两相驱动型时栅位移传感器测角系统误差建模与分析

为了进一步拓展时栅位移传感器的应用范围,在传统场式时栅位移传感器测角系统的基础上,提出了一种两相驱动型时栅位移传感器测角系统,该系统以低分辨率、低成本的圆光栅和直接数字频率合成器构成了一种新的“时间行波”,结合传统时栅位移传感器的处理技术,构成一个新的测角系统。对该测角系统的误差模型进行研究,实验结果表明：该测角系统的主要误差成分为光栅信号的不正交、不等幅与残余直流电平三项误差源,通过该误差模型可以有效地减小时栅位移传感器的原始误差、提高了测角系统的测量精度,精度达到±3.2″。     

浅地表层界面折射波走时模拟

在工程与环境勘查中进行折射波法勘探时,其勘探对象通常为浅地表的层界面.由于当层界面起伏时无法得到折射波走时曲线的确切表达式,同时为了了解多个层界面的折射波走时曲线之间的相互影响,基于费马原理和斯奈尔定律实现了浅地表多层起伏界面折射波的走时模拟.利用水平层折射波时距曲线公式验证了编制程序的正确性,并模拟了野外常见地质模型的折射波走时.     

基于两级插补机制的NURBS曲线插补器研究

针对非均匀有理B样条（non-uniform rational B-spline,NURBS）曲线高速高精加工过程中计算负载高的问题,提出一种基于两级插补机制的NURBS曲线插补器方案,在主控端执行第一级插补,完成曲线预处理等粗插补工作;在运动控制端执行第二级插补,完成加减速及实时位置输出等精插补工作。同时,设计并开发基于ARM-FPGA架构的实验平台,可用于两级插补器的实验验证,具有一定的现实参考意义。     

AVO流体反演技术在低孔渗砂岩气藏预测中的应用

西湖凹陷A构造的砂岩气藏,主要埋藏于3000m以下的深层,且发育于浅水沉积环境,储层物性较致密,厚度横向变化大,导致储层的AVO响应复杂,常规AVO分析难以对储层流体进行有效识别。研究了AVO流体反演技术在该构造含气储层预测中的应用。该技术在对储层以及非储层速度、密度、厚度等关键参数的统计分析的基础上,利用Monte－Carlo随机模型建立、地震正演模拟、流体替换等技术,获得储层在不同流体下AVO响应的验前概率;然后利用Bayes理论,估算实际地震数据AVO响应指示储层含某种流体的可能性一验后概率,从而实现储层流体的预测。实际钻探结果证实了该方法的有效性。     

四川盆地海相页岩气富集条件及勘探开发有利区

历经十余年探索实践,四川盆地海相页岩气勘探取得了一系列进展,锁定五峰组—龙马溪组为最有利产层,提出了一批页岩气富集高产理论,形成了集地质评价、开发优化、优快钻井、体积压裂、工厂化作业、清洁开发等为一体的勘探开发技术,探明了万亿立方米级储量的页岩气大气田。时值中国页岩气勘探发展的重要节点,回顾四川盆地海相页岩气勘探开发历程、梳理五峰组—龙马溪组页岩气在地质条件与富集规律上的成果认识、展望四川盆地海相页岩气勘探的重点接替领域,对推进盆地海相页岩气的勘探开发有积极意义。(1)四川盆地海相页岩气勘探开发经历了4个阶段：评层选区找目标阶段;浅层至中—深层先导试验阶段;浅层至中—深层示范区建设阶段;浅层至中—深层上产、深层评价、常压页岩气评价、立体开发评价、超深层和新层系探索阶段。(2)四川盆地五峰组—龙马溪组的沉积条件优越,深水陆棚相高有机质含量页岩呈连续稳定分布;页岩气主要赋存在有机孔隙中,页岩储层在纵向上集中发育,连续厚度大;川南地区和川东南涪陵区块的构造相对简单,气源持续补给、远离古/今剥蚀区和大型断裂逸散区是页岩气富集保存的有利区;目前,五峰组—龙马溪组的页岩气资源量为33.19×10<...     

Reaction behaviors and specific exposed crystal planes manipulation mechanism of TiC nanoparticles

Titanium carbide (TiC) nanoparticles with well-designed exposed crystal planes perform intriguing prospects for functional and engineering applications. In this study, a simple and controllable in situ synthesis strategy was proposed for the synthesis of TiC nanoparticles with specific morphology. Reaction behaviors suggested that most of TiC nanoparticles were formed by an instantaneous reaction between Al₃Ti and Al₄C₃ in the Al-rich melt and the resultant morphology was controlled by the discrepant growing rates of (100) and (111) crystal planes. In addition, a growth morphology control model was presented for the prediction and manipulation of the morphology of TiC nanoparticles by the doping of different alloying elements Me (Me = Cu, Mg, Mn, Zn, and Si). According to the morphological observations and density functional theory analyses including the interface energy, charge density differences, and orbital hybridization: Cu, Mg, and Zn atoms could stabilize the Al/TiC(111) interface, whereas Mn and Si atoms promoted the rapid growing and disappearance of the TiC(111) planes in the Al melt. This work provides a feasible way to intelligently design and manipulate TiC nanoparticles with desirable exposed crystal planes, and exhibits a promising prospect for personalized applications.     

Nondestructive measurements of residual stress in air plasma-sprayed thermal barrier coatings

Premature spallation of thermal barrier coatings (TBCs) is a critical issue during the service of gas turbines, and nondestructive evaluation is crucial to address this problem. Herein, a novel approach that indicates delamination by measuring the residual stress evolution of thermally grown oxide (TGO) for air plasma spraying (APS) TBCs is proposed and verified via the combination of photoluminescence piezo-spectroscopy (PLPS) and X-ray computed tomography. A mineral-oil-impregnating approach and a cold-mount low-shrinkage epoxy-mounting approach are used to alleviate the signal attenuation by pores and microcracks in APS TBCs, improving the detectable PLPS signal and X-ray transmission for stress measurement and delamination characterization, respectively. We have nondestructively measured the TGO residual stress mapping in APS TBCs and its evolution with oxidation. Furthermore, the evolution of TGO morphology and critical microcracks are obtained by X-ray computed tomography. The synchronous evolution of TGO residual stress, TGO thickness, and critical microcracks as a function of oxidation time is obtained and correlated. The transition point, as experimentally identified, at which the TGO stress starts to drop, agrees well with the critical moment of microcrack coalescence. This directly verifies that the TBC delamination can be effectively indicated by residual stress evolution of TGO in APS TBCs.     

Sintering parameter optimization of Tb3Al5O12 magneto-optical ceramics by vacuum sintering and HIP post-treatment

Transparent terbium aluminum garnet (TAG) ceramics were achieved by the vacuum sintering plus HIP post-treating from the coprecipitated TAG nanoparticles. The influences of vacuum sintering temperature and sintering aid TEOS on the optical quality of the TAG ceramics were studied. The results show that with the increase of sintering temperature, the optical quality of TAG ceramics is improved gradually, and the in-line transmittance of the TAG ceramics treated at 1720°C for 20 hours under vacuum and then HIP post-treated at 1700°C for 3 hours under 200 MPa argon gas is 81.6% at 1064 nm. The sintering additive TEOS can improve the optical quality of TAG ceramics and inhibit the valence state change of Tb³⁺ ions to Tb⁴⁺ during the annealing process. The Verdet constant of the TAG ceramics at 632.8 nm is about −178 rad·T⁻¹·m⁻¹ at room temperature, which is 1.3 times that of the commercial TGG crystals (−134 rad·T⁻¹·m⁻¹).     

Enhanced luminescence and thermal stability of (Sr,Ca)AlSiN3:Eu2+ via superficial organic carbon modification

The Eu²⁺-activated nitride phosphors have been widely used in solid-state lighting, but the applications in high-power white-light-emitting diodes (wLEDs) field require higher thermal stability of luminescent materials. The oxidation of Eu²⁺ and the damage of nitride host in the Eu²⁺-activated nitride phosphors are the two crucial reasons for the luminescence loss while operating. A superficial organic carbon modification is performed on the red-emitting (Sr,Ca)AlSiN₃:Eu²⁺ phosphor via the incorporation of organic carbon by solution mixing and thermal post-treatment under the N₂-H₂ atmosphere. After the superficial organic carbon modification, the oxidation of Eu²⁺ and the formation of impurity phases on the phosphor surface are effectively reduced. When the superficial organic carbon modified sample was treated in the 2 wt.% sucrose solutions, the relative brightness is strengthened by 2.15%, the thermal quenching characteristic is improved by 8.9% at 300℃, and the aging test results show an excellent thermal stability. All above indicate that the superficial organic carbon modification is a promising technique to enhance the thermal stability of analogous Eu²⁺-activated nirtide phosphors.     

Electrochemical investigation of La0.4Sr0.6TiO3 synthesized in air for SOFC application

Journal of Applied Electrochemistry - La-doped titanate materials have been widely investigated as alternative Ni-free anodes for solid oxide fuel cells (SOFCs). In this study, La0.4Sr0.6TiO3 (LST)...