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Amanda D’Cruz Mangesh G. Kulkarni Lekha Charan Meher Ajay K. Dalai 《Journal of the American Oil Chemists' Society》2007,84(10):937-943
A series of alkali metal (Li, Na, K) promoted alkali earth oxides (CaO, BaO, MgO), as well as K2CO3 supported on alumina (Al2O3), were prepared and used as catalysts for transesterification of canola oil with methanol. Four catalysts such as K2CO3/Al2O3 and alkali metal (Li, Na, K) promoted BaO were effective for transesterification with >85 wt% of methyl esters. ICP-MS analysis
revealed that leaching of barium in ester phase was too high (~1,000 ppm) when BaO based catalysts were used. As barium is
highly toxic, these catalysts were not used further for transesterification of canola oil. Optimization of reaction conditions
such as molar ratio of alcohol to oil (6:1–12:1), reaction temperature (40–60 °C) and catalyst loading (1–3 wt%) was performed
for most efficient and environmentally friendly K2CO3/Al2O3 catalyst to maximize ester yield using response surface methodology (RSM). The RSM suggested that a molar ratio of alcohol
to oil 11.48:1, a reaction temperature of 60 °C, and catalyst loading 3.16 wt% were optimum for the production of ester from
canola oil. The predicted value of ester yield was 96.3 wt% in 2 h, which was in agreement with the experimental results within
1.28%. 相似文献
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Amanda Baker Michael Lanagan Clive Randall Elena Semouchkina George Semouchkin Khalid Z. Rajab Richard Eitel Khalid Z. Rajab Raj Mittra Sorah Rhee Peter Geggier Claus Duschl Günter Fuhr 《International Journal of Applied Ceramic Technology》2005,2(6):514-520
At the Keck Smart Materials Integration Laboratory at Penn State University, low-temperature co-fired ceramic (LTCC) material systems have been used to fabricate a number of devices for a variety of applications. This article presents an overview of the integration of the concepts and materials that we have used to achieve miniaturization and unique device function. Examples of microwave filters, metamaterial antennas, and a dielectrophoretic cell sorter will be presented, with emphasis on device modeling and design, prototype construction methods, and test results. 相似文献
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The experience of the Mississippi State University (MSU) Libraries illustrates the challenges presented by moving from consortial to local chat, as well as an evaluation of the advantages of chat reference in an academic setting. Countering the consortial, instant-messaging model prevalent in virtual reference today, the MSU Libraries have found chat offers advantages in an academic community. Moving to a local setting, it was possible for the MSU Libraries to maintain quality control over chat transactions while building relationships with faculty and students across campus. 相似文献
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Telehealth and ubiquitous computing for bandwidth-constrained rural and remote areas 总被引:1,自引:1,他引:0
The information and communication technology infrastructure available in rural and remote areas may often not have the bandwidth to support all types of telehealth applications; therefore, for example, some traditionally envisaged videoconferencing-based telehealth applications may not be able to be used or not used in their anticipated form at this time. While the level of broadband services available may impose limitations on these types of telehealth applications, in this review article, we identify applications that allow the maximizing of telehealth benefits in the presence of low-bandwidth connectivity and have potential benefits well-matched to rural and remote area healthcare challenges. In particular, we include consideration of how ubiquitous computing might potentially bring non-traditional approaches to telehealth that can also come into usage more immediately in bandwidth-constrained rural and regional areas. In this article, we review the benefits of ubiquitous computing for rural and remote telehealth including social media-based preventative, peer support and public health communication, mobile phone platforms for the detection and notification of emergencies, wearable and ambient biosensors, the utilization of personal health records including in conjunction with mobile and sensor platforms, chronic condition care and management information systems, and mobile device–enabled video consultation. 相似文献
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Alireza Pourshahid Daniel Amyot Liam Peyton Sepideh Ghanavati Pengfei Chen Michael Weiss Alan J. Forster 《Electronic Commerce Research》2009,9(4):269-316
A number of recent initiatives in both academia and industry have sought to achieve improvements in e-businesses through the
utilization of Business Process Management (BPM) methodologies and tools. However there are still some inadequacies that need
to be addressed when it comes to achieving alignment between business goals and business processes. The User Requirements
Notation (URN), recently standardized by ITU-T, has some unique features and capabilities beyond what is available in other
notations that can help address alignment issues. In this paper, a URN-based framework and its supporting toolset are introduced
which provide business process monitoring and performance management capabilities integrated across the BPM lifecycle. The
framework extends the URN notation with Key Performance Indicators (KPIs) and other concepts to measure and align processes
and goals. An example process for controlling access to a healthcare data warehouse is used to illustrate and evaluate the
framework. Early results indicate the feasibility of the approach. 相似文献
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Fabrication and Optical Properties of Periodic Ag Nano‐Pore and Nano‐Particle Arrays with Controlled Shape and Size over Macroscopic Length Scales 下载免费PDF全文
Colm T. Mallon Kiang W. Kho Houda Gartite Robert J. Forster Tia E. Keyes 《Advanced Engineering Materials》2018,20(1)
A facile and economical route to preparation of highly ordered sliver pore or particle arrays with controlled pore‐shape and size extended over cm2 areas is described. The substrates are prepared at planar and curved surfaces via sphere‐imprinted polymer (PDMS) templating using polystyrene spheres with diameters of 820, 600, or 430 nm. Nano‐pore arrays are created by sputtering 80 nm of Ag directly onto the templates and nano‐particle arrays are prepared by electrode‐less deposition of Ag from Tollen's reagent. The shape of the nano‐pore or particles in the array conformed to that of the imprint of the sphere on the template. Stretching the flexible template enable creation of cuboid shaped nano‐voids and nano‐particles following Ag deposition. Diffuse reflectance from the spherical Ag nano‐cavity arrays showed absorbance maxima at wavelengths comparable similar to the diameter of the templating sphere, whereas reflectance from the cuboid arrays, showed little correlation with the sphere diameter. The cuboid nano‐particle arrays showed the most intense visible absorption which is red‐shifted compared to the spherical arrays. White light diffraction from the arrays, observed by rotating 1 cm2 substrates relative to a fixed light source, reflected exactly the symmetry axes of the periodic nano‐features in the arrays demonstrating the remarkable macroscopic order of the periodic structures. Raman spectra of 1‐benzenethiol adsorbed at the arrays indicated SERS enhancements from the substrates are attributed mainly to surface nano‐roughness with only moderate contributions from the periodically corrugated structures. Despite excitation at the major resonance dip in the reflectance spectrum, a weak, localized rim dipole mode is found to elicit a small increase in the SERS enhancement factor for the 430 nm diameter spherical arrays. FDTD studies of nano‐void arrays provided insights into v arious factors affecting the SERS experiment and confirmed the array's plasmonic spectra are dominated by propagating plasmon modes under microscope excitation/collection angles. 相似文献