Development of a Wear Test Apparatus for Screening Bearing-Flange Materials in Computer Tape Drives

An accelerated-wear test apparatus was developed to screen bearing-flange materials. During the test, tape edges rub against two flat test specimens (which are easy to fabricate). The clamping arrangement of the specimens provides the same contact with the tape during repeated tests. The tape is loaded against the sample by deadweight loading, which ensures constant loading, irrespective of tape guiding. Acceleration in wear is obtained by increasing the load at the interface of the tape and the test specimen. Wear tests were conducted on several metals, ceramics and cermets, coatings, and surface treatments. We find that ceramics and cermets have the lowest wear.     

Metal Core Recession and Head Stain Studies of MIG Heads Sliding against Cobalt-Doped Gamma Iron Oxide and Metal Particle Tapes

Metal-in-gap (MIG) heads are commonly used for high-density magnetic recording. Metal core recession and head stains increase the gap between the tape and the head, resulting in signal loss. In this study, accelerated sliding wear tests of Co-γFe₂O₃, and metal particle (MP) tapes against MIC heads made of three different amorphous and, nanocrystalline metals were conducted under various operating conditions. Metal core recess and propensity for head staining were measured. The degree of tape contact with a recessed core was also measured by pressing the tape against a glass slide with Cr grids and using an optical interference technique. The authors found that the core recess was about the same for all three core metals. Core recess by MP tape was larger than that, by oxide tape. The tape speed appeared to have little effect on the recess value. The authors also found that significant recess may occur during initial contouring of the head surface; however, after sliding for about 250 km, core recess reaches a steady-stale value which may be either higher or lower than the initial values. The mechanism of core recession was studied. The authors believe that core recession occurs as a consequence of the debris trapped, between the tape and the core, in addition to that caused by some tape contact. Formation of head stains was observed in all combinations. The stains fanned on the metal cores were heaviest for CoNbZr metal, followed by CoTaZr and FeTaC. Co-γFe₂O₃ tape produced a more severe stain than the MP tape. The apparent roughening of head rubbing surface observed for CoNbZr heads sliding against Co-γFe₂O₃, tape was due to the formation of stains.     

Electro-optical studies in chemically deposited La/Nd doped (Cd-Pb) S films

Results of photoluminescence emission spectra, photoluminescence decay, and temperature dependence of photoluminescence brightness of chemically deposited La- and Nd-doped films are reported. Along with these results of photoconductivity, X-ray diffraction, and SEM studies are also presented and discussed.     

Proteomics analysis of carbon-starved Mycobacterium smegmatis: induction of Dps-like protein

Mycobacterium tuberculosis is a globally successful pathogen,infecting more than one third of total world's population. Thesebacteria have the remarkable ability to persist in the hostfor long periods of time unrecognized by the immune system andthen to re-emerge later in life causing the disease. The physiologyof such persistent or dormant bacilli is not very well characterized.Some evidence suggests that the dormant bacilli survive in anutrient-deprived state that is similar to the stationary phaseof the bacteria with respect to gene expression and physiology.Under this assumption we have studied the survival of Mycobacteriumsmegmatis in carbon starvation conditions as a model for mycobacterialpersistence. M.smegmatis, being a fast-growing strain, servesas a good model to study starvation responses. Using the two-dimensionalelectrophoresis-based proteomics approach, we identified a proteinwhich was found to be expressed preferentially under starvationconditions. This protein is homologous to a family of proteinscalled Dps (DNA binding Protein from Starved cells) that areknown to protect DNA under various kinds of environmental stressesand its existence has, so far, not been reported in mycobacteria.Upon expression and purification of this protein, we observedthat it has non-specific DNA-binding ability. Formation of acage-like dodecamer structure is a characteristic feature ofDps. Using comparative modelling we were able to show that Dpsfrom M.smegmatis could form a dodecamer structure similar tothe crystal structure of Dps from Escherichia coli.     

Dielectric films for Si solar cell applications

Thin films of many dielectric materials have been used in the past for fabrication of solar cells and as a part of their device structure. However, current efforts to reduce solar cell costs in commercial production have led to simplification of cell design and fabrication. Use of self-aligning techniques has obviated the need for photolithography and conventional masking with dielectric films for cell fabrication. Currently, the most favored dielectric material in Si solar cell production is SiN:H, deposited by the plasma-enhanced chemical vapor deposition (PECVD) process. The SiN:H layer and its processing play multiple roles of serving as an antireflection coating, a surface passivating layer, a buffer layer through which metal is fired, and a means of transporting hydrogen into the bulk of the solar cell. In order to optimize the solar cell performance, the SiN:H layer must meet some conflicting demands. The various applications of the SiN:H layer in solar cell fabrication are described here.     

On the influence of environment gases, relative humidity and gas purification on dielectric charging/discharging processes in electrostatically driven MEMS/NEMS devices

In this paper, we investigate the impact of environment gases and relative humidity on dielectric charging phenomenon in electrostatically actuated micro- and nano-electromechanical systems (MEMS and NEMS). The research is based on surface potential measurements using Kelvin probe force microscopy (KPFM). Plasma-enhanced chemical vapor deposition (PECVD) silicon nitride films were investigated in view of applications in electrostatic capacitive RF MEMS switches. Charges were injected through the atomic force microscope (AFM) tip, and the induced surface potential was measured using KPFM. Experiments have been performed in air and in nitrogen environments, both under different relative humidity levels ranging from 0.02% to 40%. The impact of oxygen gas and hydrocarbon contaminants has been studied for the first time by using different gas purifiers in both air and nitrogen lines. Voltage pulses with different bias amplitudes have been applied during the charge injection step under all investigated environmental conditions in order to investigate the effect of bias amplitude. The investigation reveals a deeper understanding of charging and discharging processes and could further lead to improved operating environment conditions in order to minimize the dielectric charging. Finally, the nanoscale KPFM results obtained in this study show a good correlation with the device level measurements for capacitive MEMS switches reported in the literature.     

Compressive deformation behavior of Al 2024 alloy using 2D and 4D processing maps

The hot deformation behavior of Al 2024 was studied by isothermal hot compression tests in the temperature range of 250–500 °C and strain rate range of 10⁻³ to 10² s⁻¹ in a computer-controlled 50 kN servo-hydraulic universal testing machine (UTM). The results show that the flow stress of Al 2024 alloy increases with strain rate and decreases after a peak value, indicating dynamic recovery and recrystallization. The processing map exhibits two domains of optimum efficiency for hot deformation at different strains, including the low strain rate domain at 500 °C and between 10⁻² and 10⁻¹ s⁻¹ and the high strain rate domain in 250 and 300 °C in the strain rate range of 10¹ to 10² s⁻¹. An attempt has been made in this article to generate a new hybrid 4D process map which illustrates contours of power dissipation and instability in the 3D space of strain rate, temperature, and strain.     

Metallurgical re-examination of wear modes I: erosive,electrical arcing and fretting

Solid particle erosion, electrical-arc-induced wear, fretting corrosion and fretting wear modes were studied. Scanning electron microscope examinations generally show significant differences in the different wear modes. Further scanning and transmission electron microscope examinations of the cross sections of worn samples show very little, if any, plastic deformation near the worn surfaces. Microhardness measurements on the cross section of arced samples show an increase of about 25% near the worn surface. Surface analysis of fretting and fretting corrosion wear samples show the existence of an adherent layer that is heavily oxidized in most cases. The source of the adherent layer can be either of the two mating surfaces. It was also found that the same surface may undergo both loss of the original surface layer and gain of an adherent layer. The metallurgical techniques described in this paper can be successfully used to diagnose the wear of solid surfaces.     

Gray-box identification of dynamic models for the bleaching operation in a pulp mill

The development and application of gray-box identification techniques for modelling the bleaching operation in a Bleached Chemi-Thermo Mechanical Pulp (BCTMP) mill are explained. The process is characterized as a delay dominant recycle process with significant input nonlinearities. The identification was carried out using routine operating data in which the outputs were measured irregularly. The effects of these characteristics and consequent modifications of the system identification techniques are discussed. The resulting models are being used for online prediction and model-based controller design at the mill with satisfactory performance.