常见金属眼镜架中有害元素的含量分析

本文针对市面上常见金属眼镜架的主要成分,利用X射线荧光光谱进行无损检测,测定并分析其中主要成分,并对其进行分类总结。     

Toward Energy-Efficient and Trustworthy eHealth Monitoring System

The rapid technological convergence between Internet of Things(IoT),Wireless Body Area Networks(WBANs)and cloud computing has made e-healthcare emerge as a promising application domain,which has significant potential to improve the quality of medical care.In particular,patient-centric health monitoring plays a vital role in e-healthcare service,involving a set of important operations ranging from medical data collection and aggregation,data transmission and segregation,to data analytics.This survey paper firstly presents an architectural framework to describe the entire monitoring life cycle and highlight the essential service components.More detailed discussions are then devoted to {\em data collection} at patient side,which we argue that it serves as fundamental basis in achieving robust,efficient,and secure health monitoring.Subsequently,a profound discussion of the security threats targeting eHealth monitoring systems is presented,and the major limitations of the existing solutions are analyzed and extensively discussed.Finally,a set of design challenges is identified in order to achieve high quality and secure patient-centric monitoring schemes,along with some potential solutions.     

NH_3-OH体系中共沉淀法同时回收钕铁硼废料中Nd-Pr-Co-Fe

为了避免回收单一钕铁硼废料中有价元素带来的操作复杂和资源浪费等问题,本研究采用共沉淀法共沉淀出钕铁硼废料中的有价元素Me(Nd,Pr,Co,Fe),制备可用于生产再生钕铁硼的原料;根据质量守恒和同时平衡原理,采用MATLAB软件建立Me(Nd,Pr,Co,Fe)-OH--NH3热力学模型,绘制lg[Me]-p H曲线模拟共沉淀工艺,并根据模拟结果确立了共沉淀工艺;模拟和实验的结果表明:根据lg[Me]-p H模拟结果可以确立一步共沉淀法的p H:6~10,Fe3+比Fe2+更易于沉淀完全;在上述条件下获得的共沉淀粉末主相均为Nd,Pr,Co,Fe的化合物,且有价元素的百分比含量均大于99.4%;其中,当p H值在8左右时回收率最高,在该条件下金属元素Me(Nd,Pr,Co,Fe)的沉淀效率分别为:98.7%,99.9%,93.6%,99.9%。该结果也表明共沉淀法工艺不仅高效,而且所制备的共沉淀粉末可以满足制备二次钕铁硼的需要。     

氨汽提尿素装置高压系统降压操作控制

通过对氨汽提尿素装置高压系统合成操作压力的理论分析,结合实际工况降低高压系统操作压力,使装置的设备运转状况得到有效改善。     

大型复杂工程管理的方法论

本文首先对大型工程系统中的复杂性展开详细分析,然后结合复杂性管理中的各种概念和理论,进一步探讨大型复杂工程管理上的综合集成管理方法论,以供参考。     

Room Temperature Ferromagnetism in Co-doped CuAlO2 Nanofibers Fabricated by Electrospinning

One-dimensional, diluted magnetic semiconductor nanofibers have attracted increasing attention for their unique magnetic properties, large specific surface area, and high porosity. These qualities lead to excellent performance in magneto-optical devices, magnetic resonance imaging, ferrofluids and magnetic separation. The purpose of this study is to fabricate P-type one dimensional CuAlO2-based diluted magnetic semiconductor nanofibers. First, we fabricated Cu Al0.95Co0.05O2 nanofibers with an average diameter of 1 μm with the electrospinning method. The annealed nanofibers were thermally treated at a temperature of 1 100 ℃ and then shrunk to a diameter of about 650 nm. We used X-ray diffraction measurements and Raman spectra to confirm that the Cu Al0.95Co0.05O2 nanofibers had a single impurity free delafossite phase. The X-ray photoelectron spectroscopy analysis indicates that Co was present in the +2 oxidation state, resulting in an room temperature ferromagnetism in the Cu Al0.95Co0.05O2 fiber. This contrasts with nonmagnetism in pristine CuAlO2 fiber. The coercivity(Hc) value of 65.26 Oe and approximate saturation magnetization(Ms) of 0.012 emu/g demonstrate good evidence of ferromagnetism at room temperature for Cu Al0.95Co0.05O2 nanofibers.     

石墨烯与金属盐及金属氧化物复合的研究现状

在电化学方面,石墨烯被公认为最具有研究前景的锂电电极材料之一。但是由于制造工艺等因素的影响,石墨烯还无法直接用于锂电池的工业化生产。相比之下,石墨烯与金属盐及金属氧化物复合作为锂电电极材料,人们研究得更加全面而且更加容易实现工业化。介绍了几种石墨烯与金属盐及金属氧化物复合的方法,原理简单,效果显著,在生产和研究方面都有着广阔的应用前景。     

小半径缓和曲线钢板组合梁整体顶推技术

近年来,在山区桥梁设计中越来越多的应用了钢板组合梁。因此,以某工程为例,其采用钢板组合梁,桥梁平面位于小半径圆曲线及缓和曲线上,场地受限,仅能采用顶推工艺,因此总结了小半径缓和曲线钢板组合梁整体顶推技术要点,从而为类似工程提供一定借鉴。