溶胶-凝胶法制备ZAO薄膜研究

研究了用溶胶．凝胶法制备ZAO薄膜的工艺、掺杂及其显微结构。用六水合氯化铝在溶胶中引入Al2O3。掺杂Al的含量为1％，3％，6％和9％。用浸涂法在石英玻璃基片上浸涂ZnAO薄膜，研究了热处理、掺杂对ZAO薄膜相组成和显微结构的影响。X射线衍射结果表明，衍射图谱中无Al2O3的衍射峰。随着掺杂量的变化，ZnO主要衍射峰的位置、晶面间距均发生了有规律的变化，说明Al掺杂进了ZnO晶格中。研究结果表明，溶胶浓度、Al掺杂量、热处理温度都影响薄膜的显微结构。当薄膜厚度较大时，热处理过程中ZnO晶粒呈现明显的择优生长现象。     

Phase equilibrium in binary aqueous mixtures of interest in alcoholic distillation using a modified PSRK equation of state

Phase equilibrium in binary mixtures that are found in wine and must distillation processes have been modeled using the predictive Soave-Redlich-Kwong equation, with original and modified molecular parameters. In wine and must distillation, the presence of polar substances found in the mixture to be distilled and the many components (i.e., those different from ethanol and water), called congeners, makes it difficult to model these mixtures. Thus, the prediction and correlation of the concentration of the distilled product, which is the most interesting variable, become very complex, and some experimental data are needed. The cases studied considered nine binary water + congener mixtures. The congeners considered are acetic acid, acetaldehyde, ethyl acetate, furfural, methanol, 3-methylbutanol, 2-methyl-1-propanol, 1-pentanol, and 1-propanol. These are the substances that are considered to be legal compounds by the Chilean legislation governing the production of a spirit called Pisco. The work allows evaluation of the advantages, disadvantages, and expected accuracy of this model. Comparison with available literature data is done.     

动力学仿真软件在1LB─240型水平摆式犁油缸运动选型中的应用研究

以1LB-240型水平摆式犁中用于犁体换向的油缸设计为例,首先对其在田间的工作状况进行运动学、动力学分析,然后应用机械三维设计软件SolidW orks及内嵌其中的动力学仿真软件DDM对其仿真,找出了犁耕作业过程中油缸的恰当运动方式———匀速运动,为农业机械产品的设计开发提供了一条新的思路。     

Preparation and elements analysis of porous fluorescent glasses

A large variety of porous fluorescent glasses were prepared and the concentration of different elements in these glasses was analyzed. The start porous glasses were soaked in a solution containing soluble salts and then heated at 650 ℃ for 3 h to decompose the salts in the pores into oxides. Fluorescent agents, such as UO3, Eu203, were impregnated into the porous glasses to prepare the fluorescent glasses. The results show that soaking is a feasible method to prepare the glass sphere with compositions distinguishable from each other and easy to be located in a complicated background. Six or more components can be impregnated together into one glass sample and the concentration of them can be analyzed accurately. UO3 and Eu203 can be impregnated into porous glass to make the glass strongly fluorescent. Higher concentration of Eu203 produces stronger fluorescence while higher concentration of UO3 reduces the fluorescence intensity because of the concentration quenching effect.     

现浇框剪结构中若干钢筋构造问题的治理

近年我国钢筋混凝土现浇框架-剪力墙结构中，由于钢筋构造不当，偏差超出规范规定的情况经常发生，影响了结构受力和工程验收。主要问题有：主筋偏位、框架柱接头设计不当、框架纵向钢筋变径频繁、井式梁按主次梁绑扎、梁吊筋绑扎混乱、以膨胀螺栓代替同直径Ⅱ级钢筋等。对此进行治理时，一是设计者要把设计意图交代清楚，施工图有足够深度，节点有大样，交底详细；二是施工人员要熟知结构理论，不断丰富施工经验，具备严谨的施工作风。     

欠平衡钻井中钻具的腐蚀与磨蚀

在对文献调研的基础上，综述了国内外在欠平衡钻井中对金属钻具的腐蚀与磨蚀方面所做的工作，主要包括各种影响因素的分析、相应防腐剂的组成和应用。然后指出在欠平衡钻井中为了更有效的防止钻具腐蚀，在开发新型防腐刺的同时，应根据油田具体实际情况对现有的防腐剂进行复配，筛选出符合自己需要的防腐剂。     

基于功效系数法的采空区稳定性判别方法研究

矿石开采后遗留下的采空区,对矿山而言始终是一种安全隐患,采空区的稳定与否关系到矿山的生产安全.本文根据矿山的实际情况,选取了5个最能充分反映采空区特征的参数作为评价指标,并基于变异系数法的客观性以及功效系数法的简单高效性,提出一种功效系数法采空区稳定性判别模型,并结合数值分析方法对某矿山7个采空区稳定性进行了判别与对比...     

四川大渡河流域偏岩子金矿床地质特征及金的赋存状态

偏岩子金矿床位于康滇地轴北端的大渡河成矿带上,是世界上稀有的氟镁石型金矿床。产于上震旦统灯影组中,矿物的组成比较丰富,已查明的矿物多达50多种。矿石类型以氟镁石-石英型为主,矿体同时受到地层和构造的双重控制。通过电子探针（EPMA）、扫描电镜（SEM）等测试,发现载金矿物以氟镁石、黄铁矿、黝铜矿等矿物为主;按照金的化学状态可将金的赋存状态分为独立矿物、络合物和晶格金这三大类,按照金与载体矿物之间的嵌布关系可分为有包裹金、裂隙金和晶隙金这三大类,金的粒度跨度较大,主要集中在2～10 μm,属于明金、显微金。     

新疆某低品位硫化铅锌矿石选矿试验研究

新疆某低品位铅锌矿石矿物组成简单,同时矿物伴生关系复杂、嵌布粒度不均匀。为有效回收矿石中的铅和锌,采用铅锌优先浮选工艺,通过铅锌浮选条件试验确定适宜的选矿工艺流程及药剂制度。结果表明:针对铅品位1.04%、锌品位1.66%的原矿石,在磨矿细度为-0.074 mm占70%的条件下,采用2次粗选优先选铅、铅粗精矿再磨至-0.038 mm占100%后3次精选,可获得铅品位45.16%、锌品位1.21%的铅精矿;选铅尾矿经CuSO₄活化后,采用“2粗3精”选锌;全流程闭路试验最终可获得铅品位44.16%、铅回收率85.04%的铅精矿,及锌品位43.31%、锌回收率92.45%的锌精矿,较好地实现了铅锌分离回收。研究结果可为同类型矿石的开发利用提供有益参考。     

高强轻集料混凝土桥面施工泵送技术

轻集料混凝土（LWAC）由轻质多孔集料和水泥石胶结而成。在施工过程中，LWAC由于集料多孔的性质，会从水泥浆中吸收水分，造成混凝土坍落的降低，影响混凝土的泵送性能；另外，LWAC的收缩变形比普通混凝土大，更易使混凝土形成裂缝。通过对LWAC高性能化等技术手段，配制出干表观密度小于1950kg/m^3，易于泵送和体积稳定性好的混凝土。使纤维增强泵送高强（CL40）LWAC技术第一次成功地在我国桥梁工程应用。