B2O3/TiO2-ZrO2催化剂上环己酮肟的气相Beckmann重排反应

用共沉淀法制备了TiO2-ZrO2复合氧化物载体，BET，DTA，XRD表征结果表明，该复合载体具有较大的比表面和较好的热稳定性，对于环己酮肟气相Beckmann重排反应制己内酰胺，用复合载体制备的B2O3／TiO2-ZrO2催化剂，比分别以TiO2,ZrO2为载体所制备的B2O3/TiO2和B2O3／ZrO2催化剂具有更高的活性和选择性，实验表明，催化剂表面中等强度的酸位是环己酮肟气相Beckmann重排反应的有效活性中心。     

水乳型丙烯酸酯建筑防水胶的研制(Ⅱ)

摘 要 研究水乳型丙烯酸酯建筑防水胶与水泥的配比及共混性能、共混固化物胶膜的力学性能、耐冷热性能及老化性能。     

催化裂化装置反应再生系统优化改造

重点介绍了呼和浩特石油化工公司重油催化裂化装置反应再生系统优化改造的目的、内容及运用的新技术;着重从物料平衡、原料及产品性质、催化剂性质、装置能耗、操作参数等方面与改造前进行了对比。装置改造后,在原料明显变重,催化剂单耗明显降低的情况下,生焦率下降了0.13个百分点,轻质油收率提高了3.54个百分点;汽油诱导期较改造前延长了140min,烯烃体积分数降低了1.9个百分点;柴油十六烷值比改造前提高了4个单位;装置能耗较改造前下降了906MJ/t,年创经济效益1030.9×10~4RMB￥。     

草酸二异辛酯的合成

以酸化膨润土(SO42-/Bentonite)固体酸为催化剂、草酸和异辛醇为原料合成草酸二异辛酯。考察了焙烧温度对催化剂活性的影响。结果表明,焙烧温度为500℃时催化剂活性最好。考察了反应温度、原料配比、催化剂用量和反应时间等因素对酯化反应的影响,确定了最佳酯化反应工艺条件,即n(异辛醇)∶n(草酸)为3.5∶1、w(SO42-/Bentonite)为2.0%、反应温度140℃、反应时间3 h;在该条件下草酸的转化率达到96.4%。催化剂重复使用6次后,草酸的转化率仍可达到94.4%。     

延长分米波电视发射管使用寿命的探讨（上）

文章从原理上讨论了影响分米波电视发射管寿命的若干因素。并提出了若干延长寿命的建议：（１）正确的灯丝加热方法是行之有效的措施，经验证明：过分强调降低灯丝电压往往得到相反的效果。（２）必须有良好的冷却方式。（３）通过对帘栅电路的分析，说明对此电路必须作很好的处理以消除故障和防止寄生振荡。     

Finite-difference analysis of dielectric-loaded cavities using thesimultaneous iteration of the power method with the Chebyshevacceleration technique

A numerical procedure using the finite-difference technique, simultaneous iteration based on the power method, and the Chebyshev-polynomial preconditioning is proposed to analyze dielectric-loaded cavities. The merit of this method is that no matrix inversions are invoked and the convergence rate of the power method is greatly accelerated by the preconditioning. The TE, TM, and hybrid modes in axisymmetrical cavities loaded with a rod or ring dielectric resonator are analyzed. For the hybrid modes, an H_r-H_z formulation is proposed. Accurate numerical results are obtained efficiently and no spurious solutions are found by the present method     

均匀设计在遗传算法中的应用研究

通过分析均匀设计和遗传算法的内在关系，指出从某个角度上可以把均匀设计看作是遗传算法的一种特例，并针对遗传算法初始参数众多、难配置的问题，提出了利用均匀设计优化配置选择参数的方法，在一定程度上可以避免遗传算法参数配置的盲目性．仿真试验结果证明了该方法是合理、可行的。     

Fuzzy estimation of feed-cutting force from current measurement-a case study on intelligent tool wear condition monitoring

It is very important to use a reliable and inexpensive sensor to obtain useful information about manufacturing processing, such as cutting force for monitoring automated machining. In this paper, the feed-cutting force is estimated using inexpensive current sensors installed on the ac servomotor of a computerized numerical control (CNC) turning center, with the results applied to the intelligent tool wear monitoring system. The mathematical model is used to disclose the implicit dependency of feed-cutting force on feed-motor current and feed speed. Afterwards, a neuro-fuzzy network is used to identify the cutting force with current measurement only. This hybrid math-fuzzy approach will reduce the modeling uncertainty and measurement cost. Finally, the estimated cutting force is applied in the tool-wear monitoring process. Successful experiments demonstrate robustness and effectiveness of the suggested method in the wide range of tool-wear monitoring applications.     

淤泥地基上土石围堰设计方案的探讨

新会区东南、中南部属冲积平原,西江、潭江两水横贯其中,岛丘众多,主干道时分时合,纵横交错,形成广阔的沙田地带,因此,堤围上也修建了相当数量的水闸,以满足防洪、排涝、航运以及灌溉的要求。水闸多为破堤而建,需要填筑围堰来保证主体工程的顺利施工。沙田地区的地基往往比较松软,淤泥层较厚,下面以金牛头水闸重建加固工程为例,探讨淤泥地基上土石围堰设计。     

~(141)CeO_2经气管内注入后在肺及淋巴结内的动态分布

本文报告了应用γ放射性测量和放射自显影方法,观察~(141)CeO_2经气管内注入后在大鼠肺及局部淋巴结中动态分布的特点。实验结果表明,~(141)Ce 在肺内与在不同部位、不同个体和单个淋巴结中的分布都是很不均匀的;其滞留量随时间而变化。