Hybrid gas-to-particle conversion and chemical vapor deposition for the production of porous alumina films

Porous alumina films can be found in a wide variety of materials, including filters, thermal insulation components, dielectrics, biomedical and catalyst supports, coatings and adsorbents. Production methods for these films are as equally diverse as their applications. In this work, a hybrid process based upon chemical vapor deposition and gas-to-particle conversion is presented as an alternative technique for producing porous alumina films, with the main advantages of solvent-free, low substrate-temperature operation. In this process, nanoparticles were produced in the vapor phase by reaction of aluminum acetylacetonate in the presence of oxygen. Downstream of this reaction zone, these nanoparticles were collected via thermophoresis onto a cooled substrate, forming a porous film. Some deposited films were subjected to post-processing in the form of annealing in air. Fourier-transform infrared spectra and X-ray energy-dispersive spectroscopy analysis confirmed the production of alumina at processing temperatures above 973 K. X-Ray diffraction revealed that the films were amorphous. Film thickness, ranging from 30 to 250 μm, and the average deposition rate were determined from scanning electron microscopy results. From transmission electron microscopy, the average primary particle size was determined to be approximately 18 nm and the formation of nanoparticle aggregates was evident. Annealing of the films at temperatures ranging from 523 to 1173 K in the presence of air did not have an effect on particle size. The specific surface area of the powder composing the films ranged from 10 to 185 m² g⁻¹, as determined from nitrogen gas adsorption by the Brunauer–Emmett–Teller method.     

用于热核巨共振研究的大面积BGO闪烁探测器

报道了大面积BGO闪烁控制器用于132MeV^16O ^197Au反应中形成的热核巨共振研究，利用飞行时间法鉴别中子、γ。用EGS4程序模拟探讨器对γ连续谱的响应，利用BGO闪烁探测器中Ge俘获中子发射的γ对探测器进行了能量刻度。     

激光起爆与点火系统中光纤连接器

介绍了激光起爆与点火系统中光纤连接器的原理、种类、技术特性及损耗，并对激光起爆与点火系统中光纤连接器的研制动向进行了概括，最后得出一些结论。     

接地故障保护的设置和整定(三)

7 TT系统接地故障保护 TT系统的电源中性点直接接地,而电气设备的外露可导电部分则经各自的PE线接地。这样在大多数情况下,由于故障回路包括两个接地电阻,使接地故障电流太小,不足以使过电流保护动作切断接地故障电流。而且由于故障电流小,故障点未被熔焊,故障点阻抗是难以估计的接触电阻。因此,TT系统接地故障回路阻抗和故障电流难以估算。所以,必须设置漏电电流动作保护。     

一种有机硫类絮凝剂DTC的合成及性能评价

讨论了由有机伯胺或仲胺和CS2合成二硫代氨基甲酸盐DTC的反应及副反应,简介了合成工艺。根据红外光谱确认了由三乙烯四胺合成的二硫代氨基甲酸盐（以下简称DTC）的结构。以含原油350 mg/L、含悬浮固体55.1 mg/L,含Fe^2＋10.0 mg/L的模拟污水为实验水样,考察了该DTC的絮凝性能,在40℃、pH=6-7、沉降时间30分钟条件下DTC的适宜加量为20 mg/L,此时污水含油量为9.0 mg/L;使用DTC的适宜pH范围在4-8,pH=6为最佳值,适宜温度范围为10-45℃,温度高于45℃时DTC可发生热分解;DTC的除油效果随污水中Fe^2＋浓度增大而改善。在含油89.1 mg/L、含悬浮固体55.1 mg/L、含Fe^2＋13.2 mg/L的油田污水中,DTC的除油率最高,远高于常用絮凝剂PFS,PAC,CPAM,HPAM和PAM。当污水中不含Fe^2＋时,DTC无絮凝除油效果。讨论了DTC在Fe^2＋参与下的絮凝过程。图5表1参8。     

TBM地区低孔渗高产气储层预测

 本文从TBM地区目的层的地质和地球物理特征分析出发，以三维地震资料为基础，综合利用人工和神经网络波形分类等定性储层预测方法和利用反演及敏感地震属性分析，对TBM地区低孔渗砂岩分布区开展了砂体展布特征分析和天然气高产区预测研究。根据研究结果部署了10口钻井，已完钻的4口井中有3口获得高产气流（其中DK27井日产天然气36.8×10⁴m³）。值得指出的是，目前所用的预测方法还不能预测厚度小于6m的单砂层或砂层组构成的储层。     

Orign软件在分析化学实验中数据库的建立及应用

介绍了利用Orign7.0在分析化学实验数据处理中的优势,建立分析化学实验的数据库,绘制学生实验的质量控制图,对学生的实验进行有效的监控;对异常数据进行合理的取舍;核实学生实验结果进行形成性评价。累积存储教学资料,提高实验效率和实验教学质量。     

Experimental Study on the Effect of Steel-fibre in Conerete Thick Cap

The effect of steel fibre used in concrete was systematically analyzed by model testing of 30 2-pile thick caps of steel-fibre reinforced concrete, in which the model scale was 1：5. The experiment system composed of a loading device, strain measurement system and a data-acquisition system was used, also an electromechanic centigrade scale, a lens and a Y J-25 static resistance strainometer were used.The experimental results show that the volumetric rate of steel fibre and draw ratio have an important influence on its load-bearing capacity. The incorporation of steel fibre can effectively improve the extension and reduce the thickness of the caps.     

国外大型调水工程渠道运行控制综述

与常规的以经验为主的运行方式相比，考虑了水动力学影响、以多渠池串联的整个渠道系统为研究对象的渠道运行控制在增加调水工程的安全性、降低运行成本、提高输水效率等方面能取得更佳的效果。国外关于调水工程渠道控制的研究起步较早，基于非线性偏微分圣维南方程组发展了多种离散化、线性化等简化方法，建立了相应的控制模型，并从不同角度确定了其控制方法以及控制算法。参考已有的研究思路和方法，总结国外渠道运行控制的成果，对我国南水北调工程的运行控制有着重要的借鉴意义。     

高密度澄清池在邯钢第二污水处理厂的应用

高密度澄清池是一种新型高效的澄清池。介绍了高密度澄清池的工艺原理、运行条件和主要参数及在邯钢第二污水处理厂的应用情况。