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71.
Riedl T Gemming T Mickel C Eymann K Kirchner A Kieback B 《Microscopy research and technique》2012,75(6):711-719
This article explores the achievable transmission electron microscopy specimen thickness and quality by using three different preparation methods in the case of a high-strength nanocrystalline Cu-Nb powder alloy. Low specimen thickness is essential for spatially resolved analyses of the grains in nanocrystalline materials. We have found that single-sided as well as double-sided low-angle Ar ion milling of the Cu-Nb powders embedded into epoxy resin produced wedge-shaped particles of very low thickness (<10 nm) near the edge. By means of a modified focused ion beam lift-out technique generating holes in the lamella interior large micrometer-sized electron-transparent regions were obtained. However, this lamella displayed a higher thickness at the rim of ≥30 nm. Limiting factors for the observed thicknesses are discussed including ion damage depths, backscattering, and surface roughness, which depend on ion type, energy, current density, and specimen motion. Finally, sections cut by ultramicrotomy at low stroke rate and low set thickness offered vast, several tens of square micrometers uniformly thin regions of ~10-nm minimum thickness. As major drawbacks, we have detected a thin coating on the sections consisting of epoxy deployed as the embedding material and considerable nanoscale thickness variations. 相似文献
72.
Sudip Misra P. Venkata Krishna Akhil Bhiwal Amardeep Singh Chawla Bernd E. Wolfinger Changhoon Lee 《The Journal of supercomputing》2012,62(1):4-23
Reliable routing of packets in a Mobile Ad Hoc Network (MANET) has always been a major concern. The open medium and the susceptibility of the nodes of being fault-prone make the design of protocols for these networks a challenging task. The faults in these networks, which occur either due to the failure of nodes or due to reorganization, can eventuate to packet loss. Such losses degrade the performance of the routing protocols running on them. In this paper, we propose a routing algorithm, named as learning automata based fault-tolerant routing algorithm (LAFTRA), which is capable of routing in the presence of faulty nodes in MANETs using multipath routing. We have used the theory of Learning Automata (LA) for optimizing the selection of paths, reducing the overhead in the network, and for learning about the faulty nodes present in the network. The proposed algorithm can be juxtaposed to any existing routing protocol in a MANET. The results of simulation of our protocol using network simulator 2 (ns-2) shows the increase in packet delivery ratio and decrease in overhead compared to the existing protocols. The proposed protocol gains an edge over FTAR, E2FT by nearly 2% and by more than 10% when compared with AODV in terms of packet delivery ratio with nearly 30% faulty nodes in the network. The overhead generated by our protocol is lesser by 1% as compared to FTAR and by nearly 17% as compared to E2FT when there are nearly 30% faulty nodes. 相似文献
73.
Bernd Altmayer Klaus W. Eichhorn und Roland Plapp 《Zeitschrift für Lebensmitteluntersuchung und -Forschung A》1982,175(3):172-174
Zusammenfassung Traubenmoste aus dem Weinanbaugebiet der Rheinpfalz wurden auf ihren Patulingehalt untersucht. Nach Extraktion und Reinigung wurde Patulin mit Hilfe der Hochleistungsflilssig- und Dünnschichtchromatographie bestimmt. Zur Extraktion des Patulins erwies sich die Verwendung von Extrelutsdulen als vorteilhaft. In 62% der untersuchten Proben (55) war kein Patulin nachweisbar, 22% enthielten weniger als 50 g, 16% mehr als 50 g Patulin pro Liter. Durch praxisübliche Mostschwefelung (100 mg Kaliumpyrosulîit/1) und Vergärung mit Hefen der GattungSaccharomyces konnte vorhandenes Patulin entfernt werden.
Analysis of patulin in grape juices and wine
Summary Grape juices from the wine-growing region of the palatinate Rheinpfalz were analysed for patulin. After extraction and purification patulin was determined by high performance liquid chromatography and thin layer chromatography. The use of Extrelut-columns for the extraction of patulin was found advantageous. 62% of the analysed samples (55) were free of patulin, 22% contained less than 50 g/l, 16% more than 50 g/l. By addition of sulfur dioxide to the must and fermentation withSaccharomyces sp. patulin could be removed from the samples.相似文献
74.
Andreas Heinrich Andreas L. Hrner Achim Wixforth Bernd Stritzker 《Thin solid films》2006,510(1-2):77-81
Surface Acoustic Waves on piezoelectric substrates can be used to investigate the dynamic conductivity of thin films in a non-contact and very sensitive way, especially at low conductivities. Here, we report on such surface acoustic wave studies to characterize thin manganite film like La0.67Ca0.33MnO3, exhibiting a Jan Teller effect with a strong electron phonon interaction and a metal insulator transition at high temperatures.
We report on the deposition of La0.67Ca0.33MnO3 on piezoelectric substrates (LiNbO3 in different crystal cuts, employing a pulsed laser deposition technique. The structural quality of the thin films are examined by X-Ray Diffraction, Scanning Electron Microscope and Energy Dispersive X-ray spectroscopy. For the electrical characterization, we employ the surface acoustic wave technique, accompanied by conventional direct current resistance measurements for comparison. 相似文献
75.
Nicole Altvater-Mackensen Gregor Balicki Lucie Bestakowa Bianca Bocatius Johannes Braun Lars Brehmer Verena Brune Kirstina Eigemeier F&#;sun Erdem Ralf Fritscher Anne Jacobs Bernd Klingsporn Marcin Kosinski Julia Kuntze Ju-Ra Lee Anna Osterhage Martin Probost Thorsten Risch Tobias Schmitt Wolfgang G. Stock Anja Sturm Katrin Weller Kerstin Werner 《Scientometrics》2005,63(3):463-529
Summary We operationalize scientific output in a region by means of the number of articles (as in the SciSearch database) per year and technology output by means of the number of patent applications (as in the database of the European Patent Office) per priority year. All informetric analyses were done using the DIALOG online-system. The main research questions are the following: Which scientific and technological fields or topics are most influent within a region and which institutions or companies are mainly publishing articles or holding patents? Do the distributions of regional science and technology fields and of publishing institutions follow the well-known informetric function? Are there - as it is expected - only few fields and few institutions which dominate the region? Is there a connection between the economic power of a region and the regional publication and patent output? Examples studied in detail are seven German regions: Aachen, Düsseldorf, Hamburg, Köln (Cologne), Leipzig - Halle - Dessau, München (Munich), and Stuttgart. Three different indicators were used, science and technology attraction of a region (number of scientific articles and patents), science and technology intensity (articles and patents per 1,000 inhabitants), and science and technology density (articles and patents per 1 billion EURO gross value added). Top region concerning both attraction and intensity is Munich, concerning density it is Aachen. 相似文献
76.
Andrzej Dziech Przemysław Ślusarczyk Bernd Tibken 《Journal of Intelligent and Robotic Systems》2004,39(4):447-458
In this paper an image data compression scheme based on Periodic Haar Piecewise-Linear (PHL) transform and quantization tables is proposed. Effectiveness of the compression for different classes of images is evaluated. The comparison of the compression quality using PHL and DCT transforms is given. 相似文献
77.
78.
Fachjournalist Bernd Niebuhr Dipl.‐Ing. 《Mauerwerk》2009,13(6):363-363
79.
Bernd Maienschein 《现代制造》2022,(2):42-43
<正>“Halle 2020”是Frankenthal市水泵和阀门生产厂KSB公司的一个扩建项目。这一项目不仅仅增加了KSB公司的生产面积,而且也扩展了KSB公司物流中心高架立体库的现代化和存储能力。Viastore公司收到了重建工厂的合同。 相似文献
80.