普钙产品转化率的数值计算方法

对影响普钙产品转化率的各种因素进行了分析,利用MATLAB 软件包得到了转化率的计算公式,提出了确定未分解磷矿的比例和由倍半氧化物引起的有效磷退化幅度的方法,为生产系统的预测和调整提供了一种途径。     

Synthesis and characterization of copolythiophene

Copolythiophenes (Co‐PTs), poly(3‐hexylthiophene‐co‐3‐thiophene carboxylic acid) (P3HT‐TCa), poly(3‐hexyloxylthiophene‐co‐3‐thiophene carboxylic acid) (P3HOT‐TCa), and poly(3‐phenylthiophene‐co‐3‐thiophene carboxylic acid) (P3PhT‐TCa), were synthesized by chemical oxidized polymerization to investigate the effect of copolymerization on the properties of polythiophenes (PTs). Gel permeation chromatography showed that the molecular weight (MW) of Co‐PT was lower than that of homopolythiophene. Fourier transform infrared (FTIR) spectra indicated that the copolymerization was successful between the monomers. The λ_max of Co‐PTs gave a “blue shift” in ultraviolet‐visible (UV‐VIS) spectra. Photoluminescence (PL) spectra showed that the PL intensity of Co‐PT became weaker than that of homopolythiophene and the disappearance of PL had been observed in P3HOT‐TCa. The thermal stability of Co‐PT was influenced by the carboxyl for its low decomposition temperature. Furthermore, the copolymerization between multi‐wall carbon nanotube containing thiophene ring (MWNT‐Th) and 3‐hexyloxylthiphene could also take place successfully. © 2007 Wiley Periodicals, Inc. J Appl Polym Sci 2007     

矾土尖晶石钢包浇注料的研制与应用

采用特级矾土熟料为骨科，天然出合成的镁铝尖晶石为部分基质，选用新型复合结合剂研制成矾土尖晶石质钢包浇注料．使用结果表明：一次性寿命较传统的铝镁浇注料提高８０％以上．     

Inspection of Remanent Polarization in the Ferroelectric Ceramic PZT 95/5 Through Pyroelectric Effect

Shock-induced depoling of the ferroelectric (FE) ceramic PZT 95/5 is utilized in a number of pulsed power devices. Nondestructive testing of remanent polarization of PZT 95/5 is developed by pyroelectric effect in this paper. Approximately linear relation between the change of polarization during low- to high-temperature rhombohedral FE phase and the remanent polarization was found through pyroelectricity of a single piece of PZT 95/5 ceramics. The change of polarization of a prototype for shock-driven pulsed power during the FE_HT↔FE_LT phase transformation was also investigated through directly measuring the pyroelectric current. Results indicate that pyroelectric effect caused by the reversible FE_HT–FE_LT phase transition could be used as a non-destructive inspection for the remanent polarization of a prototype about shock-driven pulsed power supply.     

Thermal and crystallization characteristics of poly(ethylene terephthalate) with poly(oxybenzoate‐p‐trimethylene terephthalate) copolymer

Poly(ethylene terephthalate) (PET) was blended with two different poly(oxybenzoate‐p‐trimethylene terephthalate) copolymers, designated T28 and T64, with the level of copolymer varying from 1 to 15 wt %. All samples were prepared by solution blending in a 60/40 (by weight) phenol/tetrachloroethane solvent at 50°C. The crystallization behavior of the samples was studied by DSC. The results indicate that both T28 and T64 accelerated the crystallization rate of PET in a manner similar to that of a nucleating agent. The acceleration of PET crystallization rate was most pronounced in the PET/T64 blends with a maximum level at 5 wt % of T64. The melting temperatures for the blends are comparable to that of pure PET. The observed changes in crystallization behavior are explained by the effect of the physical state of the copolyester during PET crystallization as well as the amount of copolymer in the blends. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 86: 1599–1606, 2002     

Oxidative dehydrogenation of ethane over Co–BaCO3 catalysts using CO2 as oxidant: effects of Co promoter

Co–BaCO₃ catalysts exhibited high catalytic performance for oxidative dehydrogenation of ethane (ODE) using CO₂ as oxidant. The maximal formation rate of C₂H₄ was 0.264 mmol · min⁻¹ · (g · cat.)⁻¹ (48.0% C₂H₆ conversion, 92.2% C₂H₄ selectivity, 44.3% C₂H₄ yield) on 7 wt% Co–BaCO₃ catalyst at 650 °C and 6000 ml. (g · cat.)⁻¹. h⁻¹. Co–BaCO₃ catalysts were comparatively characterized by XRF, N₂ isotherm adsorption-desorption, XRD, H₂-TPR and LRs. It was found that Co⁴⁺–O species were active sites on these catalysts in ODE with CO₂. The redox cycle of Co–O species played an important role on the catalytic performance of Co–BaCO₃ catalysts. On the other hand, the co-operation of BaCO₃ and BaCoO₃ was considered to be one of possible reasons for the high catalytic activity of these catalysts.     

Solid state interfacial reactions in electrodeposited Ni/Sn couples

Ni/Sn couples,prepared by sequentially electroplating Ni layers and Sn layers on metallized Si wafers,were employed to study the mierostructures and growth kinetics of Ni-Sn intermediate phases,when the Ni/Sn couples were aged at room temperature or annealed at temperatures from 150 to 225℃for various times.The results show that the NiSn phase and Ni_3Sn_4 phase are formed,respectively,in the aged couples and annealed couples.The Ni_3Sn_4 layer is continuously distributed between the Ni and Sn sides in t...     

基于TCN的地铁列车控制方案的研究

本文针对地铁车厢内控制设备分散的问题,设计了基于TCNRTP的地铁列车控制网络系统。采用NS2网络模拟软件构建的虚拟网络环境,编写消息数据传输层协议,通过测试列控网络的通信效率,得出了影响通信效率的因素;通过配置列控通信设备的基本功能和设定装置运行参数达到配置网络化通信的目的。     

实验动物在血液制品中的应用

目的：阐述实验动物在血液制品生产质量控制过程中应用的重要性。方法：按《中华人民共和国药典》2005年版三部要求及相关项目的技术规范进行血液制品质量控制。结果：血浆数量150吨,可同时生产以下品种的产品,人血白蛋白共30批次,总瓶数约40万瓶（折10g）;免疫球蛋白类：共30批次,总瓶数约30万瓶（折2.5g）;人纤维蛋白原：共30批次,总瓶数约15万瓶（折0.5g）;人凝血酶原复合物：共30批次,总瓶数约12万瓶（折300IU）;人凝血因子Ⅷ：共30批次,总瓶数约10万瓶（折200IU）。需使用家兔870只、豚鼠300只小鼠750只。结论：实验动物应用于血液制品生产质量控制发挥了非常重要的作用。     

策应鄱阳湖生态经济区建设 推动吉安进位赶超绿色崛起

建设鄱阳湖生态经济区是国家从战略全局和长远发展出发作出的一项重大决策。如何主动策应鄱阳湖生态经济区建设,推动吉安进位赶超、跨越发展,是摆在我们各级政府和科技部门面前一项亟待解决的问题。为此,一是要提高认识,统一思想,切实增强策应规划的使命感和责任感;二是要结合实际,突出重点,全面对接鄱阳湖生态经济区规划;三是要加强领导,落实措施,确保吉安进位赶超、绿色崛起取得明显成效。