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991.
Jun-Bin Ko Sung Wook Lee Dong Eun Kim Young Un Kim Gang Li Seung Goo Lee Tae-Sun Chang Dojin Kim Yong Lak Joo 《Journal of Porous Materials》2006,13(3):325-330
(1 − x)SiO2-(x)ZrO2 (x = 0.1, 0.2) composite fiber mats were prepared by electrospinning their sol-gel precursors of zirconium acetate and tetraethyl
orthosilicate (TEOS) without using a polymer binder. The electrospun composite fibers were characterized by powder X-ray diffraction
(XRD), scanning electron microscopy (SEM), fourier transform infrared spectroscopy (FT-IR) and mercury porosimetry. The composite
fibers having a tetragonal crystalline ZrO2 were obtained by calcining the electrospun composite fibers at high temperatures. The results show that the structure and
crystallization of ZrO2 in the composite fibers can be controlled by sintering temperature, while the porosity and morphology of the fiber mats did
not depend on the sintering temperature. 相似文献
992.
微波辐射磷钨酸催化合成环己酮1,2-丙二醇缩酮 总被引:1,自引:0,他引:1
在微波辐射下,以磷钨酸为催化剂,对以环己酮和1,2-丙二醇为原料合成环己酮1,2-丙二醇缩酮进行了研究.较系统的研究了反应物投料比、微波辐射功率、微波辐射时间、催化剂用量、带水剂用量诸因素对产品收率的影响.最佳反应条件为:环己酮为0.2mol,n(环己酮):n(1,2-丙二醇)=1.0:1.5,微波辐射功率600W,辐射时间16min,催化剂用量为反应物总质量的0.5%,带水剂(环己烷)15mL.在此条件下,环己酮1,2-丙二醇缩酮的产率可达82.0%. 相似文献
993.
Ki-Pung Yoo Hun Yong Shin Min Jeong Noh Seong Sik You 《Korean Journal of Chemical Engineering》1997,14(5):341-346
To design a supercritical fluid extraction process for the separation of bioactive substances from natural products, a quantitative
knowledge of phase equilibria between target biosolutes and solvent is necessary. How-ever, mostly no such information is
available in literature to date. Thus in the present study, illustratively the solubility of bioactive coumarin and its various
derivatives (i.e., hydroxy-, methyl-, and methoxy-derivatives) in supercritical CO2 were measured at 308.15–328.15 K and 10–30 MPa. Also, the pure physical properties such as normal boiling point, critical
constants, acentric factor, molar volume and standard vapor pressure for coumarin and its derivatives were estimated. By these
estimated information, the measured solubilities were quantitatively correlated by an approximate lattice equation of state
proposed recently by the present authors. 相似文献
994.
垃圾焚烧管式布风流化床的冷态实验 总被引:3,自引:1,他引:3
在床截面为300mm×300mm、床高为4. 4m的管式布风流化床实验台上,分别对宽筛分下不同颗粒粒度、不同床层高度、不同截面流速、布风的均匀性以及非平衡布风时颗粒流化特性进行实验研究,为未来垃圾衍生燃料的流化燃烧实验提供基础数据。管式布风流化床的开孔方向与夹角大小对床层压降变化影响明显,向下开孔角度越小,动能消耗越大,但床层稳定性能好。随着料层高度增加,各布风管间的布风更趋于平衡,流化的稳定与均匀性能也越好。管组压降失衡时,床层压降不平衡明显增加,波动幅度增大,不稳定性明显高于正常流化状态。 相似文献
995.
996.
997.
Copolythiophenes (Co‐PTs), poly(3‐hexylthiophene‐co‐3‐thiophene carboxylic acid) (P3HT‐TCa), poly(3‐hexyloxylthiophene‐co‐3‐thiophene carboxylic acid) (P3HOT‐TCa), and poly(3‐phenylthiophene‐co‐3‐thiophene carboxylic acid) (P3PhT‐TCa), were synthesized by chemical oxidized polymerization to investigate the effect of copolymerization on the properties of polythiophenes (PTs). Gel permeation chromatography showed that the molecular weight (MW) of Co‐PT was lower than that of homopolythiophene. Fourier transform infrared (FTIR) spectra indicated that the copolymerization was successful between the monomers. The λmax of Co‐PTs gave a “blue shift” in ultraviolet‐visible (UV‐VIS) spectra. Photoluminescence (PL) spectra showed that the PL intensity of Co‐PT became weaker than that of homopolythiophene and the disappearance of PL had been observed in P3HOT‐TCa. The thermal stability of Co‐PT was influenced by the carboxyl for its low decomposition temperature. Furthermore, the copolymerization between multi‐wall carbon nanotube containing thiophene ring (MWNT‐Th) and 3‐hexyloxylthiphene could also take place successfully. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 2007 相似文献
998.
山东东华水泥有限公司是隶属于淄博矿业集团有限责任公司的子公司,东华水泥5000t/d新型干法水泥熟料线是淄矿建设“煤、电、材”产业链的建材板块龙头项目,第一条5000t/d水泥熟料生产线已于2005年2月投产,目前生产稳定,产品质量优良。配套200万吨粉磨站于2005年11月顺利投产。东华公司根据本公司的实际情况,结合国家资源综合利用的产业政策,委托天津水泥工业设计院设计,利用5000t/d水泥熟料生产线的余热配套一座纯低温余热电站(同时对2号5000t/d水泥熟料生产线配套余热电站进行规划)。 相似文献
999.
Haixia Xiang Cuiping Yu Jinchun Gao Shulan Li Yongle Wu Ming Su Yuanan Liu 《国际射频与微波计算机辅助工程杂志》2014,24(3):401-411
This article introduces the concurrent dual‐band digital predistortion (DPD) architecture with only one upconvertion unit, which is suitable for the linearization of wideband power amplifiers (PAs) excited by concurrent dual‐band signals. By extending the conventional dynamic deviation reduction (DDR) model to the concurrent dual‐band mode, we propose two DDR‐based concurrent dual‐band models, the dual‐band DDR (DB‐DDR) model and the simplified dual‐band DDR (SDB‐DDR) model. The performance of these two models is experimentally assessed with two types of wideband PAs (a GaN Class F PA and a GaN Doherty PA) driven by the concurrent dual‐band signal, and compared with the prior two‐dimensional digital predistortion (2D‐DPD) model and the two‐dimensional modified memory polynomial (2D‐MMP) model. The results prove the good DPD performance and low computational complexity of the proposed models. © 2013 Wiley Periodicals, Inc. Int J RF and Microwave CAE 24:401–411, 2014. 相似文献
1000.
Semantic annotation approaches link entities from a knowledge base to mentions of entities in text to provide additional content-related information. Recently increasing use of resources from the Linked Open Data (LOD) Cloud has been made to annotate text documents thanks to the network of machine-understandable, interlinked data. While existing approaches to semantic annotation in the LOD context have been proven to be well performing with the English language, many other languages in general and the Korean language in particular are still underrepresented. We investigate the applicability of existing semantic annotation approaches to the Korean language by adapting two popular approaches in the semantic annotation field and evaluating those approaches on an English-Korean bilingual sense-tagged corpus. Further, general challenges in internationalization of annotation approaches are summarized. 相似文献