Comparison of ablative and compressive mechanical behavior of several PICA-like ablative materials

It is significant to compare the ablative and compressive mechanical behavior of different PICA-like materials in the engineering applications. The plasma wind tunnel ablation tests with high-entropy air and CO_2 atmospheres, and compressive experiments in the ambient and 150℃, were conducted for three kinds of PICA-like materials(CF/PR-Si, CBCF/PR-SiOC and NQF/PR-Si composites). The traditional carbon/phenolic(C/PR) braided composites were also used for comparison. PICA-like materials have the better thermal insulation than traditional C/PR composite, especially for CBCF/PR-SiOC composite. The ablation behavior of CF/PR-Si and CBCF/PR-SiOC PICA-like materials in the CO_2 atmosphere can produce a large amount of SiO_2 in the form of coatings, oxide layers and skeletons on the ablated surface, which are greatly different from that in the air atmosphere.The compressive behavior of PICA-like material is greatly depended on the fiber fabrics, and exhibits the large discrete characteristics. The longer fiber in the PICA-like materials plays the role in maintaining the material integrity, while it may increase the thermal conductivity.     

水雷声引信系统海试考核方法探讨

对水雷声引信系统海上试验的考核方法进行了探讨,重点介绍了战技指标的概念和定义,并针对主要指标要求,分别详细介绍了考核评判标准。     

Effect of Drying on Particle Size and Sensitivities of Nano hexahydro-l,3,5-trinitro-l,3,5-triazine

Nano hexahydro-l,3,5-trinitro-l,3,5-triazine （RDX） was prepared using a bi-directional rotation mill and dried under different conditions （liquid, temperature and drying）. It shows that the samples cake seriously and the particles grow up obviously by ordinary drying in different liquids at 70 ℃, which occurs again after vacuum drying. With the increase of temperature, the degrees of caking and aggregation are enhanced. Well dispersed sample maintaining constant particle size is extracted by supercritical drying, especially freeze drying. Furthermore, the me- chanical sensitivities of I-RDX, O-RDX and F-RDX, of which the average sizes are 88.03 μm, 15.32 μm and 0.16 μm, respectively, are evaluated. Compared with I-RDX, the friction, impact and shock sensitivities of O-RDX are slightly lower. However, the friction, impact and shock sensitivities of F-RDX are reduced by 30%, 99.0% and 59.9%, respectively.     

高原环境对冲压式气动舵机工作特性的影响研究

为了研究高原环境对冲压式气动舵机工作特性的影响,建立了一种冲压式气动舵机的数学模型,并以此为基础进行仿真研究。结果显示气源压力减小会降低舵机振荡线性化精度,输入端控制信号幅值过大会引起舵片饱和,导致舵机控制力不足。分析表明,为保证冲压式舵机在高原环境下的正常使用,需重点关注气源压力和控制信号幅值的变化范围。     

飞机投弹出舱过程自动记录装置

介绍一种飞机投弹出舱过程自动记录装置。该装置没有对飞机的机械接口和电气接口进行任何改变,只需利用飞机现有挂弹架的挂弹钩接口安装设备,通过光敏开关感应光线强弱变化,判断飞机武器舱门是否打开,从而自动触发高速摄像机拍摄,完成飞机投弹出舱过程的记录任务。     

Biocompatible electrospun tactic poly(methyl methacrylate) blend fibers

Uniform and beads free fibers of pristine syndiotactic PMMA (s-PMMA), isotactic PMMA (i-PMMA), and their blends in the ratio of s:i = 3:1, 1:1 and 1:3 were successfully prepared using the electrospinning technique. The tactic PMMA blend fibers showed unique thermal stability and glass transition temperatures compared to their pristine counterparts. An interesting endotherm peak was observed for the s:i = 1:3 electrospun fibers, which might indicate a complex formation between the two tactic PMMAs. Systematic surface functionalities study by attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR) revealed the interactions between these two tactic PMMAs. Biocompatibility of tactic PMMA and their blend fibers was first time comparably investigated using HeLa as the model mammalian cell line; an intriguing observance was first revealed that the blend fibers showed better biocompatibility than both pristine ones, though the behind mechanism is not well understood yet.     

TiB2 Powders Synthesis by Borothermal Reduction in TiO2 Under Vacuum

TiB₂ powders were synthesized by borothermal reduction in nanoscale TiO₂ with boron under vacuum. Reaction processes were investigated, and the effect of by‐product B₂O₃ was evaluated. Results showed that TiO₂ was firstly reduced by boron to form TiBO₃ and Ti₂O₃, and then to produce TiB₂ and B₂O₃ with increasing temperature. The reaction processes of TiB₂ powders synthesis included two‐step reduction in TiO₂ by boron and the removal of B₂O₃. The presence of B₂O₃, which was previously reported as the most important factor in promoting the coarsening of ZrB₂ and HfB₂ powders by borothermal reduction, did not lead to significant coarsening of TiB₂ powders. Due to the minor effect of B₂O₃, TiB₂ powders with small particle size and low oxygen content could be prepared by direct heat treatment of TiO₂ and boron at 1550°C under vacuum for 1 h. The particle size and oxygen content of synthesized TiB₂ powders were ~0.9 μm and ~1.7 wt%, respectively.     

A Decomposition Route for Synthesis of Al2O3 Crystal and its Applications as Thermal Conductivity Filler

Platelike α‐Al₂O₃ powder was obtained at 850°C by thermal decomposition of ammonium aluminum carbonate hydroxide precursor, which was treated by hydrofluoric acid. The results showed the decomposition of the as‐prepared precursors experienced via three steps, adsorption of physical water, dehydration of crystalline water, and decomposition of the precursor, and the activation energies of the above three steps were calculated using the Coats–Redfern method. Meanwhile, the intermediate of (NH₄)₃AlF₆ obtained played an important role in decreasing activation energy of the decomposition and phase transformation. Moreover, the thermal conductivity of the epoxy resin filled with platelike alumina was improved obviously.     

Injury Mechanisms of Lactic Acid Bacteria Starter Cultures During Spray Drying: A Review

Lactic acid bacteria (LAB) starter cultures can be processed by many drying techniques, among which spray drying has great potential. However, injuries of LAB during spray drying lead to a low survival rate. The microbial injuries of LAB during spray drying are specifically induced by dehydration inactivation, thermal inactivation, and balance between the two. To reduce the drying temperature, new drying techniques based on spray drying were tried; that is, low-temperature vacuum–spray drying and spray–freeze drying.