Tensile properties and fracture characteristics of spray cast alloy IC6 （Ni-7.8Al-14Mo-0.05B）

Tensile testing results of spray cast Ni3Al-based superalloy indicated that the yield strength and tensile strength increase with the increasing of temperature and reached maximum at around 760℃, then decrease with the increasing of temperature. After high temperature isostatic pressing (HIP), yield strength decreased and ductility and tensile strength increased. Stereographic projection showed that no matter at room temperature, medium temperature or high temperature, cracks extend along (111).     

Corrosion of two kinds of cast steels containing chromium in hot concentrated alkaline

A typical hot concentrated alkaline corrosion environment exists in alumina metallurgical industry, so that steel materials with outstanding alkaline corrosion resistance are strongly demanded for its processing equipment. In this paper, the corrosion resistance of two kinds of martensitic cast steels containing chromium in static 303g/L NaOH alkaline solution at 85℃ was studied through polarization and potential-time curves, corrosion weight loss and corrosion morphology analysis. Experimental results showed that protection effect by passive film of cast steel containing Cr was temporary. The low carbon steel without Cr content also exhibited chemical passivity in the same solution. The corrosion mode of the tested Cr-containing cast steel was composed of active dissolving corrosion and caustic embrittlement cracking. Dissolving corrosion was the primary mechanism for the induced weight loss, while severe caustic embrittlement cracking was secondary. With the increase of chromium content in the cast steel, the tendency of the caustic embrittlement cracking decreased, while the active dissolving corrosion increased.     

Microstructure refinement of Sn-Sb Peritectic alloy by power ultrasonic

Sn-Sb peritectic alloy was treated with 400 W, 600 W and 800 W ultrasonic, respectively, to study the effect of power ultrasonic on solidification microstructure. Results show that power ultrasonic can refine α phase and β phase of the alloy, as well as eliminate gravitational segregation. Moreover, 600 W ultrasonic demonstrated the best refining effect, not only homogenous and fine solidification microstructure can be obtained, the cubical β phase crystals can also be spheroidized.     

INFLUENCES OF TRACE ADDITIONS OF STRONTIUM AND PHOSPHORUS ON ELECTRICAL RESISTIVITY AND VISCOSITY OF LIQUID Al-Si ALLOYS

ＩＮＦＬＵＥＮＣＥＳＯＦＴＲＡＣＥＡＤＤＩＴＩＯＮＳＯＦＳＴＲＯＮＴＩＵＭＡＮＤＰＨＯＳＰＨＯＲＵＳＯＮＥＬＥＣＴＲＩＣＡＬＲＥＳＩＳＴＩＶＩＴＹＡＮＤＶＩＳＣＯＳＩＴＹＯＦＬＩＱＵＩＤＡｌＳｉＡＬＬＯＹＳ①ＧｕｉＭａｎｃｈａｎｇ，ＪｉａＪｕｎ，...     

电离层涡旋加热波的传播特性理论分析

涡旋波加热是目前电离层加热试验技术研究的一个热点,但主要侧重于试验现象的分析和解释,对涡旋加热波传播特性及空间场分布特性的讨论很少.文章从菲涅耳衍射理论出发,利用厄米-高斯模和拉盖尔-高斯模的相互转换关系,对电离层涡旋加热波在自由空间的传播特性进行了理论分析,推导了其解析表达式.结果表明涡旋电磁波在传播时,可保持自身表达形式的不变性.依据解析表达式,仿真分析了涡旋波空间幅相分布与拉盖尔-高斯模阶数的关系,给出了涡旋场峰值波束指向的求解方法和公式.这些结论为利用涡旋波深入开展电离层加热研究,实现可控的涡旋加热场空间分布提供了一定的理论指导.     

原子吸收分光光度法测定土壤中的镍的方法研究

本文对微波消解-原子吸收分光光度法测定土壤样品中的镍元素的分析方法进行了探讨,并对不同类型土壤消解后赶酸与不赶酸的测定结果进行了比较。结果表明,原子吸收法测定土壤中的镍必须赶酸,但赶酸的方法可以简化,并利用连续光源原子吸收光谱图进行了验证。     

Reaction of (C_5H_5)_2NdCl·2LiCl with n-Butyllithium: Formation and Crystal Structure of [Li(DME)_3][(C_5H_5)_3Nd(μ-H)Nd(C_5H_5)_3]

Reaction of (C_5H_5)_2NdCl·2LiCl with n-Butyllithium: Formation and Crystal Structure of [Li(DME)_3][(C_5H_5)_3Nd(μ-H)Nd(C_5H_5)_3]     

固体超强酸催化合成乙酸松油酯的实验与应用

使用自制的固体超强酸催化剂 ,将松油醇和乙酸酐合成乙酸松油酯 ,催化剂用量 3% ,反应时间 3h,反应温度 40℃ ,松油醇转化率 99% ,乙酸松油酯选择性 97% ,分馏得到纯度 95 %的产品 ,生产工艺进入中试阶段。