活化铁矿粉技术及其效果评价

随勘探技术发展,高压超高压油气井日益增多,高密度、超高密度钻井液使用也越来越多.室内为配制密度大干2.4 g/cm3的超高密度钻井液,采用铁矿粉作为加重剂,并通过表面活化的原理对铁矿粉进行表面处理,以提高钻井液的固相容纳能力.该活化工艺借鉴了国内外相关产品的技术特点,以优选的表面活性剂为主要活化材料,并添加了无机盐和硅酸盐作为助吸附材料,提高了活化效果.室内实验表明,用活化铁矿粉加重的钻井液体系能保持良好的流变性和悬浮能力,能保证钻进时的正常循环,并且摩阻系数也低于常规铁矿粉加重钻井液.     

氟碳铈矿／直氟碳钙铈矿混层结构中新规则混层矿物的超微结构研究

用电子衍射和晶格像技术研究了钙稀土氟碳酸盐矿物中的氟碳铈矿（Ｂ）／直氟碳钙铈矿（Ｓ）混层结构，发现并确定了Ｂ＿４Ｓ＿４、Ｂ＿８Ｓ＿６、Ｂ＿１Ｓ＿６、Ｂ＿７Ｓ＿４和Ｂ＿２Ｓ＿１５种新规则混层矿物的对称性、晶胞参数及理论晶体化学式。根据所获得的高分辨晶格像真实而直观地揭示出该类Ｂ＿ｍＳ＿ｎ（ｍ＞ｎ）型新规则混层矿物的长周期有序堆垛结构特征及变化规律。     

Comparisons of PWM and one-cycle control for power amplifier with multilevel converter

Based on the concepts of cascade multilevel converters and one-cycle technique, comparisons are conducted to characterize the distortion of the pulsewidth modulation (PWM) and one-cycle control methods that were applied to converters. Simulation results for the different control schemes are obtained in PSIM software initially to see the effect of one-cycle control different from that of PWM control. Through the comparisons, the advantages and disadvantages are identified for each method. The one-cycle scheme is better than PWM control in reducing undesirable harmonics and tracing dynamic waveforms. Simulation and experimental results are also provided to verify the conclusions.     

用CPLD实现的高速数字图像存储转发装置

本文叙述了一种利用CPLD器件实现的高速数字图像存储转发装置,它被用于一个数字视频图像传输系统中.该装置的主要功能是将来自于CCD的数字图像数据存入大容量存储器中,并可以对数据进行编码,变换成PCM码输出.由于采用了VHDL语言设计,实现了分立器件难以实现的功能,提高了系统的可靠性,并可以方便地移植到各种CPLD器件中.     

Preparation and characterization of polyurethane microcapsules containing n‐octadecane with styrene‐maleic anhydride as a surfactant by interfacial polycondensation

A series of polyurethane microcapsules containing a phase change material (PCM) of n‐octadecane was successfully synthesized by an interfacial polymerization in aqueous styrene‐maleic anhydride (SMA) dispersion with diethylene triamine (DETA) as a chain extender reacting with toluene‐2,4‐diisocyanate (TDI). The average diameter of microPCMs is in the range of 5–10 μm under the stirring speed of 3000–4000 rpm. Optical and SEM morphologies of microPCMs had ensured that the shell was regularly fabricated with the influence of SMA. FTIR results confirmed that the shell material was polyurethane and the SMA chains associated on core material reacted with TDI forming a part of shell material. The shell thickness was decreasing in the range of 0.31–0.55 μm with the molar ratio of DETA/TDI from 0.84 to 1.35 and the weight of core material increasing from 40 to 80% (wt %). By controlling the weight ratio of PCM as 40, 50, 60, 70, and 80% in microPCMs, it was found using DSC that the T_m and T_c of microPCMs were in the range of 29.8–31.0^oC and 21.1–22.0°C and an obvious phase change had been achieved nearly the same temperature range of that of PCM. The results from release curves of microPCM samples prepared by 1.4, 1.7, and 2.0 g of SMA indicated the release properties were affected by the amount of the dispersant, which attributed to the emulsion effect and shell polymerization structure. The above results suggest that the shell structure of microPCMs can be controlled and the properties of microPCMs determined by shell will perform proper practical usage. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102: 4996–5006, 2006     

YAG：Ce Phosphors for WLED via Nano-Pesudoboehmite Sol-Gel Route

The sub-micron sized YAG ： Ce phosphors were synthesized via a modified sol-gel method by peptizing nano-pesudoboehmite particulate. It is found that YAG phase from the dried gel powders appears at 1000 ℃ then the pure YAG phase exists at a relatively lower sintering temperature of 1400 ℃. The smaller sizes of phosphors in the ranges of 1 - 3 μm are obtained due to the contribution of seeding effects of nano-sized alumina particles to strengthen each step of the processes. Both the excitation and emission spectra of photoluminescence of the phosphor obtained at 1400 ℃ meet well with the spectroscopic requirements of the WLED phosphors.     

TCA785移相控制芯片应用方法的改进

TCA785是德国西门子公司生产的一种性能优秀的移相控制芯片 ,该器件具有温度适应范围宽 ,对过零点的识别更加可靠 ,输出脉冲的整齐度更好 ,移相范围更宽等优点 ,此外 ,由于TCA785的输出脉冲宽度可以手动自由调节 ,因此 ,该器件可广泛应用在晶闸管控制系统中。文章根据TCA785芯片的使用特点以及在逆变器实际运用中可能出现的一些问题 ,提出了一种改进的设计方法     

微波等离子体化学气相沉积的 a-Si∶H 性能研究

本文着重对微波等离子体化学气相沉积法高速沉积的 a-Si∶H 膜的物理性能进行评价研究.测量了沉积膜的光电性能、暗电导激活能、光禁带宽度、光吸收特性、沉积膜中悬键态密度以及氢含量等,并讨论沉积条件对膜性能的影响.结果表明,在沉积速率高达30～90(?)/s 情况下,膜的光电导(光照强度10~5Lux)与暗电导比值可达10~3～10~5,暗电导率从10~(-3)到10~(-11)((?)cm)~(-1),其激活能在0.23～0.88eV 之间(0～200℃温度范围内),光禁带宽度为1.40～2.20eV,氢含量约为2～20%.     

Improved coupled-mode theory for nonlinear directional couplers

An improved coupled-mode equation for nonlinear directional couplers (NLDC) with Kerr-like nonlinear media is proposed. The method is based on the generalized reciprocity relation in which two sets of field solutions satisfying Maxwell's equations are for the NLDC and for the isolated nonlinear waveguide. That leads to a reasonable result that all the coefficients in the coupled-mode equations, including the coupling coefficient, become power dependent. For the NLDC with a self-focusing or self-defocusing nonlinear material, the authors examine how the coupling coefficient, the coupling length, and the guided power depend on the input power in the range of coupling stronger than in previous reports. It is found that the critical power at which the coupling length becomes infinity does not increase as much with the two guides for the case of self-focusing media     

用MAXScript脚本语言生成分形图形

介绍了分形生成技术的原理与性质、MAXScript脚本语言的特点及功能，详细叙述了用MAXScript脚本语言生成分形图形的设计思想和实现方法。针对分形几何的特点，以具有严格自相似性的分形树为例，通过解释源代码、描述程序运行过程和结果，以及对生成的图片用3DSMAX进行再处理，分析了在3DSMAX环境中用MAXScript脚本语言生成分形图形这一新方法的优点和不足。