里氏硬度法评估套筒灌浆料抗压强度

为研究装配式建筑中钢筋套筒连接灌浆料强度的无损检测技术,设计制作了4组套筒灌浆料试件,测试了其表面里氏硬度和抗压强度.结果表明：套筒灌浆料标准试件的表面里氏硬度服从正态分布,2次测试和对称侧面测试的结果具有重复性;采用剔除2个最大值和2个最小值的方法处理数据,套筒灌浆料表面里氏硬度离散性显著减小,偏差在±20HL;套筒灌浆料表面里氏硬度与其抗压强度具有显著相关性,采用指数回归拟合的综合效果最好.     

高层建筑结构舒适度的模糊可靠性分析及设计

根据模糊集和截集的概念,将模糊可靠性设计问题转化为常规可靠性设计问题。利用此观点对高层建筑结构的舒适度进行了模糊可靠性分析及设计研究。     

碳纤维增强塑料(CFRP)加固混凝土柱机理研究

介绍了碳纤维增强塑料的特点及其材料性能，并对CFRP加固混凝土柱的机理进行了分析论述，最后对今后的应用研究中需要解决的问题提出了建议，得出CFRP是一种新型的建筑材料，具有良好的发展前景。     

Extraction of palladium（Ⅱ） with OTMSO from acidic media

The extraction of palladium(Ⅱ) from acidic media with cyclic sulfoxide deriva-tive-α-octyl-tetrahydrothiophene-Ⅰ-oxide (OTMSO) was investigated. The extraction efficiency of palla-dium(Ⅱ) with OTMSO is 97.1% at 0.3mol·L~(-1) OTMSO. The plots of the extraction efficiency for palla-dium(Ⅲ) appear to lie on a convex curve having a minimum of extraction efficiency at 1-2 mol·L~(-1) HCl. Theextraction reaction of palladium(Ⅱ) with OTMSO is endothermic, and ΔH_(OTMSO)~=12.2kJ·mol~(-1). The coor-dination number was studied with slope method. The result indicates that coordination number is 2. FT-IRspectra were used to analyze the structure of complex and coordinated atom in complex. Pd is coordinated withboth oxygen and sulfur atom in S=O group in OTMSO. The situation and intensity of peaks contributed bycomplex prepared from various acidity were different. The recovery of palladium(Ⅱ) with OTMSO from scrapcontaining palladium was discussed. After silver and bismuth were removed, the feed solution w     

Collector matching in origin potential flotation

Through thermodynamic calculation and electrochemistry analysis~ taking the galena as example,the ba-sis for collector matching in origin potential flotation (OPF) was studied. The results of thermodynamic calculation show that the upper limit value of pH and flotation potential of diethyldithiocarbamate (DDTC) is higher than that of xanthogenate (KBX), which indicates that the collecting ability of DDTC for galena is better than that of KBX.The results of the interface capacitance analysis show that lead diethyldithiocarbamate (PbD2) is more steady than lead xanthogenate (Pb(BX)2) on the galena surface under the oxidation condition; the resistance analysis shows thatD2 (DDTC oxidizes into its dimmer) and dixanthogen (BX)2 will occur non-faradic desorption on the pyrite electrodesurface when the potentials are above 0.13 V and 0.2 V respectively. A synthetical criterion ΔE of collecting ability and selectivity was proposed. The results predicted by this criterion are confirmed through flotation experiments of ore.     

真空热处理对Ti6Al4V基体/NiCrAlY涂层体系组织结构及元素扩散行为的影响

采用电弧离子镀(AIP)技术在Ti6Al4V基体表面沉积制备了NiCrAlY涂层. 通过金相观察(OM)、扫描电镜(SEM)与能谱(EDS)分析、 X射线衍射(XRD)分析以及显微硬度测试, 研究了真空热处理对NiCrAlY涂层组织性能的影响, 讨论了Ti6Al4V基体/NiCrAlY涂层界面元素扩散规律. 结果表明: 700.℃真空热处理后, NiCrAlY涂层中开始析出γ′-Ni3Al相, 这提高了涂层的表面硬度; 在700.℃温度下, Ti6Al4V基体/NiCrAlY涂层界面由外至内出现Ni3(Al,Ti)、 TiNi和Ti2Ni中间化合物层, 并随着温度提高, 界面处中间化合物层增厚; 700.℃时, 主要发生了镍、钛元素的扩散, 铬元素在870.℃开始发生扩散. 当温度提高到950.℃后, 由于镍元素大量向Ti6Al4V基体扩散引起涂层的退化失效.     

Discussion on compact mechanism of air-stream and synchro-formed clamp plate impact molding

1 .Introduction Due to many advantages such as simple molding machine structure high compact compaction of sand mold, speed and well-distributed the air-stream impact molding method However, has been extensively used in production.when this molding method is applied to mold complicated pattern with wider top surface and deep     

镁合金无铬化学转化处理的研究第一部分——工艺参数的优化及膜层性能的测试

介绍了一种新型无毒的镁合金无铬化学转化处理方法。正交试验获得的最佳工艺参数为:8g/LNa ,0.5g/LCO32?,0.01g/L辅助成膜剂N,处理时间30min,处理温度30°C。研究了膜层的耐蚀性及其与不同漆膜之间的附着力。结果表明,在优化工艺下获得的膜层具有优良的耐蚀性(耐中性盐雾试验时间>96h)和漆膜附着力(达到1级)。     

不同熔渣对钢包铝镁铬材料渣蚀行为的影响

选取冶炼取向硅钢和铝镇静钢的精炼终渣及钢包用铝镁铬砖,采用静态坩埚法于1600 ℃×3 h下进行熔渣侵蚀试验,对渣蚀后试样作显微结构分析,并测定熔渣的化学成分和熔化温度.结果显示,随着熔渣中Al2O3含量的升高和碱度的增加,熔渣的熔点升高,粘度增加.粘度较大的熔渣与耐火材料接触后扩散较慢,对耐火材料的侵蚀和渗透减弱.并且当熔渣与耐火材料的反应产物为高熔点的CA2、CA6和MA尖晶石相且连续交错分布时,能堵塞液相扩散通道,抑制熔渣向耐火材料内部的进一步渗透.     

氧化铈复合钛酸镧钙介质陶瓷的微波性能

以1%(质量分数)CuO为烧结助剂,采用固相合成法制备了(1-x)Ca0.6La0.27TiO3 xCeO2单纯和复合微波介质陶瓷材料.研究了此体系陶瓷的微观结构和微波介电性能.研究表明:当x从0增加到1时,体系的相对介电常数εr从111.2线性降低到22.5;谐振频率温度系数τf从x=0时的正值 297.8×10-6/℃线性变化为x=1的负值-54.2×10-6/℃;而无载品质因数与谐振频率乘积Qf值则呈非线性增加.当x=0.85,且在1 400 ℃烧结,可获得εr=32.2,Qf=6682GHz,τf= 5×10-6/℃的新型微波介质陶瓷.