乙环唑的合成研究

介绍了以2,4-二氯苯乙酮为原料通过催化溴化、缩合反应、与三氮唑钠反应制得原药,原药含量达到92%以上.并对合成条件进行了研究,取得了较为满意的结果.     

庙宇平坝防洪治理方案研究

庙宇平坝地处大溪河右岸支流庙宇沟上游山间盆地内,仅靠一条人工开凿的排洪洞和天然消坑排泄洪水,过流能力不足致使每年都遭受洪涝灾害。根据庙宇平坝地形条件及防洪现状,复核现有排洪设施泄流能力,分析存在的问题,结合庙宇平坝地形条件及区内实际情况,采取整个消水洞的扩建及进口前100 m的河道支护,从而提高泄洪能力,降低庙宇平坝水位,有效减少洪水淹没历时及淹没深度。     

电石渣在环氧丙烷生产中的循环利用

总结了电石渣生产环氧丙烷工艺中的设计与应用。运行情况表明，该工艺具有明显的经济效益和社会效益。     

粉末材料合成金刚石中工艺参数的选取

合理地选取工艺参数,有利于合成优质金刚石.文章综述了粉末材料合成金刚石中工艺参数对合成效果的影响以及粉末材料合成金刚石中工艺参数的选取原则.     

New polyimide–silica organic–inorganic hybrids

A series of polyimide–silica hybrid films with silica contents up to 30 wt % were successfully prepared by the sol‐gel reaction of tetraethoxysiliane in the presence of poly(amic acid) containing pendent hydroxyl groups. The films were yellow and transparent when the silica content was less than 11 wt %. The chemical structure of the films was characterized by Fourier transform infrared spectroscopy, and the morphology of the films was investigated by scanning electronic microscopy and atomic force microscopy. Thermogravimetric analysis, differential scanning calorimetry, and stress–strain tests were used to measure the performance of the films. The results indicate that the glass‐transition temperatures and decomposition temperatures of the hybrid films increased with increasing silica content, whereas the tensile strength had a maximum with the variety of silica contents. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 88: 2210–2214, 2003     

Seeded Crystallization of Leucite

The leucite crystallization kinetics from a hydrothermally derived precursor seeded with nano-crystalline leucite was investigated by X-ray diffraction and non-isothermal differential thermal analysis. The nano-crystalline leucite was prepared by high-energy milling of high-purity leucite powder and the leucite precursor was prepared by the hydrothermal method of silica sol, aluminum nitrate, and potassium nitrate. After the seeds were introduced, the crystallization temperature of the precursor was lowered by 100°C and the transition phase kalsilite did not appear during the crystallization process. When the seeded precursor was heat treated at 700°C, a small amount of cubic leucite was stabilized to room temperature. The seeded precursor showed an exothermic peak between 800° and 920°C under different heating rates. The activation energy for the growth of leucite from the seeded precursor was 256(SD9) kJ/mol.     

Decolorisation and mineralisation of CI Reactive Black 8 by the Fenton and ultrasound/Fenton methods

The effects of pH, ferrous ion and hydrogen peroxide dosage on the decolorisation and mineralisation of CI Reactive Black 8 by the Fenton process with/without ultrasonic irradiation were investigated. It was verified that the presence of ultrasonic irradiation did not enhance the decolorisation of CI Reactive Black 8 significantly by Fenton's reagents, but it enhanced the chemical oxygen demand removal efficiency. The enhancement was more pronounced for lower (<0.89 mm) or higher (>1.78 mm) ferrous ion dosage. The optimal pH for chemical oxygen demand removal was 3.0. Chemical oxygen demand removal efficiency increased with the increasing H₂O₂ dosage and reached the highest level at 5.88 mm, but further increase in H₂O₂ dosage would not increase removal efficiency significantly.     

塑料充模流动粘性模型研究

对多种塑料在不同温度下的剪切速率一稳态剪切粘度数据进行Cross粘性模型参数拟合，得到了表征材料粘度的模型参数(B，Tb，τ^*，n)。其拟合效果良好，能较准确地描述塑料熔体在一定剪切速率和温度范围内的粘流特性，为工程计算和塑料熔体模流分析提供了数据支持。结果表明，该方法有较广泛的适用性。     

以人为本的儿童医院候诊设施及服务系统的构建原则初探——以无锡儿童医院输液候诊区为例

旅游发展既促进了江南水乡传统建筑景观的保护,又对其产生了消极影响。旅游的消极影响表现在旅游容量对水乡建筑环境的压力,旅游的商业化、低俗化对建文章从以人为本(HCD)的设计理念出发,结合服务设计中接触点的分析方法,以无锡儿童医院输液候诊区为例,进行服务流程失败点的分析。提出以设计介入儿童医院候诊设施及服务系统构建的四大原则,旨在提升国内儿童医院候诊效率和服务水平,为新医疗服务模式提供案例参考。     

试谈计算机软件测试管理的应用

计算机的软件测试是软件工程构成部分之一,同时软件测试也是检验软件开发人员及软件产品是否合格的重要凭据。就软件测试管理系统活动及应用两个方面的内容进行研究,并对管理工具的存在进行简单的介绍。