SO2-4/ZrO2-SiO2的制备及其催化合成丁酸丁酯

采用分别沉淀/混合沉淀法、改性共沉淀法和以硅溶胶为硅源的共沉淀法制备了SO2-4/ZrO2-SiO2固体超强酸催化剂;考察了沉淀剂及沉淀终点的pH等制备条件对分别沉淀/混合沉淀法制备的SO2-4/ZrO2-SiO2催化剂催化合成丁酸丁酯活性的影响;探索了ZrO2-SiO2的制备方法、反应时间对SO2-4/ZrO2-SiO2催化剂活性的影响.实验结果表明,以硝酸铵为沉淀剂,当沉淀终点的pH为7～8时,采用分别沉淀/混合沉淀法制备的SO2-4/ZrO2-SiO2催化剂的活性较高(酯化率88.7%),但分别沉淀/混合沉淀法制备的ZrO2-SiO2组成不均匀;以硅溶胶为硅源采用共沉淀法制备的SO2-4/ZrO2-SiO2催化剂催化合成丁酸丁酯,在正丁醇0.48 mol、正丁酸0.40 mol、反应时间3 h、不添加任何带水剂的条件下,酯化率高达96.4%,该方法制备的催化剂稳定性和再生性能好,制备成本低.     

Bandpass filters with reconfigurable transmission zeros using varactor-tuned tapped stubs

In this letter, bandpass filters with one or two tunable transmission zeros are proposed. The reconfigurable transmission zeros are implemented through varactors in combination with tapped quarter-wavelength stubs. Based on mixed mode simulations including EM simulation and circuit simulation, the proposed filters were designed and fabricated on low-cost FR4 board. The measurement results verified the design concepts.     

燕皮传统加工工艺中碱液对肉糜特性的影响

燕皮是以猪肉和甘薯粉为原料,手工制成的薄如纸且经煮不烂的传统食品。在传统制作燕皮过程中添加山榉灰配制的碱液是影响肉糜品质的关键步骤。通过测定制作燕皮过程中各工序样品的氮溶解指数、持水性、乳化稳定性、pH值和粘度,利用SDS-PAGE分析样品中的蛋白质组分、利用光学显微镜观察它们的结构变化,证实植物碱液能够提高样品的氮溶解指数、持水性和乳化稳定性并且延迟了肉糜硬化。同时实验证明碳酸碱(Na2CO3或K2CO3)可替代传统工艺中的植物碱,为后续标准化、工业化生产提供可行条件。     

TBM掘进隧洞回填固结灌浆施工的探讨

豆砾石回填灌浆和固结灌浆在引黄工程南干线长达90kmTBM施工中得到成功的应用。文中介绍了引黄工程南干线4^#-7^#隧洞豆砾石回填灌浆、特殊地质洞段的固结灌浆的灌浆设备、材料、浆液配比、压力、工艺等诸方面的现场施工情况。     

粉末涂料在汽车涂装中的应用

介绍了粉末涂料的组成、优越性以及各种性能，分析了粉末涂料在汽车涂装中的经济性，肯定了粉末涂料在汽车工业中的应用前景。     

转炉溅渣护炉改质剂的开发研究

影响转炉溅渣护炉效果的关键因素是终渣成分的控制,采用改质剂对转炉终渣成分进行调整,降低渣中FeO含量和炉渣温度,提高MgO含量和炉渣熔点及粘度,有利于改善炉渣与炉衬的粘结效果,并提高溅渣层的耐蚀性能,缩短溅渣起孕时间,在一定程度上抑制炉渣中铁的氧化物与炉衬中石墨的反应.     

An optical instrumentation using a sensor with a sensordummyagainst noises on sensor and transmission line

This short paper discusses the method of effectively canceling equal status normal mode noise not only on a sensor line but also on a transmission line of an optical instrument using a sensor with a sensordummy resistance     

丙烯腈－苯乙烯共聚物水解磺化产物对泥浆的稳定作用

在实验室条件下对用丙烯腈－苯乙烯共聚物在硫酸存在下的水解磺化产物（ＨＳＡＳ）处理的泥浆性能进行了评定。ＨＳＡＳ处理的泥浆有较小的滤失性，较好的耐盐和抗高温性。     

USERS' TWO-DIMENSIONAL INTEREST AND ITS STORAGE METHOD

The users' interest can be mined from the web cache and can be used widely. The interest can be specialized by the two-tuple (term, weight) in the simple interest model, in which the association relations are not mined, and then the interest cannot be associated in expressing the users' interest. Based on analyzing the WWW cache model, this letter brings forward a two-dimensional interest model and gives the interrelated methods on how to store the two-dimensional interest model effectively.     

游梁式抽油机二次平衡分析

为解决游梁式抽油机能耗大、效率低的问题，设计了二次平衡装置。这种装置通过是挂在抽油机后端的平衡重的平衡作用，降低一次平衡曲柄轴净扭矩的两个峰值，达到减少能耗提高效率的目的。对抽油机的二次平衡作了较详尽的理论分析，给出了实行二次平衡后曲柄轴净扭矩的计算公式和安装二次平衡装置前后曲柄轴净扭矩曲线图。在大庆油田两口井上进行的现场试验结果表明，安装二次平衡装置后，两口井年节约电费分别为0.25万元和1．17万元，经济效益明显。