壳聚糖和粉煤灰对间甲酚的吸附处理

用壳聚糖和粉煤灰对含间甲酚的废水进行吸附处理,考察了壳聚糖的用量、振荡时间、振荡速度以及粉煤灰与壳聚糖的混合比对处理效果的影响.结果表明:在常温下,对于初始质量浓度为56 mg/L的间甲酚,当壳聚糖用量为3 g/L,以170 r/min的转速吸附振荡0.5 h,去除率可达到88%以上;在上述条件下,加入质量比4:1的粉煤灰与壳聚糖混合物5g/L时,间甲酚的去除率可达到91%.     

川东石炭系气藏排水采气工艺技术及其应用

四川盆地东部石炭系气藏是中国石油西南油气田公司的主力气藏之一，经过20多年的开发，出水气井增多、开发难度加大，必须进行排水采气才能维持正常生产。由于石炭系气藏大部分生产井存在井深、地层压力系数低、温度高、静液面深、复产后井口套压高的特点，常规排水采气工艺不能满足气藏的要求。针对这些难点，研究出深井高压气举、低压深井的优选管柱、深井高温泡排三项适合石炭系气藏的排水采气工艺，并在现场十多口井上进行了试验，增产效果显著。     

On the behavior of microstructures with multiple length scales

The current study aims to provide fundamental insight into the behavior of microstructures containing grain sizes that span multiple length scales. A commercial 5083 Al alloy was selected as the material of interest to facilitate comparison with recently published data. The materials studied here were prepared via the thermal consolidation of powders that were cryomilled for different times (i.e., 0, 2, 4, and 8 hours). Following consolidation, the resultant microstructure was characterized by an equiaxed grain morphology with a size distribution centered around 200∼300 nm. Dispersed among the 200- to 300-nm grains were coarse-grained regions or ligaments with a grain size ranging from 600 nm to 2 μm. The occurrence of coarse-grained regions is rationalized on the basis of recrystallization or subgrain coarsening, whereas the occurrence of equiaxed fine regions is proposed to be a result of continuous grain growth. Two types of microstructures were selected for study, containing coarse-grained volumes of approximately 28 pct and 43 pct that corresponded to an ultimate tensile strength (UTS) of 566 MPa and 535 MPa, and a fracture strain of 3.2 pct and 3.5 pct, respectively. The observed ductility and the relevant toughening mechanisms were discussed in light of the presence of multiple length scales.     

Mechanical properties of iron processed by severe plastic deformation

In the present study, the mechanical properties of Fe processed via severe plastic deformation (equal-channel angular pressing (ECAP)) at room temperature were investigated for the first time. The grain size of annealed Fe, with an initial grain size of about 200 μm, was reduced drastically during ECAP. After eight passes, the grain size reaches 200 to 400 nm, as documented by means of transmission electron microscopy (TEM). The value of microhardness during pressing increases 3 times over that of the starting material after the first pass and increases slightly during subsequent pressing for higher-purity Fe. Examination of the value of microhardness after eight passes as a function of post-ECAP annealing temperature shows a transition from recovery to recrystallization, an observation that resembles the behavior reported for heavily deformed metals and alloys. The tensile and compression behaviors were examined. In tension, a drop in the engineering stress-engineering strain curve beyond maximum load was observed both in the annealed Fe and the ECAP Fe. This drop is related to the neck deformation. The fracture surface, examined by scanning electron microscopy (SEM), shows vein patterns, which is different from the dimples found on the fracture surface of annealed Fe. In compression, an initial strain-hardening region followed by a no-strain-hardening region was observed in the ECAP Fe. The yield strength in tension of the ECAP Fe was observed to be higher than that in compression. The strengthening mechanisms and softening behavior are discussed.     

长庆油田苏平1井固井技术研究与应用

苏平l井完井方式运用了技术套管一次上返、悬挂尾管和筛管技术。该井技术套管段井眼大、裸眼段长，加上大斜度、小间隙的尾管段．对水泥浆体系的性能要求较高。总结分析了长庆天然气水平井苏平l井的固井技术问题，介绍了苏平l井的井身结构与地层性质。通过研究．确定采用低失水GSJ水泥浆体系。该体系成功地应用在三次工程建井过程中，解决了长裸眼、大灰量、大斜度、尾管小间隙等固井技术问题。固井质量达到工程要求。     

酚醛树脂复合板在热连轧机中的应用

重点分析了现有F7机架出口导卫装置的情况。原导卫材料是由铸钢制造 ,由于摩擦和高温常常引起热连轧带钢表面划伤 ,根据现场实际情况用酚醛树脂复合板替代铸钢导卫装置。实践表明 ,这种改造即可行又可靠 ,并取得了好的效果     

PRO——一种新的地震资料处理方法

PRO(影像的参数展开)技术是由俄罗斯地球物理学家开发的一种崭新的地震资料处理技术。本文从PRO基本原理入手,简单介绍了PRO的速度分析原理。PRO速度分析和成像均以信号的椭圆展开和参数展开为基础,其中参数展开方法考虑波型转换、介质的横向不均匀造成传播速度的变化。该技术抛开了传统共中心点叠加的思想,从根本上解决了以CMP方法为基础的传统地震处理技术遇到的困难。通过模型与实例分析对比,PRO比传统CMP方法更优越。     

乙烯-1-辛烯共聚物增韧应用研究

介绍了聚烯烃系弹性体（POE）的特点及其在PP增韧改性中的应用，同时还报道了马来酸酐接枝的POE在极性聚合物复合体系中的应用研究。     

Lipase‐catalyzed dynamic kinetic resolution of (R,S)‐fenoprofen thioester in isooctane

A lipase‐catalyzed enantioselective hydrolysis process under in situ racemization of the remaining (R)‐thioetser substrate with trioctylamine as the catalyst was developed for the production of (S)‐fenoprofen from (R,S)‐fenoprofen 2,2,2‐trifluoroethyl thioester in isooctane. Detailed investigations of trioctylamine concentration on the enzyme activation and the kinetic behavior of the thioester in racemization and enzymatic reactions were conducted, in which good agreement between the experimental data and theoretical results was observed. © 2002 Society of Chemical Industry