病下肢病变的膝下动脉成形术

目的探讨膝下动脉的球囊成形术在治疗糖尿病缺血性下肢病变中的价值。方法对５３例糖尿病合并缺血性下肢病变患者６４侧缺血性下肢进行膝下动脉Deep球囊扩张成形术。对比患者手术前后临床症状的改变及足部溃疡的变化。结果５３例患者共１１９支动脉分支接受PTA治疗，５０例患者的１０１个分支成功地开通，技术成功率为８４．９％，所有５０例患者的临床症状均明显缓解，足部溃疡均变小，无需截肢。结论膝下动脉的球囊成形术是治疗缺血性糖尿病下肢病变安全有效的微创手段     

HACCP在紫菜米果生产中的应用研究

在分析和研究紫菜米果的生产工艺的基础上,探讨了危害分析与关键点控制(HACCP)质量管理体系在其生产中的应用,以求确保产品的安全卫生,保证消费者的健康,使产品达到出口标准.     

我国废旧电脑的危害及其管理对策

论述了我国废旧电脑的产生和回收利用现状、废旧电脑对环境和人体的危害，以及废旧电脑的可再利用性，提出了对废旧电脑进行合理回收利用的管理对策。     

铜杆信息采集系统的研究

阐述了铜杆生产过程中信息采集系统的主要研究内容；概括了硬件的结构和选用的主要设备；阐述了上位机软件的主要模块及实现方法；系统采用面向对象的编程方法，界面友好，操作简单，功能完善；实际运行效果良好，具有较好的应用前景。