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61.
用差热、热重法对原丝的热性能及由不同预处理方法所引起的PVA纤维的热行为变化进行了研究;并通过模拟脱水条件,用不同升温速率,求出了经不同预处理纤维的脱水反应活化能。结果表明,PVA原丝在230℃有一软化点,三种预处理都不同程度地影响了原丝的热效应变化;纤维在180~340℃主要为脱水反应;原丝及经脱水剂、O_3和O_3综合脱水剂处理的纤维,其脱水反应的表观活化能分别为:164.3kJ/mol,92.9kJ/mol,130.5kJ/mol和117.6kJ/mol。 相似文献
62.
Guiying Li Ze He Taicheng An Xiangying Zeng Guoying Sheng Jiamo Fu 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2008,83(7):1019-1026
BACKGROUND: To investigate the microbial degradation performance of organic pollutants in the atmosphere using a biotrickling filter, two microorganism strains, Bacillus cereus S1 and Bacillus cereus S2, were selected, identified and inoculated into a twin biotrickling filter for comparison. RESULTS: Both strains showed good performance towards the degradation of model organic pollutants when gas flow rates ranged from 100 to 600 L h−1. For S1, the total maximum removal efficiency (RE) of toluene was maintained nearly 100% not only at gas flow rates of 100 L h−1 corresponding to empty bed residence time (EBRT) 199.44 s, but also at gas flow rates of 200 L h−1 (EBRT = 99.72 s) and 300 L h−1 (EBRT = 66.48 s). However, S2 had a much lower degradation capability; near 100% removal efficiency was obtained only at the gas flow rate of 100 L h−1 although both bacteria belong to the same Bacillus cereus. With further increase in gas flow rate, the total REs for both S1 and S2 decreased slightly at first and then dropped sharply to 46% and 35%, respectively, at an EBRT of 33.24 s, corresponding to a gas flow rate of 600 L h−1. Starvation for between 2 and 10 days resulted in the re‐acclimation times of both strains ranging between 1.0 and 15.5 h. CONCLUSION: Strain S1 would be a better choice for inoculation into a biotrickling filter than strain S2, because of its much higher toluene removal capacity and rapid recovery to full performance. Copyright © 2008 Society of Chemical Industry 相似文献
63.
正交实验优选盐生藻多糖的提取工艺 总被引:1,自引:0,他引:1
以盐生藻为原料,盐生藻多糖得率为指标,运用稀酸、稀碱和蒸馏水为提取剂提取盐生藻多糖,得出合适的提取剂为稀酸.进一步的正交实验表明,盐生藻多糖的最适提取工艺为:提取75min,pH=4,固液比为1∶70,温度为95℃. 相似文献
64.
65.
Associations (dimer or aggregate) of anthracene (An) fluorophores tend to interrupt the monomer emission and reduce the quantum yield (ΦPL); therefore, poly(methyl methacrylate) (PMMA) chain was used in this study to chemically link to anthracene and to block the mutual associations among the anthracene fluorophores. With this aim, the target polymers were prepared by anionic polymerizations with 9,10‐dibromoanthracene/s‐butyllithium as initiating system to proceed polymerizations of methyl methacrylate (MMA) directly or in the presence of 1,1‐diphenylethylene (DPE). Use of DPE before addition of MMA produces stable initiating anionic species and avoids potential side reactions during polymerization; however, it also introduces four β‐phenylene rings around the central anthracene ring, which interfere with the corresponding emission pattern and reduce the ΦPL (32%) value due to potential interactions between phenylene rings and anthracene. On the contrast, polymerization without participation of DPE results in polymer with central anthracene ring directly connected to two PMMA chains, which gives clean vibronic emission pattern with limited association emissions and enhanced ΦPL (52%) value. Physical blending of anthracene by PMMA is less efficient to restrain the associations and results in a film of lower ΦPL (20%). © 2007 Wiley Periodicals, Inc. J Appl Polym Sci, 2008 相似文献
66.
67.
介绍了福建炼油化工有限公司重整装置CB -60 /CB -70重整催化剂 (还原态 )分段组合装填的应用情况 ,列出了还原态催化剂和氧化态催化剂开工的不同特点。通过开工初期标定的数据与CB -6/CB -7催化剂的对比 ,说明CB -60 /CB -70催化剂有良好的活性和选择性 ,尤其是选择性、产氢率优于CB -6/CB -7,且使开工步骤得到了简化 相似文献
68.
GIS中实时建立区域拓扑关系的快速算法 总被引:1,自引:0,他引:1
针对GIS中建立区域拓扑关系的实时性要求,论文提出一个结合基于图的拓扑信息和基于几何的左转算法的区域拓扑关系生成算法。利用区域的连通性提高了算法效率,左转算法保证了算法的可靠性。 相似文献
69.
Facile synthesis of ordered nanocrystalline alumina thin films with tunable mesopore structures 总被引:1,自引:0,他引:1
Lijuan Wan Honggang Fu Keying Shi Xiqiang Tian 《Microporous and mesoporous materials》2008,115(3):301-307
Mesoporous alumina layers have attracted attention for their potential use in ultrafiltration of salts, as a heterogeneous catalyst support, an adsorbent in environmental cleanup, and in petroleum refinement. The ability to control the fast hydrolysis rate of the inorganic precursors using simple and inexpensive routes is important for that potential to be realized. Herein, we introduce a novel and facile route to synthesize mesoporous alumina thin films from the combination of inexpensive and commercially available copolymer with aluminum chloride or nitrate (salts) in an EtOH–surfactant–NH3 · H2O–salts (EsNs) system through the evaporation-induced self-assembly (EISA) method. Mesoporous alumina layers obtained utilizing the EsNs system have ordered and tunable pore structures. The ability to easily control the mesophases of the alumina layers within a short time provides distinct advantages over previously reported synthesis procedures. Most importantly, we demonstrate that the binding of surfactant and NH3 · H2O for the formation of hydrogen bond between them in the EsNs system controls the fast hydrolysis rate of the inorganic species. This allows for the synthesis of nanocrystalline alumina layers via the aluminum oxo-clusters’ assembly with the surfactant. Such simple route may be applied in the synthesis of other non-silica mesostructured oxides. 相似文献
70.
在2007年夏天一个难得凉爽的日子,我采访了思维严谨、幽默风趣的山西焦煤集团总经理柴久茂。听他解读的企业安全观,既科学实在,又引人深思,很受启发。如果每一个煤炭企业的带头人都有如此理性的安全发展观,那么我国煤矿的真正安宁和谐就会加快实现。 相似文献